ES2664644T3 - Procedimiento destinado a preparar un producto polímero que presenta un grupo de ácido 2,5-furandicarboxilato dentro de la cadena principal del polímero para ser usado en aplicaciones de botellas, películas o fibras - Google Patents

Procedimiento destinado a preparar un producto polímero que presenta un grupo de ácido 2,5-furandicarboxilato dentro de la cadena principal del polímero para ser usado en aplicaciones de botellas, películas o fibras Download PDF

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Publication number
ES2664644T3
ES2664644T3 ES12781178.4T ES12781178T ES2664644T3 ES 2664644 T3 ES2664644 T3 ES 2664644T3 ES 12781178 T ES12781178 T ES 12781178T ES 2664644 T3 ES2664644 T3 ES 2664644T3
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Spain
Prior art keywords
furandicarboxylate
polymer
bottle
prepare
film
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ES12781178.4T
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Laszlo Sipos
Gerardus Johannes Maria Gruter
Jefffrey John KOLSTAD
Matheus Adrianus Dam
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Synvina CV
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Synvina CV
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/66—Polyesters containing oxygen in the form of ether groups
    • C08G63/668—Polyesters containing oxygen in the form of ether groups derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/672—Dicarboxylic acids and dihydroxy compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C49/00—Blow-moulding, i.e. blowing a preform or parison to a desired shape within a mould; Apparatus therefor
    • B29C49/0005—Blow-moulding, i.e. blowing a preform or parison to a desired shape within a mould; Apparatus therefor characterised by the material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C49/00—Blow-moulding, i.e. blowing a preform or parison to a desired shape within a mould; Apparatus therefor
    • B29C49/02—Combined blow-moulding and manufacture of the preform or the parison
    • B29C49/06—Injection blow-moulding
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
    • C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/16—Dicarboxylic acids and dihydroxy compounds
    • C08G63/18—Dicarboxylic acids and dihydroxy compounds the acids or hydroxy compounds containing carbocyclic rings
    • C08G63/181—Acids containing aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C08G63/80—Solid-state polycondensation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C08G63/82—Preparation processes characterised by the catalyst used
    • C08G63/85—Germanium, tin, lead, arsenic, antimony, bismuth, titanium, zirconium, hafnium, vanadium, niobium, tantalum, or compounds thereof
    • C08G63/86—Germanium, antimony, or compounds thereof
    • C08G63/866—Antimony or compounds thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C49/00—Blow-moulding, i.e. blowing a preform or parison to a desired shape within a mould; Apparatus therefor
    • B29C49/02—Combined blow-moulding and manufacture of the preform or the parison
    • B29C2049/023—Combined blow-moulding and manufacture of the preform or the parison using inherent heat of the preform, i.e. 1 step blow moulding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2023/00—Use of polyalkenes or derivatives thereof as moulding material
    • B29K2023/04—Polymers of ethylene
    • B29K2023/06—PE, i.e. polyethylene
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29L—INDEXING SCHEME ASSOCIATED WITH SUBCLASS B29C, RELATING TO PARTICULAR ARTICLES
    • B29L2031/00—Other particular articles
    • B29L2031/712—Containers; Packaging elements or accessories, Packages
    • B29L2031/7158—Bottles

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Polyesters Or Polycarbonates (AREA)

Abstract

Procedimiento para preparar un polímero de poli(etilen-2,5-furandicarboxilato) que presenta un número que expresa el peso molecular medio de por lo menos 25.000, según se determina mediante GPC basándose en estándares de poliestireno, comprendiendo el procedimiento (a) una primera etapa que es (i) una etapa de transesterificación en la que el éster dimetil-2,5-furandicarboxilato (diéster) se transesterifica con etilenglicol (diol) en presencia de un catalizador de transesterificación; o (ii) proporcionar una mezcla de reacción fundida que comprende bis(2-hidroxietil)-2,5- furandicarboxilato; (b) una etapa de policondensación a presión reducida, preferentemente inferior a 1 mbar y a una temperatura elevada, preferentemente inferior a 240 °C, en la que en condiciones de fusión el producto preparado en la etapa (a) reacciona en presencia de un catalizador de policondensación y elimina el condensado del reactor; (c) secar y/o cristalizar el condensado obtenido a una temperatura comprendida entre 90 °C y 160 °C; y (d) someter el polímero de la etapa (c) a unas condiciones de condensación que comprenden un tratamiento a una temperatura elevada que finaliza a una temperatura de por lo menos 190 °C para obtener de este modo un polímero de poli(etilen-2,5-furandicarboxilato) que presenta un número que expresa el peso molecular medio de por lo menos 25.000.

Description

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Claims (1)

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ES12781178.4T 2011-10-24 2012-10-24 Procedimiento destinado a preparar un producto polímero que presenta un grupo de ácido 2,5-furandicarboxilato dentro de la cadena principal del polímero para ser usado en aplicaciones de botellas, películas o fibras Active ES2664644T3 (es)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201161550707P 2011-10-24 2011-10-24
US201161550707P 2011-10-24
NL2007650 2011-10-25
NL2007650 2011-10-25
PCT/NL2012/050738 WO2013062408A1 (en) 2011-10-24 2012-10-24 A process for preparing a polymer product having a 2,5-furandicarboxylate moiety within the polymer backbone to be used in bottle, film or fibre applications

Publications (1)

Publication Number Publication Date
ES2664644T3 true ES2664644T3 (es) 2018-04-20

Family

ID=48168128

Family Applications (1)

Application Number Title Priority Date Filing Date
ES12781178.4T Active ES2664644T3 (es) 2011-10-24 2012-10-24 Procedimiento destinado a preparar un producto polímero que presenta un grupo de ácido 2,5-furandicarboxilato dentro de la cadena principal del polímero para ser usado en aplicaciones de botellas, películas o fibras

Country Status (14)

Country Link
US (2) US9527954B2 (es)
EP (2) EP2771382B1 (es)
JP (1) JP6621237B2 (es)
KR (2) KR102250679B1 (es)
CN (1) CN104024301B (es)
BR (1) BR112014009029B1 (es)
CA (2) CA3061795C (es)
ES (1) ES2664644T3 (es)
IN (1) IN2014MN00871A (es)
MX (1) MX351452B (es)
MY (1) MY176989A (es)
SG (1) SG11201401745UA (es)
WO (1) WO2013062408A1 (es)
ZA (1) ZA201403397B (es)

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