TR201908177T4 - Bir co(ıı) veya ce(ııı) katalizörü, bir bromür tuzu ve bir solvent varlığında 5-(alkiloksimetil)furfuralin (AMF) oksijen ile oksidasyonu aracılığıyla 2,5-furandikarboksilik asidin (FDCA) hazırlanışına yönelik proses. - Google Patents

Bir co(ıı) veya ce(ııı) katalizörü, bir bromür tuzu ve bir solvent varlığında 5-(alkiloksimetil)furfuralin (AMF) oksijen ile oksidasyonu aracılığıyla 2,5-furandikarboksilik asidin (FDCA) hazırlanışına yönelik proses. Download PDF

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Publication number
TR201908177T4
TR201908177T4 TR2019/08177T TR201908177T TR201908177T4 TR 201908177 T4 TR201908177 T4 TR 201908177T4 TR 2019/08177 T TR2019/08177 T TR 2019/08177T TR 201908177 T TR201908177 T TR 201908177T TR 201908177 T4 TR201908177 T4 TR 201908177T4
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fdca
amf
furfural
solvent
alkyloxymethyl
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TR2019/08177T
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Sanborn Alexandra
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Archer Daniels Midland Co
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/68—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Furan Compounds (AREA)

Abstract

Bir Co(II) veya Ce(III) katalizörü, bir bromür tuzu ve bir solvent varlığında oksijen ile 5-(hidroksimetil)furfural (HMF) veya 5-(alkiloksimetil)furfuralın (AMF) oksidasyonu aracılığıyla 2,5-furandikarboksilik asit (FDCA) hazırlanışına yönelik bir prosestir. AMF, akabinde FDCA'ya hidrolizlenen ara ürün bileşiği 5-(alkoksikarbonil)furankarboksilik aside (AcMFA) oksitlenir. Proses tercihen T=80-130°C ve 800-1000 psi?de gerçekleştirilir. Asetik asit tercih edilen solventtir.
TR2019/08177T 2009-05-14 2010-05-14 Bir co(ıı) veya ce(ııı) katalizörü, bir bromür tuzu ve bir solvent varlığında 5-(alkiloksimetil)furfuralin (AMF) oksijen ile oksidasyonu aracılığıyla 2,5-furandikarboksilik asidin (FDCA) hazırlanışına yönelik proses. TR201908177T4 (tr)

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US17830109P 2009-05-14 2009-05-14

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TR201908177T4 true TR201908177T4 (tr) 2019-06-21

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TR2019/08177T TR201908177T4 (tr) 2009-05-14 2010-05-14 Bir co(ıı) veya ce(ııı) katalizörü, bir bromür tuzu ve bir solvent varlığında 5-(alkiloksimetil)furfuralin (AMF) oksijen ile oksidasyonu aracılığıyla 2,5-furandikarboksilik asidin (FDCA) hazırlanışına yönelik proses.

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US (1) US8558018B2 (tr)
EP (5) EP2784069B2 (tr)
CN (2) CN102459214B (tr)
BR (2) BR122017024876B1 (tr)
ES (2) ES2730100T3 (tr)
PL (1) PL2430010T3 (tr)
TR (1) TR201908177T4 (tr)
WO (1) WO2010132740A2 (tr)

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