WO2006049546A1 - Pigment composition in the form of aqueous dispersion - Google Patents

Pigment composition in the form of aqueous dispersion Download PDF

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Publication number
WO2006049546A1
WO2006049546A1 PCT/SE2005/001523 SE2005001523W WO2006049546A1 WO 2006049546 A1 WO2006049546 A1 WO 2006049546A1 SE 2005001523 W SE2005001523 W SE 2005001523W WO 2006049546 A1 WO2006049546 A1 WO 2006049546A1
Authority
WO
WIPO (PCT)
Prior art keywords
composition
particles
silica
pigment
paper
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/SE2005/001523
Other languages
English (en)
French (fr)
Inventor
Kjell Rune Andersson
Joakim Carlen
Erik Lindgren
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Akzo Nobel NV
Nouryon Pulp and Performance Chemicals AB
Original Assignee
Akzo Nobel NV
Eka Chemicals AB
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to MX2007003617A priority Critical patent/MX2007003617A/es
Priority to JP2007540280A priority patent/JP5159312B2/ja
Priority to CA2586205A priority patent/CA2586205C/en
Priority to BRPI0517258-6A priority patent/BRPI0517258A/pt
Priority to EP05793349A priority patent/EP1809711A1/en
Priority to AU2005301350A priority patent/AU2005301350B2/en
Application filed by Akzo Nobel NV, Eka Chemicals AB filed Critical Akzo Nobel NV
Priority to CN2005800358612A priority patent/CN101426865B/zh
Priority to NZ554299A priority patent/NZ554299A/en
Publication of WO2006049546A1 publication Critical patent/WO2006049546A1/en
Anticipated expiration legal-status Critical
Priority to NO20072903A priority patent/NO20072903L/no
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D17/00—Pigment pastes, e.g. for mixing in paints
    • C09D17/004—Pigment pastes, e.g. for mixing in paints containing an inorganic pigment
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D17/00—Pigment pastes, e.g. for mixing in paints
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/34—Silicon-containing compounds

Definitions

  • US Patent 4554181 discloses a recording surface including a combination of a water soluble polyvalent metal and a cationic polymer.
  • US Patent Application Publication 2004/0255820 discloses a pigment that is surface treated with a water-soluble polyvalent metal salt.
  • one aspect of the invention concerns a pigment composition in the form of an aqueous dispersion comprising:
  • Colloidal primary particles of silica or aluminosilicate have preferably been formed from an aqueous solution of alkali metal silicate where alkali metal ions are removed through an ion exchange process or where the pH of the alkali metal silicate solution has been reduced by the addition of an acid.
  • a process based on ion exchange follows the basic principles described in R.K. Her, "The Chemistry of Silica” 1979, pages 333-334 and results in an aqueous sol comprising colloidal negatively or positively charged particles of silica or aluminosilicate.
  • a process based on pH-reduction of alkali metal silicate follows the basic principles described in e.g. US patents 5176891 , 5648055, 5853616, 5482693, 6060523 and 6274112.
  • sols comprise colloidal primary particles of silica that may or may not be surface modified, for example with a metal oxide such as oxide of aluminium, titanium, chromium, zirconium, boron or any other suitable metal.
  • a metal oxide such as oxide of aluminium, titanium, chromium, zirconium, boron or any other suitable metal.
  • the surface area of the primary particles is from about 30 m 2 /g to about 600 m 2 /g, more preferably from about 30 to about 450 m 2 /g, most preferably from about 40 m 2 /g to about 400 m 2 /g particularly most preferably from about 50 m 2 /g to about 300 m 2 /g.
  • the dry content of the aqueous sol of primary particles is preferably from about 0.5 wt% to about 60 wt%, most preferably from about 1 wt% to about 50 wt%.
  • Suitable aqueous sols of colloidal primary particles of silica or aluminosilicate are commercially available, for example under the trademarks LudoxTM, SnowtexTM, BindzilTM, NyacolTM, VinnsilTM or FennosilTM.
  • a sol formed by dispersing a powder of e.g. precipitated silica, gel-type silica or fumed silica the colloidal particles in a sol prepared from alkali metal silicate by ion exchange or pH-reduction have never been dried to a powder, such as in the case for e.g. precipitated silica or gel-type silica.
  • Aggregation of primary particles in a sol to form a dispersion of porous aggregates may be performed with any suitable method, such as those described in R. K. Her, "The Chemistry of Silica” 1979, pages 364-407.
  • the degree of aggregation can be followed by measuring the viscosity and applying the Einstein and Mooney equations (see e.g. R.K. Her, "The Chemistry of Silica” 1979, pages 360-364).
  • the aggregation may be performed as a separate step or in a mixture also comprising other pigment particles.
  • a salt preferably selected from divalent, multivalent or complex salts, is added to an anionic or cationic sol also resulting in the formation of porous aggregates.
  • salts are aluminium chloride, poly aluminium chloride, poly aluminium silicate sulfate, aluminium sulfate, zirconium carbonates, zirconium acetates, alkali metal borates, and mixtures thereof.
  • a bridging substance is used to form the aggregates from the primary particles.
  • Each porous aggregate is formed from at least three primary particles, which inherently gives at least some pores.
  • the mean particle diameter of the aggregates is preferably from about 0.03 to about 25 ⁇ m, more preferably from about 0.05 to about 10 ⁇ m, most preferably from about 0.1 ⁇ m to about 5 ⁇ m. It is to be understood that the average diameter of the porous aggregates is always larger than the average diameter of the primary particles they are formed from.
  • the surface area of the aggregates is usually essentially the same as of the primary particles.
  • the pigment particles of synthetic amorphous silica or aluminosilicate is a mixture of colloidal particles in a sol prepared from alkali metal silicate by ion exchange or pH-reduction, optionally partially or fully aggregated, with particles of one or more of precipitated silica, gel-type silica or fumed silica.
  • the water soluble aluminium salt in the pigment composition can be any aluminium containing salt and is preferably present in an amount from about 0.1 wt% to about 30 wt% most preferably from about 0.2 wt% to about 15 wt%, calculated as wt% AI 2 O 3 on dry pigment particles.
  • salts include aluminium chloride, poly aluminium chloride, poly aluminium silicate sulfate, aluminium sulfate, zirconium carbonates, zirconium acetates , and mixtures thereof.
  • the aluminium may be present partly or fully on the surface of the particles of silica or aluminosilicate or in the aqueous phase.
  • the cationic polymer in the pigment composition has a molecular weight from about 2000 to about 1000000, preferably from about 2000 to about 500000, most preferably from about 5000 to about 200000.
  • the charge density is from about 0.2 meq/g to about 12 meq/g, preferably from about 0.3 meq/g to about 10 meq/g, most preferably from about 0.5 meq/g to about 8 meq/g.
  • the cationic polymer is preferably present in the pigment dispersion in an amount from about 0.1 wt% to about 30 wt%, more preferably from about 0.5 wt% to about 20 wt%, most preferably from about 1 wt% to about 15 wt%, based on the amount of dry pigment particles.
  • the composition further comprises other kinds of pigment particles such as kaolinites, smectites, talcites, calcium carbonate minerals, precipitated calcium carbonate, and mixtures thereof.
  • the content of synthetic amorphous silica or aluminosilicate particles is preferable from about 10 to 100 wt%, most preferable from about 30 wt% to 100 wt% of the total amount of pigment particles.
  • the pigment composition may also comprise other additives commonly used for paper coating such as stabilisers, rheology modifiers, optical brighteners, lubricants, insolubilizers, dyes, sizing agents etc, as well as various impurities from the raw materials.
  • the dry content of the pigment composition is preferably from about 2 wt% to about 75 wt%, most preferably from about 10 wt% to about 70 wt%.
  • the total amount of other additives (apart from optional binders) and possible impurities is preferably from 0 to about 50 wt%, most preferably from 0 to about 30 wt%, based on the dry content.
  • the invention further relates to a process for the production of a pigment composition as described above comprising mixing particles of synthetic amorphous silica or aluminosilicate, a water soluble aluminium salt and a cationic polymer having a molecular weight from about 2000 to about 1000000 and a charge density from about 0.2 meq/g to about 12 meq/g to an aqueous dispersion in a way so substantial gelling or precipitation is avoided.
  • This can be achieved by several alternative process embodiments.
  • Another alternative process comprises a step of adding particles of synthetic amorphous silica or aluminosilicate to an aqueous solution of a cationic polymer as described above followed by adding a water soluble aluminium salt.
  • Other components such as other pigment particles or binders may be added at any stage in the form of solids, liquids or dispersions.
  • the silica or aluminium silicate particles may be in the form of a solid powder or an aqueous sol of colloidal particles, that may be anionic or cationic. Unless a cationic sol is used, the cationic polymer is preferably in such an excess that it is sufficient for rendering the resulting dispersion predominantly cationic. At least if an anionic sol is used, there may be at least some aggregation of the colloidal particles.
  • Still another process embodiment comprises a step of mixing a cationic aluminium modified aqueous sol of colloidal silica or aluminosilicate with a cationic polymer.
  • a cationic aluminium modified aqueous sol of colloidal silica or aluminosilicate with a cationic polymer.
  • Other components such as other pigment particles or binders may be added at any stage in the form of solids, liquids or dispersions. Regarding suitable and preferred amounts and kinds of the components, the above description of the pigment composition is referred to.
  • the invention also concerns the use of a pigment composition as described above for coating paper or paper board.
  • the invention further concerns a process for the production of coated paper or paperboard comprising a step of applying a pigment composition as described above as a coating to at least one side of a paper or paperboard web.
  • coating refers to any method in which pigments are applied to the surface of paper or paper board, thus including not only conventional coating but also other methods such as for example pigmenting.
  • the invention finally concerns paper or paper board suitable for ink-jet printing obtainable by a process as described above.
  • Such paper or paper board comprises a substantially transparent or substantially non-transparent layer comprising pigment particles of synthetic amorphous silica or aluminosilicate and optionally other pigment particles from the coating composition, the pigment particles preferably forming a nano- structure.
  • the dry amount of coating is preferably from about 0.5 g/m 2 to about 50 g/m 2 , most preferably from about 1.0 g/m 2 to about 25 g/m 2 .
  • the amount of pigment particles from the above described pigment composition per coated side of the paper or paper board is preferably from about 0.7 g/m 2 to about 40 g/m 2 , most preferably from about 1 g/m 2 to about 20 g/m 2 . Preferably no other kind of coating has been applied on top of this layer.
  • the paper or paper board of the invention have particularly good properties for ink-jet printing, giving low line blurriness and mottling and high printing density for colours, but can advantageously also be used for other kinds of printing processes like toner, flexography, letter press, gravure, offset lithography and screen printing. It is a particular advantage that such good properties can be obtained in a simple manner by applying only small amounts of the coating and without the need to apply numerous different coating layers on the paper or paper board. This also enable the coating to be applied with a size press, such as a film press, which for practical reasons is advantageous. Furthermore, the main components of the pigment composition can be made from readily available raw materials.
  • LocronTM was diluted with 3.5 g water and SylojetTM-PVA slurry was mixed with the
  • the print results were evaluated using a print picture with seven colour blocs: cyan, magenta, yellow, red, green, blue and black.
  • the printed blocs and the unprinted paper were measured with a spectrophotometer (Color Touch 2 from Technidyne) and the colour gamut volume was calculated.
  • the gamut volume is approximated with a dodecahedral in the CEI L*a*b* colour space and the measurements of the colours give the corners in the dodecahedral (see "Rydefalk Staffan, Wedin Michael; Litterature review on the colour Gamut in the Printing Process-Fundamentals, PTF-report no 32, May 1997").
  • the results are shown in the table below:
  • Example 2 In these formulation pigment blends with equal parts (dry/dry) of the gel-type silica used was SylojetTM P612 (same as in Example 1) and an anionic silica sol, NyacolTM 9950 from Eka Chemicals, a 50 wt% sol with a mean particle size of 100 nm. As binder the same amount and the same kind of PVA as in Example 1 was used. Two coating formulations with a total pigment content of 20 wt% were prepared. A) 5 g dry silica gel (SylojetTM P612) was dispersed in solution containing 10 g NyacolTM 9950., 20 g 10 wt% PVA and 15 g water under UltraTurraxTM mixing (lO OOOrpm).
  • Example 3 In the test an anionic silica sol, BindzilTM 50/80 from Eka Chemicals was used as pigment, a 50 wt% sol with a mean particle size of 40 nm. Two formulations were prepared without any PVA-binder. A) BindzilTM 50/80 diluted to 30 wt%. B) 6 g LocronTM was diluted with 20 g water and 60 g of BindzilTM 50/80 was added under vigorous mixing (UltraTurraxTM). The mixing continued during the addition of 3 g polyDADMAC (same as in example 1) and 11 g water. The final concentration of silica became 30 wt%.
  • Example 2 Following the same procedure as in Example 1, the coatings were applied to paper and dried (coat weight 8-9 g/m 2 ) and evaluated on two printers. The results are shown in the table below:

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Paper (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)
  • Ink Jet Recording Methods And Recording Media Thereof (AREA)
  • Paints Or Removers (AREA)
  • Ink Jet (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
PCT/SE2005/001523 2004-11-08 2005-10-13 Pigment composition in the form of aqueous dispersion Ceased WO2006049546A1 (en)

Priority Applications (9)

Application Number Priority Date Filing Date Title
JP2007540280A JP5159312B2 (ja) 2004-11-08 2005-10-13 水性分散液の形態の顔料組成物
CA2586205A CA2586205C (en) 2004-11-08 2005-10-13 Pigment composition in the form of aqueous dispersion
BRPI0517258-6A BRPI0517258A (pt) 2004-11-08 2005-10-13 composição de pigmento na forma de dispersão aquosa
EP05793349A EP1809711A1 (en) 2004-11-08 2005-10-13 Pigment composition in the form of aqueous dispersion
AU2005301350A AU2005301350B2 (en) 2004-11-08 2005-10-13 Pigment composition in the form of aqueous dispersion
MX2007003617A MX2007003617A (es) 2004-11-08 2005-10-13 Composicion de pigmento en la forma de dispersion acuosa.
CN2005800358612A CN101426865B (zh) 2004-11-08 2005-10-13 水分散体系形式的颜料组合物
NZ554299A NZ554299A (en) 2005-10-13 2005-10-13 Pigment composition with silica in the form of aqueous dispersion for coating paper
NO20072903A NO20072903L (no) 2004-11-08 2007-06-07 Pigmentsammensetning i formen av vandig dispersjon

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP04105595.5 2004-11-08
EP04105595 2004-11-08

Publications (1)

Publication Number Publication Date
WO2006049546A1 true WO2006049546A1 (en) 2006-05-11

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PCT/SE2005/001523 Ceased WO2006049546A1 (en) 2004-11-08 2005-10-13 Pigment composition in the form of aqueous dispersion
PCT/SE2005/001522 Ceased WO2006049545A1 (en) 2004-11-08 2005-10-13 Pigment composition in the form of aqueous dispersion
PCT/SE2005/001524 Ceased WO2006049547A1 (en) 2004-11-08 2005-10-13 A process for the production of coated paper

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PCT/SE2005/001522 Ceased WO2006049545A1 (en) 2004-11-08 2005-10-13 Pigment composition in the form of aqueous dispersion
PCT/SE2005/001524 Ceased WO2006049547A1 (en) 2004-11-08 2005-10-13 A process for the production of coated paper

Country Status (16)

Country Link
EP (3) EP1809712A1 (https=)
JP (3) JP5159312B2 (https=)
KR (3) KR100887002B1 (https=)
CN (3) CN101056955B (https=)
AR (3) AR051756A1 (https=)
AU (3) AU2005301350B2 (https=)
BR (3) BRPI0517262A (https=)
CA (3) CA2586207C (https=)
MX (3) MX2007004959A (https=)
MY (3) MY145100A (https=)
NO (3) NO20072903L (https=)
NZ (1) NZ554297A (https=)
RU (3) RU2375397C2 (https=)
TW (3) TWI308583B (https=)
WO (3) WO2006049546A1 (https=)
ZA (3) ZA200704417B (https=)

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WO2010149676A1 (en) 2009-06-26 2010-12-29 Akzo Nobel Chemicals International B.V. Coated substrate and method for the preparation thereof
US8114486B2 (en) 2006-02-28 2012-02-14 Evonik Degussa Corporation Colored paper and substrates coated for enhanced printing performance
US8834680B2 (en) 2007-07-16 2014-09-16 Akzo Nobel N.V. Filler composition
US11479917B2 (en) 2014-03-14 2022-10-25 Stora Enso Oyj Method for manufacturing a packaging material and a packaging material made by the method

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US8057637B2 (en) 2007-12-26 2011-11-15 International Paper Company Paper substrate containing a wetting agent and having improved print mottle
ES2390619T3 (es) 2008-03-31 2012-11-14 International Paper Company Hoja de impresión con calidad mejorada de impresión a niveles bajos de aditivos
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US8460511B2 (en) 2008-10-01 2013-06-11 International Paper Company Paper substrate containing a wetting agent and having improved printability
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US8574690B2 (en) 2009-12-17 2013-11-05 International Paper Company Printable substrates with improved dry time and acceptable print density by using monovalent salts
US8652593B2 (en) 2009-12-17 2014-02-18 International Paper Company Printable substrates with improved brightness from OBAs in presence of multivalent metal salts
US8440053B2 (en) 2010-04-02 2013-05-14 International Paper Company Method and system using surfactants in paper sizing composition to inhibit deposition of multivalent fatty acid salts
US8608908B2 (en) 2010-04-02 2013-12-17 International Paper Company Method and system using low fatty acid starches in paper sizing composition to inhibit deposition of multivalent fatty acid salts
WO2011139481A1 (en) 2010-05-04 2011-11-10 International Paper Company Coated printed substrates resistant to acidic highlighters and printing solutions
SE536746C2 (sv) * 2010-05-12 2014-07-08 Stora Enso Oyj En komposition innehållande mikrofibrillerad cellulosa och en process för tillverkning av en komposition
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JP5575594B2 (ja) * 2010-09-17 2014-08-20 富士フイルム株式会社 インク組成物、インクセットおよび画像形成方法
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EP2640894B2 (en) 2010-11-17 2020-07-01 Hewlett-Packard Development Company, L.P. Surface sizing composition for print media in digital printing
JP5817601B2 (ja) * 2012-03-14 2015-11-18 株式会社リコー トナー、並びに、現像剤及び画像形成装置
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FI126543B (fi) * 2013-05-17 2017-02-15 Fp-Pigments Oy Menetelmä pigmenttejä sisältävän kationisen, korkean kuiva-aineen vesidispersion valmistamiseksi, pigmenttejä käsittävä vesidispersio ja sen käyttö
KR101637934B1 (ko) * 2015-03-30 2016-07-08 한국화학연구원 다공성 알루미노 실리카의 제조방법 및 이에 따라 제조되는 다공성 알루미노 실리카
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US8834680B2 (en) 2007-07-16 2014-09-16 Akzo Nobel N.V. Filler composition
EP2362016B1 (en) 2007-07-16 2019-01-30 Akzo Nobel Chemicals International B.V. Filler composition
WO2010149676A1 (en) 2009-06-26 2010-12-29 Akzo Nobel Chemicals International B.V. Coated substrate and method for the preparation thereof
US11479917B2 (en) 2014-03-14 2022-10-25 Stora Enso Oyj Method for manufacturing a packaging material and a packaging material made by the method

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