JP7381613B2 - アニオン性界面活性剤を含有する溶解性固体繊維性物品 - Google Patents
アニオン性界面活性剤を含有する溶解性固体繊維性物品 Download PDFInfo
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- JP7381613B2 JP7381613B2 JP2021573208A JP2021573208A JP7381613B2 JP 7381613 B2 JP7381613 B2 JP 7381613B2 JP 2021573208 A JP2021573208 A JP 2021573208A JP 2021573208 A JP2021573208 A JP 2021573208A JP 7381613 B2 JP7381613 B2 JP 7381613B2
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- VZTGWJFIMGVKSN-UHFFFAOYSA-O trimethyl-[3-(2-methylprop-2-enoylamino)propyl]azanium Chemical group CC(=C)C(=O)NCCC[N+](C)(C)C VZTGWJFIMGVKSN-UHFFFAOYSA-O 0.000 description 1
- XFNJVJPLKCPIBV-UHFFFAOYSA-P trimethylenediaminium Chemical compound [NH3+]CCC[NH3+] XFNJVJPLKCPIBV-UHFFFAOYSA-P 0.000 description 1
- 238000001797 two-dimensional small-angle X-ray scattering Methods 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 229940100445 wheat starch Drugs 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
- 239000000230 xanthan gum Substances 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 description 1
- 239000004711 α-olefin Substances 0.000 description 1
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Description
「溶解性」は、溶解性固体物品が水に完全に溶解するか、又は、以下に記載するハンド溶解試験に従って、水中で混合すると均一な分散液をもたらすことを意味する。溶解性固体物品は、ハンド溶解法によって測定されるとき、約1~約30ストローク、あるいは約2~約25ストローク、あるいは約3~約20ストローク、またあるいは約4~約15ストロークのハンド溶解値を有することができる。
本発明の繊維性物品は、複数の繊維要素、例えば、複数のフィラメントを含むことができる。
本発明の、フィラメント及び/又は繊維などの繊維要素は、1つ以上のポリマー構造化剤を含む。ポリマー構造化剤に加えて、繊維要素は、界面活性剤系と、比較的高い重量平均分子量のカチオン性ポリマーを含む任意成分と、を更に含んでもよい。繊維要素の例は、米国特許出願第16/431,115号に見出すことができ、当該文献は参照により組み込まれる。
溶解性繊維性物品及び/又は繊維要素は、乾燥繊維要素換算及び/若しくは乾燥溶解性繊維性物品換算で、並びに/又は繊維要素形成組成物の、約1重量%~90重量%、あるいは10重量%~約80重量%、あるいは約20重量%~約70重量%、あるいは約30重量%~約65重量%、またあるいは約35重量%~約60重量%のポリマー構造化剤を含むことができる。
溶解性繊維性物品及び/又は繊維要素は、乾燥繊維要素換算及び/若しくは乾燥溶解性繊維性物品換算で、並びに/又は繊維要素形成組成物の、約10重量%~約90重量%、あるいは約20重量%~約80重量%、あるいは約30重量%~約70重量%、またあるいは約40重量%~約65重量%の界面活性剤系を含有することができる。
RO(CH2CH2O)nSO3M
式中、Rは、8~18個の炭素、あるいは12~18個の炭素を有するアルキル又はアルケニルであり、nは、少なくとも0.5超、あるいは2~3の平均値を有し、Mは、ナトリウム、カリウム、アンモニウム、又は置換アンモニウムなどの可溶化カチオンである。
繊維性物品は、繊維要素形成組成物の、又は乾燥繊維要素換算及び/若しくは乾燥溶解性繊維性物品換算で、約0.05重量%~約5重量%のカチオン性ポリマー、約0.1重量%~約2重量%のカチオン性ポリマー、約0.2重量%~約1.5重量%のカチオン性ポリマー、約0.3重量~約1.0重量%のカチオン性ポリマー、約0.4重量%~約0.75重量%のカチオン性ポリマーを含有することができる。
ヘアケア組成物は、(a)カチオン性グアーポリマーを含み得る。カチオン性グアーポリマーは、カチオン的に置換されたガラクトマンナン(グアー)ガム誘導体である。これらのグアーガム誘導体の調製に用いられるグアーガムは、典型的に、グアープラントの種から天然に産出される材料として得られる。グアー分子自体は、単員ガラクトース単位が交互にマンノース単位上にある、一定の間隔で分岐する直鎖状マンナンである。マンノース単位は、β(1-4)グリコシド結合によって互いに結合している。ガラクトース分岐は、α(1-6)結合によって生じる。グアーガムのカチオン性誘導体は、ポリガラクトマンナンのヒドロキシル基と反応性四級アンモニウム化合物との間の反応によって得られる。グアー構造上へのカチオン性基の置換度は、上述の必要なカチオン性電荷密度を提供するのに十分でなくてはならない。
ヘアケア組成物は、(b)約1,000g/mol~約200万g/mol未満の重量平均分子量を有し得るカチオン性合成ポリマーを含み得、カチオン性グアーポリマーは、約2meq/g~約10meq/gの電荷密度を有し得る。ヘアケア組成物は、組成物の総重量に対して約0.01%~約2.5%のカチオン性合成ポリマーを含み得る。
i)1つ以上のカチオン性モノマー単位、及び任意に、
ii)負電荷を有する1つ以上のモノマー単位、及び/又は
iii)非イオン性モノマー、から形成され得る。
ここで、コポリマーの次の電荷は正電荷である。これらの3種のモノマーの比は「m」、「p」及び「q」で表され、ここで「m」は、カチオン性モノマーの数であり、「p」は、負電荷を有するモノマーの数であり、「q」は、非イオン性モノマーの数である。
Yは、C1~C22アルキル、アルコキシ、アルキリデン、アルキル、又はアリールオキシであり、
Ψは、C1~C22アルキル、アルキルオキシ、アルキルアリール又はアルキルアリールオキシであり、
Zは、C1~C22アルキル、アルキルオキシ、アリール又はアリールオキシであり、
R1は、H、C1~C4の直鎖又は分枝鎖アルキルであり、
sは、0又は1であり、nは、0又は≧1であり、
T及びR7は、C1~C22アルキルであり、
X-は、ハロゲン、ヒドロキシド、アルコキシド、サルフェート又はアルキルサルフェートである。
分散組成物は、モノマー対モノマー基準でマンノースとガラクトースとの比が5:1~1:1であるガラクトマンナンポリマー誘導体を含んでもよく、ガラクトマンナンポリマー誘導体は、カチオン性ガラクトマンナンポリマー誘導体、及び正味の正電荷を有する両性ガラクトマンナンポリマー誘導体からなる群から選択される。本明細書で使用するとき、用語「カチオン性ガラクトマンナン」は、カチオン性基が付加されたガラクトマンナンポリマーを指す。用語「両性ガラクトマンナン」は、ポリマーが正味の正電荷を有するようにカチオン性基及びアニオン性基が付加されたガラクトマンナンポリマーを指す。
分散組成物は水溶性のカチオン変性デンプンポリマーを含み得る。本明細書で使用するとき、用語「カチオン変性デンプン」とは、デンプンが分解されて比較的小さい重量平均分子量に達する前にカチオン性基が付加されたデンプン、又はデンプンの変性後にカチオン性基が付加されて所望の重量平均分子量に達したデンプンを指す。用語「カチオン変性デンプン」の定義には、両性変性デンプンも含まれる。用語「両性変性デンプン」とは、カチオン性基及びアニオン性基が付加されたデンプン加水分解物を指す。
分散組成物は、アクリルアミドモノマーとカチオン性モノマーとのカチオン性コポリマーを含み得る。カチオン性コポリマーは、アクリルアミドモノマーとカチオン性モノマーとの合成カチオン性コポリマーであってよい。
(i)次式AMのアクリルアミドモノマー:
式中、R9は、H又はC1~4アルキルであり、R10及びR11は、独立して、H、C1~4アルキル、CH2OCH3、CH2OCH2CH(CH3)2、及びフェニルからなる群から選択されるか、共にC3~6シクロアルキルである。
(ii)次式CMに適合するカチオン性モノマー:
式中、k=1であり、v、v’、及びv’’はそれぞれ、独立して、1~6の整数であり、wは0、又は1~10の整数であり、X-はアニオンである。
好適なカチオン性セルロースポリマーは、トリメチルアンモニウム置換エポキシドと反応したヒドロキシエチルセルロースの塩であり、これは、当業界(CTFA)ではポリクオタニウム10と称され、Dow/Amerchol Corp.(Edison,N.J.,USA)から、Polymer LR、JR、及びKGシリーズのポリマーで入手可能である。カチオン性セルロースの他の好適な種類としては、当業界(CTFA)ではポリクオタニウム24と呼ばれる、ラウリルジメチルアンモニウム置換エポキシドと反応させたヒドロキシエチルセルロースのポリマー性第四級アンモニウム塩が挙げられる。これらの材料は、Dow/Amerchol Corp.より、Polymer LM-200の商品名で入手可能である。カチオン性セルロースの他の好適な種類としては、当業界(CTFA)ではポリクオタニウム67と呼ばれる、ラウリルジメチルアンモニウム置換エポキシド及びトリメチルアンモニウム置換エポキシドと反応させたヒドロキシエチルセルロースのポリマー性第四級アンモニウム塩が挙げられる。これらの材料は、Dow/Amerchol Corp.から、SoftCAT Polymer SL-5、SoftCAT Polymer SL-30、Polymer SL-60、Polymer SL-100、Polymer SK-L、Polymer SK-M、Polymer SK-MH、及びPolymer SK-Hという商品名で入手可能である。
繊維要素は、伸長助剤を含むことができる。伸長助剤の非限定的な例としては、ポリマー、他の伸長助剤、及びこれらの組み合わせを挙げることができる。
物品は、任意に、約1重量%~約25重量%の可塑剤、一実施形態では約3重量%~約20重量%の可塑剤、一実施形態では約5重量%~約15重量%の可塑剤を含むことができる。
本明細書に記載される組成物は、毛髪、毛包、及び/又は頭皮を含む皮膚を洗浄、コンディショニング及び/又は処理するために使用され得る。これらの消費者基材を処理するための方法は、a)有効量の物品を手に適用する工程と、b)物品を水で濡らして固体を溶解する工程と、c)溶解した材料を標的消費者基材に適用して泡立ちを形成し、洗浄かつ任意にコンディショニングする工程と、d)希釈した処理組成物を消費者基材からすすぐ工程と、を含んでもよい。これらの工程は、所望のクレンジング及び又は処理効果を達成するために必要に応じて何度でも繰り返すことができる。
繊維性物品を利用する製品の非限定例としては、ハンドクレンジング基材、ヘアシャンプー、ヘアコンディショナー又は他のヘアトリートメント基材、ボディクレンジング基材、シェービング準備用基材、薬剤又は他のスキンケア活性物質を含むパーソナルケア基材、保湿基材、日焼け止め基材、長期皮膚有益剤基材(例えば、ビタミン含有基材、α-ヒドロキシ酸含有基材など)、脱臭基材、香料含有基材などが挙げられる。
界面活性剤及び任意にカチオン性ポリマーを含むシャンプー成分は、繊維要素及び/又は繊維性物品が誘発条件に曝されると、繊維要素及び/又は繊維性物品から放出されてもよい。一実施例では、繊維要素及び/又は繊維性物品、あるいはこれらの一部が、そのアイデンティティを失ったとき、言い換えれば、その物理的構造を失ったときに、繊維要素及び/又は繊維性物品、あるいはこれらの一部から1つ以上の活性剤が放出されてもよい。例えば、ポリマー構造化剤が溶解したとき、融解したとき、又はその構造が失われるような何らかの他の変形工程を経たときに、繊維要素及び/又は繊維性物品は、その物理的構造を失う。一実施例では、繊維要素及び/又は繊維性物品の形態が変化したとき、繊維要素及び/又は繊維性物品から1つ以上の活性剤が放出される。
本発明の繊維要素は、任意の好適なプロセスによって作製することができる。繊維要素を作製するための好適なプロセスの非限定的な例は以下に記載される。
a.1つ又は複数のポリマー構造化剤と、任意に、高融点油脂材料及び/又は1つ以上の界面活性剤を含む1つ以上の他の成分と、を含むフィラメント形成組成物48を提供する工程であって、フィラメント形成組成物は、約5.5を超える、あるいは約5.8を超える、あるいは6.0を超えるpHを含み得る、工程と、
b.紡糸用ダイ50などを介して、フィラメント形成組成物48を、1つ以上のポリマー構造化剤及び任意に1つ以上の他の成分を含む、フィラメントなどの1つ以上の繊維要素32に紡糸する工程と、を含む。1つ以上の他の成分は、意図される使用条件に曝されたときに、繊維要素から放出可能であり得る。繊維要素32中に存在する1つ以上のポリマー構造化剤の総濃度は、乾燥繊維要素換算及び/又は乾燥繊維性物品換算で、80重量%未満、及び/又は70重量%未満、及び/又は65重量%未満、及び/又は50重量%以下であってもよく、1つ以上の活性剤の総濃度は、繊維要素中に存在する場合、乾燥繊維要素換算及び/又は乾燥繊維性物品換算で、20重量%超、及び/又は35重量%超、及び/又は50重量%以上、65重量%以上、及び/又は80重量%以上であってもよい。
1.Kuraray(登録商標)製Poval32-80、Poval 3-80(50:50ブレンド)
2.Sino-Lion製Eversoft(商標)UCS-50SG
3.Clariant(商標)製Hostapon(登録商標)CGN
4.Solvay(登録商標)製Mackam(登録商標)DAB ULS
5.BASF(登録商標)製Jordapon(登録商標)CI Prill
6.BASF(登録商標)製デシルグルコシド
7.SLE1S(70%):Tianjin Tianzhi Fine Chemical
8.SLE3S(28%):P&G Chemicals
9.ウンデシル硫酸ナトリウム(70%):P&G Chemicals
10.Solvay(登録商標)製Mackam(登録商標)LHS
11.Dow(登録商標)製Versene(商標)220
12.ADM(商標)製クエン酸
13.Solvay(登録商標)製ポリクオタニウム-6、PolyDADMAC、MW:150,000、CD:6.2、商品名:Mirapol(登録商標)100s、31.5%活性、40%固形物
14.Amerchol(登録商標)製ポリクオタニウム-10、UCARE(商標)Polymer JR-30M、MW:2,000,000、CD:1.25
15.Amerchol(登録商標)製ポリクオタニウム-10、Poly.LR400、MW:400,000、CD:0.7
16.Rhodia(登録商標)製ポリクアット-76:Mirapol(登録商標)AT 1、MW:1,100,000、CD:1.6
17.Solvay(登録商標)製Jaguar(登録商標)C500、MW:500,000、CD:0.7
18.Croda製Crodasinic(商標)LS35-LQ-(RB)
19.ADM(商標)製ソルビトール
20.Dow(登録商標)製Polyox(商標)N60K、ポリエチレンオキシド
21.Momentive(登録商標)製Y-14945、アモジメチコン
22.Kalama(登録商標)Chemical製安息香酸ナトリウム
23.IsalChem123 AS:P&G Chemicals製アルキル硫酸
特に指定がない限り、定義の節で記載されたものを含む本明細書に記載の全ての試験及び以下の試験方法は、試験前最低2時間、約22℃±2℃の温度及び42%±4%の相対湿度に調整した部屋で調整された試料に対して行われる。試験した試料は、「使用可能ユニット」である。本明細書で使用するとき、「使用可能ユニット」は、シート、ロール材から得た平らな部分、予め変換された平らな部分、及び/又は単プライ製品若しくは多プライ製品を意味する。全ての試験は、同一環境条件下及びこのように調整した室内で実施する。しわ、破れ、穴などの欠陥を有する試料は試験しない。本明細書に記載のとおりに調整された試料は、試験目的に関し、乾燥試料(例えば「乾燥フィラメント」)であると見なされる。全ての計器は、製造業者の仕様書に従って較正する。
±0.001gの感度限界の上皿化学天秤を使用して、12個の使用可能ユニットを積み重ねて繊維性物品の坪量を測定する。風防を使用して、天秤を気流及び他の外乱から保護する。3.500インチ±0.0035インチ×3.500インチ±0.0035インチと測定された精密切断ダイを使用して、全ての試料を調製する。
坪量=(積み重ねた試料の質量)/[(積み重ねた試料内の正方形1個の面積)×(積み重ねた試料内の正方形の数)]
例えば、
坪量(lbs/3000ft2)=[[積み重ねた試料の質量(g)/453.6(g/lbs)]/[12.25(in2)/144(in2/ft2)×12]]×3000
又は、
坪量(g/m2)=積み重ねた試料の質量(g)/[79.032(cm2)/10,000(cm2/m2)×12]
結果を0.1lbs/3000ft2又は0.1g/m2単位で報告する。積み重ねた試料の面積が少なくとも100平方インチになるように、上述のものと同様の精密カッターを使用して試料寸法を変更又は様々に変えてもよい。
汚れ吸着剤を製造物品内及び/又は製造物品上で特定した又は承知している場合、汚れ吸着剤の電荷密度は、BTGから入手可能なMutek PCD-04粒子電荷検出器、又は同等の機器を使用することによって決定することができる。BTGによって提供される以下のガイドラインを使用する。明らかに、汚れ吸着剤を含む製造物品の製造業者は、どのような汚れ吸着剤(複数可)が彼らの製造物品に含まれているのかについて承知している。したがって、製造物品において使用される汚れ吸着剤のそのような製造業者及び/又は供給元は、汚れ吸着剤の電荷密度を決定することができる。
走査型電子顕微鏡(Scanning Electron Microscope、SEM)又は光学顕微鏡、及び画像解析ソフトウェアを使用して、離散繊維要素又は繊維性物品内の繊維要素の直径を求める。繊維要素を測定のために適切に拡大するように、200~10,000倍の倍率を選択する。SEMを使用する場合には、電子ビーム中での繊維要素の帯電及び振動を避けるために、試料に金又はパラジウム化合物をスパッタリングする。SEM又は光学顕微鏡を用いて得られた画像(モニタースクリーン上)から繊維要素の直径を測定するにはマニュアルの手順を用いる。マウス及びカーソルツールを使用して、ランダムに選択された繊維要素の縁部を探し、その後、その幅(すなわち、その点における繊維要素の方向に対して垂直な)にわたって繊維要素の他方の縁部まで測定する。目盛り付きの較正された画像解析ツールにより、μm単位で実際の読取値を取得するための目盛りが提供される。繊維性物品内の繊維要素については、SEM又は光学顕微鏡を使用して、繊維性物品の試料全体からいくつかの繊維要素を無作為に選択する。繊維性物品の少なくとも2つの部分を切り取り、この方法で試験する。統計解析のために、このような測定を全部で少なくとも100回実施し、次いで、全てのデータを記録する。記録したデータを用いて、繊維要素の直径の平均値(平均)、繊維要素の直径の標準偏差、及び繊維要素の直径の中央値を計算する。
分光計:Bruker Avance(商標)700MHz
プローブ:Z軸勾配を備えたBruker Diff30高出力拡散プローブ
増幅器:GREAT 40 A
パルスシーケンス:ledbpgp2s
繊維要素組成物測定用に繊維要素を調製するために、繊維要素の外面上に存在する任意の除去可能であるコーティング組成物及び/又は材料を除去することによって、繊維要素を調整する。それを実行する方法の例としては、繊維要素を変化させずに外部のコーティングを除去する好適な溶媒で、繊維要素を3回洗浄することである。その後、繊維要素の水分が10%未満となるまで、繊維要素を、温度23℃±1.0℃で、空気乾燥させる。調整した繊維要素の化学分析を次いで完了させ、フィラメント形成材料、及び活性剤に関しての繊維要素の組成の構成と、繊維要素内に存在するフィラメント形成材料、及び活性剤の濃度を決定する。
必要材料:
試験対象繊維性物品:3~5個の繊維性物品(最終製品試料)を試験し、個別の繊維性物品試料のそれぞれのストローク数の平均を計算して、繊維性物品の平均ハンド溶解値として記録する。この方法では、消費者用販売可能物品、又は消費者使用繊維性物品の全体を試験する。消費者用販売可能物品又は消費者使用繊維性物品全体が50cm2を超える設置面積を有する場合には、最初に、50cm2の設置面積を有するように繊維性物品を切断する。
10ccシリンジ
プラスチック製秤量ボート(約3インチ×3インチ)
100mLガラスビーカー
水:(以下の特性を有するCincinnati市水道水又は等価物:合計硬度=155mg/L(CaCO2として);カルシウム含量=33.2mg/L;マグネシウム含量=17.5mg/L;リン酸含量=0.0462mg/L)使用される水は、1ガロン当たりの水7グレイン(grains per gallon、gpg)硬度及び40℃±5℃である。
・水80mLをガラスビーカーに加える。
・水が40℃±5℃の温度になるまでビーカー内の水を加熱する。
・ビーカーからシリンジによって15mLの水を秤量ボートに移す。
・水を秤量ボートに移す10秒以内に、手袋をはめた手(繊維性物品試料を保持するための非利き手で、カップのように丸めた形の手)の掌に繊維性物品試料を置く。
・利き手を使用して、秤量ボートから繊維性物品試料に水を素早く添加して、直ちに5~10秒間濡らす。
・反対側の利き手(同様に手袋もはめている)を用いて、2回の急速な円形ストロークで擦る。
・2回のストローク後に、手の中の繊維性物品を目視検査する。繊維性物品試料が完全に溶解している場合、ストローク数=2溶解ストロークを記録する。完全に溶解していない場合、残りの繊維性物品試料を更に2回の円形ストローク(合計4回)で擦り合わせ、溶解度を観察する。2回の更なるストローク後に繊維性物品試料が固体片を含有しない場合、ストローク数=4溶解ストロークを記録する。合計4回のストローク後、繊維性物品試料が依然として、溶解していない繊維性物品試料の固体片を含有する場合、繊維性物品試料が完全に溶解するか、又は合計ストロークが30に達するかのいずれか早い方まで、引き続き更に2回の円形ストロークで残りの繊維性物品試料を擦り合わせ、各更に2回の円形ストローク後に繊維性物品試料の残りの固体片が残っているか否かを確認する。合計ストローク数を記録する。固体繊維性物品試料片が上限の30ストローク後に残った場合であっても、30溶解ストロークを記録する。
・更に4つの繊維性物品試料のそれぞれについて、このプロセスを繰り返す。
・5つの個々の繊維性物品試料の記録された溶解ストロークの値の算術平均を計算し、繊維性物品の平均ハンド溶解値として記録する。平均ハンド溶解値は、最も近い単一の溶解ストローク単位で報告する。
ラメラ構造試験方法は、小角X線散乱(small-angle x-ray scattering、SAXS)及び広角X線散乱(wide-angle x-ray scattering、WAXS)を使用して、ラメラ構造体が、調整された乾燥状態の物品、又は調整された乾燥状態にすでにあった後に湿潤した物品のいずれかに存在するかを判定する。物品を、試験前に最低2時間、温度22℃±2℃及び相対湿度42%±4%で調整する。本明細書に記載のとおり調整された溶解性物品は、本発明の目的上、調整された乾燥状態である。全ての機器は、製造業者の仕様書に従って較正する。
調整された乾燥状態で直接分析される試料を調製するために、直径約1.0cmのディスクの標本を物品の中心から分離し、4~5mmの孔径を有する従来のX線固体試料ホルダに装填する。(複数の標本ディスクは、複数の物品から抽出され、必要に応じて積層されて、十分な散乱断面を確保し得る。)装填された試料ホルダを、データ収集のために適切な機器内に直ちに配置する。
3つの試料を、乾燥した調整された状態から湿潤させて分析する。乾燥し、調整された溶解性物品から標本を抽出し、3種の個別の調製(それぞれは、異なる材料対水の質量比で処理する)を行うため、水に濡らす。調製される3つの異なる材料対水の質量比は、1:5;1:9;及び1:20である。各質量比に関して、直径1cmの1つ以上の標本(必要に応じて)を、乾燥した調整された状態の1つ以上の物品の幾何学的中心から抽出し、意図される材料対水質量比を達成するために、23℃±2.0℃の濾過脱イオン(DI)水で水和する。3つの材料/水混合物の各々(各々は、異なる質量比に対応する)を、目視で均質になるまで、スパチュラを使用して、室温で手作業により、低せん断下で穏やかに撹拌する。次に、各材料/水混合物を、直径が2.0mmの外径及び0.01mmの壁の厚さを有する、個別の石英キャピラリー管に直ちに装填する。毛細管を、調製物からの水の蒸発を防止するために、エポキシ樹脂などのシーラントで直ちに密封する。シーラントを、試料分析の前に、少なくとも2時間及び23℃±2.0℃の温度で乾燥するまで乾燥させる。各調製された湿潤試料を適切なX線機器に導入し、データを収集する。
試料を、0.3°~3.0°2θの角度範囲にわたり、2次元(2D)透過モードで、SAXSを使用して試験し、x線散乱パターンにおける任意の強度バンドの存在及び間隔を観察する。試験を、SAXS機器(NanoSTAR,Bruker AXS Inc.(Madison,Wisconsin,U.S.A.)又は同等物など)を使用して実施する。マイクロフォーカスCu x線管を、550umのScanTex Pinholeで50kV、0.60mAで操作した。試料から検出器までの距離は107.39cmであり、検出器はVantec2K 2次元領域検出器だった。試料を固体試料ホルダに入れ、大気条件下で分析時間600sで分析した。密封された液体試料を、真空下で機器において分析する。
専門官能試験員は、0(少量)~8(大量)の定性的尺度の泡立ちの量を判定した。
・水温を100F±2度に設定する
・水圧1.5GPM±0.1GPM
・水硬度:実験室水、典型的には8~11グレイン/ガロン硬度
各切断された試料がVIR Electronic Thickness Tester Model II(Thwing-Albert Instrument Company(Philadelphia,PA)から入手可能)のロードフット搭載面よりも大きなサイズになるように、繊維性物品試料から5つの試料を切り取ることによって、繊維性物品の厚さを測定する。典型的に、ロードフット搭載面は、約3.14平方インチの円形表面積を有する。試料を水平な平面とロードフット搭載面との間に固定する。ロードフット搭載面は、15.5g/cm2の拘束圧を試料に印加する。各試料の厚みは、平面とロードフット搭載面との間に生じるギャップである。厚みは、5つの試料の平均の厚みとして計算される。結果をミリメートル(mm)で報告する。
繊維要素、及び/又は粒子、及び/又は繊維性物品中に存在する含水(水分)率を、以下の含水率試験方法を使用して測定する。事前に切断されたシートの形態である繊維要素、及び/又は粒子、及び/又は繊維性物品、あるいはそれらの一部(「試料」)を、試験の前に少なくとも24時間、22℃±2℃の温度及び42%±4%の相対湿度に調整した部屋に置く。各繊維性物品試料は、少なくとも4平方インチの面積を有するが、天秤の計量皿上に適切に大きさを合わせるのに十分小さい寸法である。上述の温度及び湿度条件下で、少なくとも小数点第4位まで測定できる天秤を用いて、10分間に検出される、前の重量からの変化が0.5%未満になるまで、5分間ごとに試料の重量を記録する。最終重量を、「平衡重量」として記録する。10分以内に、試料を、乾燥させるために、強制空気乾燥器中のホイル上に、22℃±2℃、相対湿度42%±4%で、24時間置く。24時間の乾燥後、試料を取り除き、15秒以内にその重量を測定する。この重量は、試料の「乾燥重量」と呼ばれる。
A.繊維要素を含む溶解性固体繊維性シャンプー物品であって、
a.乾燥物品換算で約1重量%~約90重量%のポリマー構造化剤と、
b.乾燥物品換算で約10重量%~約90重量%、好ましくは約20重量%~約80重量%、好ましくは約30重量%~約70重量%、より好ましくは約40重量%~約65重量%の界面活性剤系と、を含み、
繊維性物品は、ラメラ構造試験方法によって判定されるとき、ラメラ構造を実質的に含まない、物品。
a.乾燥物品換算で界面活性剤系の約35重量%~約90重量%、好ましくは約40重量%~約85重量%、より好ましくは約45重量%~約80重量%、更により好ましくは約48重量%~約76重量%の一次アニオン性界面活性剤と、
b.乾燥物品換算で界面活性剤系の約から約10重量%~約65重量%、好ましくは約15重量%~約55重量%、より好ましくは約23重量%~約50重量%の補助界面活性剤と、を含む、段落A~Iに記載の物品。
a.ポリマー構造化剤及び界面活性剤系を含むフィラメント形成組成物を提供する工程であって、フィラメント形成組成物は、約5.5を超えるpHを含む、工程と、
b.フィラメント形成組成物を1つ以上のフィラメントに紡糸する工程であって、フィラメント形成組成物が紡糸可能である、工程と、
c.約340°F(171.1℃)~約350°F(176.7℃)の温度で約50~約60秒間、又は約390°F(198.9℃)~約400°F(204℃)の温度で約30~約40秒間又は415°F(212.8℃)~470°F(243.3℃)の温度で約5~約20秒間、フィラメントを乾燥させる工程と、
d.物品を形成する工程と、を含む、方法。
Claims (8)
- 繊維要素を含む溶解性固体繊維性シャンプー物品であって、
a.乾燥物品換算で10重量%~80重量%のポリビニルアルコールと、
b.乾燥物品換算で20重量%~90重量%の界面活性剤系であって、
i.乾燥物品換算で前記界面活性剤系の35重量%~90重量%のグルタメート界面活性剤、スルホコハク酸塩界面活性剤及び、これらの混合物から選択される一次アニオン性界面活性剤と、
ii.乾燥物品換算で前記界面活性剤系の10重量%~65重量%のイセチオン酸塩界面活性剤、非イオン性界面活性剤、両性界面活性剤、双性イオン性界面活性剤、及びこれらの混合物からなる群から選択される補助界面活性剤と、を含む、界面活性剤系と、を含み、
前記繊維性物品は、乾燥物品換算で0.1%未満の硫酸塩系界面活性剤を含み、
前記繊維性物品は、ラメラ構造試験方法によって判定されるとき、ラメラ構造を実質的に含まず、
前記繊維性物品は、本明細書に開示のハンド溶解試験方法によって判定されるとき、15ストローク未満のハンド溶解を含む、物品。 - a.乾燥物品換算で20重量%~70重量%のポリビニルアルコールを含む、請求項1に記載の物品。
- 前記繊維性物品は、硫酸塩系界面活性を含まない、請求項1に記載の物品。
- 前記一次アニオン性界面活性剤は、ココイルグルタミン酸ナトリウム、ココイルグルタミン酸二ナトリウム、ココイルグルタミン酸カリウム、ココイルグルタミン酸二カリウム、ココイルグルタミン酸アンモニウム、ココイルグルタミン酸二アンモニウム、ココイルグルタミン酸TEA、及びこれらの混合物からなる群から選択されるグルタメート界面活性剤である、請求項1に記載の物品。
- 前記一次アニオン性界面活性剤は、ココイルグルタミン酸二ナトリウム、ラウレススルホコハク酸二ナトリウム、及びこれらの組み合わせからなる群から選択される、請求項1に記載の物品。
- 前記補助界面活性剤がイセチオン酸塩界面活性剤である、請求項1に記載の物品。
- 乾燥物品換算で0.1%~2%のカチオン性ポリマーを更に含み、前記カチオン性ポリマーは、ゲル浸透クロマトグラフィで測定されるとき、100,000g/mol~250万g/molの重量平均分子量と、本明細書に開示の電荷密度試験方法に従って測定されるとき、0.4meg/gより大きい電荷密度と、を含む、請求項1に記載の物品。
- 前記カチオン性ポリマーは、ポリクオタニウム-6、ポリクオタニウム-10、カチオン性グアー、及びこれらの組み合わせからなる群から選択される、請求項7に記載の物品。
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US20200405587A1 (en) | 2020-12-31 |
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CN114206307A (zh) | 2022-03-18 |
JP2022536334A (ja) | 2022-08-15 |
EP3989913A1 (en) | 2022-05-04 |
CA3134222A1 (en) | 2020-12-30 |
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US11679066B2 (en) | 2023-06-20 |
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