JP5008256B2 - ポリオキシメチレン樹脂組成物の製造方法 - Google Patents
ポリオキシメチレン樹脂組成物の製造方法 Download PDFInfo
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- JP5008256B2 JP5008256B2 JP2004376257A JP2004376257A JP5008256B2 JP 5008256 B2 JP5008256 B2 JP 5008256B2 JP 2004376257 A JP2004376257 A JP 2004376257A JP 2004376257 A JP2004376257 A JP 2004376257A JP 5008256 B2 JP5008256 B2 JP 5008256B2
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- polyoxymethylene resin
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- -1 polyoxymethylene Polymers 0.000 title claims description 217
- 229920006324 polyoxymethylene Polymers 0.000 title claims description 121
- 229930040373 Paraformaldehyde Natural products 0.000 title claims description 118
- 239000011342 resin composition Substances 0.000 title claims description 79
- 238000004519 manufacturing process Methods 0.000 title claims description 56
- 229920005989 resin Polymers 0.000 claims description 71
- 239000011347 resin Substances 0.000 claims description 71
- 229920000642 polymer Polymers 0.000 claims description 70
- 229920001577 copolymer Polymers 0.000 claims description 35
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 35
- 125000005704 oxymethylene group Chemical group [H]C([H])([*:2])O[*:1] 0.000 claims description 28
- 229920000049 Carbon (fiber) Polymers 0.000 claims description 26
- 125000004432 carbon atom Chemical group C* 0.000 claims description 26
- 239000004917 carbon fiber Substances 0.000 claims description 26
- 239000001508 potassium citrate Substances 0.000 claims description 26
- QEEAPRPFLLJWCF-UHFFFAOYSA-K potassium citrate (anhydrous) Chemical compound [K+].[K+].[K+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O QEEAPRPFLLJWCF-UHFFFAOYSA-K 0.000 claims description 26
- 235000015870 tripotassium citrate Nutrition 0.000 claims description 26
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 22
- 238000000034 method Methods 0.000 claims description 20
- WTEOIRVLGSZEPR-UHFFFAOYSA-N boron trifluoride Chemical group FB(F)F WTEOIRVLGSZEPR-UHFFFAOYSA-N 0.000 claims description 18
- 239000000203 mixture Substances 0.000 claims description 18
- 239000000178 monomer Substances 0.000 claims description 16
- 229920000570 polyether Polymers 0.000 claims description 16
- 239000004952 Polyamide Substances 0.000 claims description 15
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 15
- 229920002647 polyamide Polymers 0.000 claims description 15
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
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- 150000001336 alkenes Chemical class 0.000 claims description 8
- 125000000217 alkyl group Chemical group 0.000 claims description 8
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- 229910003475 inorganic filler Inorganic materials 0.000 claims description 8
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims description 8
- 125000005702 oxyalkylene group Chemical group 0.000 claims description 8
- BGJSXRVXTHVRSN-UHFFFAOYSA-N 1,3,5-trioxane Chemical compound C1OCOCO1 BGJSXRVXTHVRSN-UHFFFAOYSA-N 0.000 claims description 7
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- 238000002156 mixing Methods 0.000 claims description 7
- 229920002554 vinyl polymer Polymers 0.000 claims description 7
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 6
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- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 claims description 6
- 229920000089 Cyclic olefin copolymer Polymers 0.000 claims description 5
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 5
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- 229920000877 Melamine resin Polymers 0.000 claims description 4
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims description 3
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- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 3
- 150000002894 organic compounds Chemical class 0.000 claims description 3
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- 229910052717 sulfur Inorganic materials 0.000 claims description 3
- 125000004434 sulfur atom Chemical group 0.000 claims description 3
- MVJKXJPDBTXECY-UHFFFAOYSA-N trifluoroborane;hydrate Chemical compound O.FB(F)F MVJKXJPDBTXECY-UHFFFAOYSA-N 0.000 claims description 3
- 125000000325 methylidene group Chemical group [H]C([H])=* 0.000 claims 2
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 93
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- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 11
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- 239000000126 substance Substances 0.000 description 10
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
- 125000001931 aliphatic group Chemical group 0.000 description 9
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 9
- 150000003839 salts Chemical class 0.000 description 9
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 8
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 7
- 239000002253 acid Substances 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- 235000019253 formic acid Nutrition 0.000 description 7
- WQEPLUUGTLDZJY-UHFFFAOYSA-N pentadecanoic acid Chemical compound CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 7
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 6
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 6
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- UKMSUNONTOPOIO-UHFFFAOYSA-N docosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCC(O)=O UKMSUNONTOPOIO-UHFFFAOYSA-N 0.000 description 6
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- VKOBVWXKNCXXDE-UHFFFAOYSA-N icosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCC(O)=O VKOBVWXKNCXXDE-UHFFFAOYSA-N 0.000 description 6
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- UTOPWMOLSKOLTQ-UHFFFAOYSA-N octacosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCC(O)=O UTOPWMOLSKOLTQ-UHFFFAOYSA-N 0.000 description 6
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 6
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 6
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- 238000012360 testing method Methods 0.000 description 6
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- 229910052784 alkaline earth metal Inorganic materials 0.000 description 5
- 125000003342 alkenyl group Chemical group 0.000 description 5
- RSOILICUEWXSLA-UHFFFAOYSA-N bis(1,2,2,6,6-pentamethylpiperidin-4-yl) decanedioate Chemical compound C1C(C)(C)N(C)C(C)(C)CC1OC(=O)CCCCCCCCC(=O)OC1CC(C)(C)N(C)C(C)(C)C1 RSOILICUEWXSLA-UHFFFAOYSA-N 0.000 description 5
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- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 5
- VZSRBBMJRBPUNF-UHFFFAOYSA-N 2-(2,3-dihydro-1H-inden-2-ylamino)-N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]pyrimidine-5-carboxamide Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C(=O)NCCC(N1CC2=C(CC1)NN=N2)=O VZSRBBMJRBPUNF-UHFFFAOYSA-N 0.000 description 4
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- UFFRSDWQMJYQNE-UHFFFAOYSA-N 6-azaniumylhexylazanium;hexanedioate Chemical compound [NH3+]CCCCCC[NH3+].[O-]C(=O)CCCCC([O-])=O UFFRSDWQMJYQNE-UHFFFAOYSA-N 0.000 description 2
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- FYNROBRQIVCIQF-UHFFFAOYSA-N pyrrolo[3,2-b]pyrrole-5,6-dione Chemical compound C1=CN=C2C(=O)C(=O)N=C21 FYNROBRQIVCIQF-UHFFFAOYSA-N 0.000 description 1
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- 125000006850 spacer group Chemical group 0.000 description 1
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- 229920001897 terpolymer Polymers 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 229920002803 thermoplastic polyurethane Polymers 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
- 150000003606 tin compounds Chemical class 0.000 description 1
- 150000003918 triazines Chemical class 0.000 description 1
- HRXKRNGNAMMEHJ-UHFFFAOYSA-K trisodium citrate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O HRXKRNGNAMMEHJ-UHFFFAOYSA-K 0.000 description 1
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- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 description 1
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- DRDVZXDWVBGGMH-UHFFFAOYSA-N zinc;sulfide Chemical compound [S-2].[Zn+2] DRDVZXDWVBGGMH-UHFFFAOYSA-N 0.000 description 1
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Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/09—Carboxylic acids; Metal salts thereof; Anhydrides thereof
- C08K5/098—Metal salts of carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/04—Carbon
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/10—Esters; Ether-esters
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/34—Heterocyclic compounds having nitrogen in the ring
- C08K5/3467—Heterocyclic compounds having nitrogen in the ring having more than two nitrogen atoms in the ring
- C08K5/3477—Six-membered rings
- C08K5/3492—Triazines
- C08K5/34922—Melamine; Derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K7/00—Use of ingredients characterised by shape
- C08K7/02—Fibres or whiskers
- C08K7/04—Fibres or whiskers inorganic
- C08K7/06—Elements
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L59/00—Compositions of polyacetals; Compositions of derivatives of polyacetals
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Polyoxymethylene Polymers And Polymers With Carbon-To-Carbon Bonds (AREA)
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2004376257A JP5008256B2 (ja) | 2004-04-23 | 2004-12-27 | ポリオキシメチレン樹脂組成物の製造方法 |
| KR1020050032445A KR100606175B1 (ko) | 2004-04-23 | 2005-04-19 | 폴리옥시메틸렌 수지 조성물 및 그의 제조방법 |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2004128932 | 2004-04-23 | ||
| JP2004128932 | 2004-04-23 | ||
| JP2004376257A JP5008256B2 (ja) | 2004-04-23 | 2004-12-27 | ポリオキシメチレン樹脂組成物の製造方法 |
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| EP3091051A4 (fr) * | 2013-12-31 | 2017-11-29 | Kolon Plastics, Inc. | Composition de résine polyacétal et article moulé la contenant |
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| JP5028758B2 (ja) * | 2004-07-27 | 2012-09-19 | 東レ株式会社 | ポリアセタール樹脂組成物、およびその製造方法 |
| JP5217101B2 (ja) * | 2006-03-23 | 2013-06-19 | 東レ株式会社 | 樹脂組成物およびそれからなる成形品 |
| JP5116022B2 (ja) * | 2007-12-27 | 2013-01-09 | 旭化成ケミカルズ株式会社 | 導電性ポリアセタール樹脂組成物、その製造方法および成形体 |
| JP2009191113A (ja) * | 2008-02-12 | 2009-08-27 | Mitsubishi Gas Chem Co Inc | ポリアセタール樹脂組成物及び該樹脂組成物を成形してなる摺動部材 |
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| US8163812B2 (en) * | 2008-12-04 | 2012-04-24 | E.I. Du Pont De Nemours And Company | Process for making thermally resistant mineral-filled polyacetal |
| KR101529706B1 (ko) * | 2008-12-31 | 2015-06-29 | 코오롱플라스틱 주식회사 | 내후성 폴리에스테르 탄성체 수지 조성물 |
| JP5601792B2 (ja) * | 2009-05-20 | 2014-10-08 | オイレス工業株式会社 | ポリアセタール樹脂組成物及び摺動部材 |
| CN101805515B (zh) * | 2010-03-17 | 2012-02-15 | 浙江俊尔新材料有限公司 | 耐磨增强聚酰胺/聚甲醛合金材料及其制备方法 |
| US20110237727A1 (en) * | 2010-03-29 | 2011-09-29 | Jung-Pao Chang | Durable polyoxymethylene composition |
| US8759431B2 (en) | 2010-03-29 | 2014-06-24 | Min Aik Technology Co., Ltd. | Durable polyoxymethylene composition |
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| JP2013224376A (ja) * | 2012-04-23 | 2013-10-31 | Asahi Kasei Chemicals Corp | 着色された樹脂組成物及び成形体 |
| EP2931804B1 (fr) * | 2012-12-13 | 2018-08-08 | Ticona LLC | Polyoxyméthylène soudable par laser et possédant des propriétés antistatiques à base de charges métalliques conductrices |
| WO2015102405A1 (fr) * | 2013-12-31 | 2015-07-09 | 코오롱플라스틱 주식회사 | Composition de résine polyacétal et article moulé la contenant |
| JP5788064B2 (ja) * | 2014-06-30 | 2015-09-30 | オイレス工業株式会社 | ポリアセタール樹脂組成物 |
| JP5781201B1 (ja) | 2014-06-30 | 2015-09-16 | ポリプラスチックス株式会社 | ポリアセタール樹脂組成物、及びこのポリアセタール樹脂組成物の成形品を備える燃料接触体 |
| JP6913443B2 (ja) * | 2016-06-24 | 2021-08-04 | 旭化成株式会社 | ポリアセタール共重合体の製造方法 |
| US10053557B2 (en) * | 2016-09-22 | 2018-08-21 | Min Aik Technology Co., Ltd. | Low wear debris polyoxymethylene composition and a ramp made of such polyoxymethylene composition suitable for various HDD designs |
| CN109735111A (zh) * | 2018-12-20 | 2019-05-10 | 上海衣页信息科技有限公司 | 一种高导电粘性加成型导电硅橡胶及制备方法 |
| JP6915764B1 (ja) * | 2019-11-29 | 2021-08-04 | 三菱瓦斯化学株式会社 | ポリアセタール繊維及びその製造方法、並びに、延伸用材料 |
| US11898033B2 (en) * | 2020-06-10 | 2024-02-13 | Mitsubishi Gas Chemical Company, Inc. | Oxymethylene copolymer resin composition and method for producing same |
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| DE4236465A1 (de) | 1992-10-24 | 1994-04-28 | Degussa | Polyoxymethylen mit verbesserter Stabilität gegen Säuren, Verfahren zu seiner Herstellung sowie Verwendung |
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| JP3821698B2 (ja) * | 2000-12-26 | 2006-09-13 | 旭化成ケミカルズ株式会社 | ポリオキシメチレン樹脂組成物及びその成形体 |
| JP4516301B2 (ja) * | 2003-11-10 | 2010-08-04 | ポリプラスチックス株式会社 | ポリアセタール樹脂組成物 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| EP3091051A4 (fr) * | 2013-12-31 | 2017-11-29 | Kolon Plastics, Inc. | Composition de résine polyacétal et article moulé la contenant |
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| JP2005330463A (ja) | 2005-12-02 |
| KR20060047234A (ko) | 2006-05-18 |
| KR100606175B1 (ko) | 2006-08-01 |
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