JP2003507300A5 - - Google Patents
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- JP2003507300A5 JP2003507300A5 JP2001516860A JP2001516860A JP2003507300A5 JP 2003507300 A5 JP2003507300 A5 JP 2003507300A5 JP 2001516860 A JP2001516860 A JP 2001516860A JP 2001516860 A JP2001516860 A JP 2001516860A JP 2003507300 A5 JP2003507300 A5 JP 2003507300A5
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- hydrolysis
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- 238000000034 method Methods 0.000 description 18
- 239000000243 solution Substances 0.000 description 8
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 6
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- 230000007062 hydrolysis Effects 0.000 description 6
- 238000006460 hydrolysis reaction Methods 0.000 description 6
- 239000003795 chemical substances by application Substances 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- 238000001354 calcination Methods 0.000 description 4
- 150000007524 organic acids Chemical class 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000011591 potassium Substances 0.000 description 3
- 229910052700 potassium Inorganic materials 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 3
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 235000021355 Stearic acid Nutrition 0.000 description 2
- 150000003863 ammonium salts Chemical class 0.000 description 2
- 235000015165 citric acid Nutrition 0.000 description 2
- 150000004673 fluoride salts Chemical class 0.000 description 2
- 150000002334 glycols Chemical class 0.000 description 2
- 229910052744 lithium Inorganic materials 0.000 description 2
- 239000002105 nanoparticle Substances 0.000 description 2
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 2
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 2
- 235000005985 organic acids Nutrition 0.000 description 2
- 235000006408 oxalic acid Nutrition 0.000 description 2
- 235000021317 phosphate Nutrition 0.000 description 2
- 229920000058 polyacrylate Polymers 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- -1 siloxanes Chemical class 0.000 description 2
- 239000008117 stearic acid Substances 0.000 description 2
- 239000010409 thin film Substances 0.000 description 2
- 239000004408 titanium dioxide Substances 0.000 description 2
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 229910010413 TiO 2 Inorganic materials 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 150000005323 carbonate salts Chemical class 0.000 description 1
- 150000003841 chloride salts Chemical class 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 229910001510 metal chloride Inorganic materials 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 238000007738 vacuum evaporation Methods 0.000 description 1
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical class [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 description 1
Applications Claiming Priority (9)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US14105799P | 1999-06-24 | 1999-06-24 | |
| US14111499P | 1999-06-24 | 1999-06-24 | |
| US60/141,114 | 1999-06-24 | ||
| US60/141,057 | 1999-06-24 | ||
| US09/500,207 | 2000-02-07 | ||
| US09/500,207 US6375923B1 (en) | 1999-06-24 | 2000-02-07 | Processing titaniferous ore to titanium dioxide pigment |
| US09/503,365 | 2000-02-14 | ||
| US09/503,365 US6440383B1 (en) | 1999-06-24 | 2000-02-14 | Processing aqueous titanium chloride solutions to ultrafine titanium dioxide |
| PCT/US2000/016355 WO2001012555A2 (en) | 1999-06-24 | 2000-06-14 | Processing aqueous titanium chloride solutions to ultrafine titanium dioxide |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2003507300A JP2003507300A (ja) | 2003-02-25 |
| JP2003507300A5 true JP2003507300A5 (enExample) | 2007-08-02 |
| JP4653916B2 JP4653916B2 (ja) | 2011-03-16 |
Family
ID=27495454
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2001516860A Expired - Lifetime JP4653916B2 (ja) | 1999-06-24 | 2000-06-14 | 塩化チタン水溶液から超微細二酸化チタンを製造する方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US6440383B1 (enExample) |
| EP (1) | EP1194380B9 (enExample) |
| JP (1) | JP4653916B2 (enExample) |
| AU (1) | AU769225B2 (enExample) |
| CA (1) | CA2375623C (enExample) |
| DE (1) | DE60015763T2 (enExample) |
| WO (1) | WO2001012555A2 (enExample) |
Families Citing this family (72)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3611303B2 (ja) * | 1997-09-02 | 2005-01-19 | 石原産業株式会社 | 中空状微粉末、該中空状微粉末を粉砕してなる薄片状酸化チタン微粉末およびそれらの製造方法 |
| NZ505774A (en) * | 2000-07-17 | 2002-12-20 | Ind Res Ltd | Oxalate stabilised titania solutions and coating compositions and catalysts formed therefrom |
| AU2001290650A1 (en) | 2000-09-05 | 2002-03-22 | Altair Nanomaterials Inc | Method for producing mixed metal oxides and metal oxide compounds |
| AU2002224394A1 (en) | 2000-10-17 | 2002-04-29 | Altair Nanomaterials Inc. | Method for producing catalyst structures |
| KR100420275B1 (ko) * | 2001-04-06 | 2004-03-02 | (주)아해 | 무기산을 이용한 사염화티타늄 수용액으로부터 TiO2 초미립 분말의 제조방법 |
| DE60202373T2 (de) * | 2001-07-20 | 2005-12-08 | Altair Nanomaterials Inc., Reno | Verfahren zur herstellung von lithiumtitanat |
| EP1282180A1 (en) * | 2001-07-31 | 2003-02-05 | Xoliox SA | Process for producing Li4Ti5O12 and electrode materials |
| US6982073B2 (en) | 2001-11-02 | 2006-01-03 | Altair Nanomaterials Inc. | Process for making nano-sized stabilized zirconia |
| EP1483206B1 (en) * | 2002-03-08 | 2010-10-20 | Altair Nanomaterials Inc. | Process for making nano-sized and sub-micron-sized lithium-transition metal oxides |
| CN1298790C (zh) * | 2002-08-07 | 2007-02-07 | 石原产业株式会社 | 二氧化钛颜料、其生产方法及包含该颜料的树脂组合物 |
| KR100475551B1 (ko) * | 2002-10-08 | 2005-03-10 | (주)아해 | 사염화티타늄과 염산수용액을 이용한 나노크기의 브루카이트상 이산화티타늄 분말의 제조방법 |
| US7140567B1 (en) * | 2003-03-11 | 2006-11-28 | Primet Precision Materials, Inc. | Multi-carbide material manufacture and use as grinding media |
| US20050100965A1 (en) | 2003-11-12 | 2005-05-12 | Tariq Ghayur | IL-18 binding proteins |
| US20050232851A1 (en) * | 2003-11-13 | 2005-10-20 | Jan Prochazka | Process to make rutile pigment from aqueous titanium solutions |
| US7482304B2 (en) | 2003-12-10 | 2009-01-27 | Altair Nanomaterials Inc. | Method for producing structures |
| US7407690B2 (en) * | 2004-03-23 | 2008-08-05 | Altair Nanomaterials Inc. | Process for surface modifications of TiO2 particles and other ceramic materials |
| US7368523B2 (en) | 2004-11-12 | 2008-05-06 | Eastman Chemical Company | Polyester polymer and copolymer compositions containing titanium nitride particles |
| CN101005833A (zh) * | 2004-08-20 | 2007-07-25 | 3M创新有限公司 | 具有半透明保护膜的透皮药物递送装置 |
| CN101006016A (zh) * | 2004-08-26 | 2007-07-25 | 三井化学株式会社 | 金红石型氧化钛超微粒子 |
| US20060051542A1 (en) * | 2004-09-03 | 2006-03-09 | Zhiyong Xia | Polyester polymer and copolymer compositions containing metallic molybdenum particles |
| US7662880B2 (en) * | 2004-09-03 | 2010-02-16 | Eastman Chemical Company | Polyester polymer and copolymer compositions containing metallic nickel particles |
| US20060110557A1 (en) * | 2004-09-03 | 2006-05-25 | Zhiyong Xia | Polyester polymer and copolymer compositions containing metallic tungsten particles |
| WO2006049831A1 (en) * | 2004-10-14 | 2006-05-11 | Tokusen U.S.A., Inc. | Method of production of high purity silver particles |
| WO2006044495A1 (en) * | 2004-10-14 | 2006-04-27 | Tokusen U.S.A., Inc. | Method for synthesizing nano-sized titanium dioxide particles |
| JP5241994B2 (ja) * | 2004-11-05 | 2013-07-17 | 戸田工業株式会社 | 酸化チタン粒子粉末及び光触媒 |
| CA2586893A1 (en) * | 2004-11-09 | 2006-05-18 | Monogen, Inc. | Vial assembly, sampling apparatus and method for processing liquid-based specimens |
| EP1807352A1 (en) * | 2004-11-11 | 2007-07-18 | Basell Poliolefine Italia S.r.l. | Preparation of tio2 powders from a waste liquid containing titanium compounds |
| JP2008519750A (ja) * | 2004-11-11 | 2008-06-12 | バーゼル・ポリオレフィン・イタリア・ソチエタ・ア・レスポンサビリタ・リミタータ | チタン化合物を含有する廃液からＴｉＯ２粉末の製造 |
| US7300967B2 (en) * | 2004-11-12 | 2007-11-27 | Eastman Chemical Company | Polyester polymer and copolymer compositions containing metallic titanium particles |
| KR100627621B1 (ko) * | 2004-11-19 | 2006-09-25 | 한국화학연구원 | 루타일형 티타니아 나노 졸의 제조방법 |
| US20060122300A1 (en) * | 2004-12-07 | 2006-06-08 | Zhiyong Xia | Polyester polymer and copolymer compositions containing steel particles |
| US20060177614A1 (en) * | 2005-02-09 | 2006-08-10 | Zhiyong Xia | Polyester polymer and copolymer compositions containing metallic tantalum particles |
| DE102005022076A1 (de) * | 2005-02-25 | 2006-09-07 | Heubach Gmbh | Pastellweißes, feinteiliges, hochdeckendes und dotiertes Rutilpigment mit verminderter Photoaktivität, ein Verfahren zu dessen Herstellung und dessen Verwendung |
| US20060210798A1 (en) * | 2005-03-16 | 2006-09-21 | Clemens Burda | Doped metal oxide nanoparticles and methods for making and using same |
| US7326399B2 (en) * | 2005-04-15 | 2008-02-05 | Headwaters Technology Innovation, Llc | Titanium dioxide nanoparticles and nanoparticle suspensions and methods of making the same |
| KR101304263B1 (ko) * | 2005-06-03 | 2013-09-05 | 후지필름 가부시키가이샤 | 안료함유 열경화성 조성물, 및, 컬러필터, 화상기록재료,및, 컬러필터의 제조방법 |
| US8557950B2 (en) | 2005-06-16 | 2013-10-15 | Grupo Petrotemex, S.A. De C.V. | High intrinsic viscosity melt phase polyester polymers with acceptable acetaldehyde generation rates |
| CN100445209C (zh) * | 2005-07-28 | 2008-12-24 | 同济大学 | 一种纳米二氧化钛粉体制备方法 |
| US7776942B2 (en) * | 2005-09-16 | 2010-08-17 | Eastman Chemical Company | Polyester polymer and copolymer compositions containing particles of titanium nitride and carbon-coated iron |
| US7655746B2 (en) | 2005-09-16 | 2010-02-02 | Eastman Chemical Company | Phosphorus containing compounds for reducing acetaldehyde in polyesters polymers |
| US7745512B2 (en) * | 2005-09-16 | 2010-06-29 | Eastman Chemical Company | Polyester polymer and copolymer compositions containing carbon-coated iron particles |
| MX2008005136A (es) * | 2005-10-21 | 2008-10-31 | Altairnano Inc | Baterias de ion de litio. |
| US7247200B2 (en) * | 2005-11-01 | 2007-07-24 | E. I. Du Pont De Nemours And Company | Titanium dioxide finishing process |
| US20070260002A1 (en) * | 2006-05-04 | 2007-11-08 | Zhiyong Xia | Titanium nitride particles, methods of making them, and their use in polyester compositions |
| US20080058495A1 (en) * | 2006-09-05 | 2008-03-06 | Donna Rice Quillen | Polyester polymer and copolymer compositions containing titanium and yellow colorants |
| EP2074064A4 (en) * | 2006-09-21 | 2013-06-05 | Tokusen U S A Inc | LOW TEMPERATURE PROCESS FOR PRODUCING TITANIUM DIOXIDE PARTICLES OF A NANOMETER SIZE |
| US8114377B2 (en) * | 2006-11-02 | 2012-02-14 | E.I. Du Pont De Nemours And Company | Process for producing titanium dioxide particles having reduced chlorides |
| JP2010514657A (ja) * | 2006-12-28 | 2010-05-06 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー | 二酸化チタンのフラックスか焼製造方法 |
| KR20090129500A (ko) * | 2007-03-30 | 2009-12-16 | 알타이어나노 인코포레이티드 | 리튬 이온 전지의 제조방법 |
| US7704470B2 (en) * | 2007-04-24 | 2010-04-27 | Haydock Consulting Services, Lc | Removal of contaminants from by-product acids |
| US7858066B2 (en) * | 2007-05-08 | 2010-12-28 | E.I. Du Pont De Nemours And Company | Method of making titanium dioxide particles |
| FI124294B (fi) * | 2007-08-16 | 2014-06-13 | Sachtleben Pigments Oy | Menetelmä hyvin dispergoituvan mikrokiteisen titaanidioksidituotteen valmistamiseksi, tuote ja sen käyttö |
| AU2008345554B2 (en) * | 2007-12-27 | 2014-02-20 | E. I. Du Pont De Nemours And Company | Method of making photoluminescent samarium-doped titanium dioxide particles |
| JP5126783B2 (ja) * | 2008-03-24 | 2013-01-23 | 日揮触媒化成株式会社 | ルチル型酸化チタン微粒子の製造方法 |
| KR100987825B1 (ko) * | 2008-05-26 | 2010-10-18 | 한국화학연구원 | 로드형 티타니아 나노입자의 제조방법 |
| CN102105319A (zh) * | 2008-06-27 | 2011-06-22 | 普罗特拉公司 | 汽车电池系统和方法 |
| CN101676215B (zh) * | 2008-09-19 | 2012-11-07 | 范莉 | 一种利用盐酸和高分子化合物协同作用制备二氧化钛纳米球的方法 |
| US20100111818A1 (en) * | 2008-10-29 | 2010-05-06 | Haydock Frederick J | Removal of contaminants from by-product hydrochloric acid |
| CN101922044B (zh) * | 2010-09-11 | 2012-02-15 | 天津大学 | 一种在二氧化钛纳米管中掺杂纳米银颗粒的方法 |
| EP2522373A1 (en) | 2011-05-11 | 2012-11-14 | Dentsply IH AB | Biocompatible component |
| US8932556B2 (en) * | 2013-03-15 | 2015-01-13 | Cristal Usa Inc. | Rutile titanium dioxide nanoparticles and ordered acicular aggregates of same |
| JP2017530084A (ja) | 2014-07-08 | 2017-10-12 | アヴァータナ・リミテッド | チタン含有鉱物からの生成物の抽出 |
| US10988828B2 (en) | 2017-11-21 | 2021-04-27 | Scandium Intrenational Mining Corporation | Extraction of scandium values from copper leach solutions |
| US10480047B1 (en) | 2018-06-28 | 2019-11-19 | Argex Titanium Inc. | Process for recovering titanium dioxide from titanium containing materials |
| CN109354062A (zh) * | 2018-11-26 | 2019-02-19 | 昆明冶金研究院 | 一种锐钛型纳米二氧化钛及其制备方法与应用 |
| CN119372485A (zh) | 2018-12-14 | 2025-01-28 | 阿瓦塔纳有限公司 | 从含钛材料中提取产品的方法 |
| US11673812B2 (en) | 2019-08-15 | 2023-06-13 | Scandium International Mining Corporation | Countercurrent process for recovering high purity copper sulfate values from low grade ores |
| US12338509B2 (en) | 2019-08-20 | 2025-06-24 | Scandium International Mining Corporation | Byproduct scandium recovery from low grade primary metal oxide ores |
| US11821057B2 (en) | 2020-03-06 | 2023-11-21 | Scandium Internatlonal Mlning Corporatlon | Recovery of critical metals from SX-EW copper raffinate and other solutions derived from leaching ores with sulfuric acid |
| KR102411275B1 (ko) * | 2021-09-15 | 2022-06-23 | 주식회사 한내포티 | 타이타늄 함유 염산용액을 이용한 아나타제형 이산화타이타늄 제조 방법 및 타이타늄 함유 염산용액을 이용한 이산화타이타늄 결정 제어 방법 |
| WO2023043095A1 (ko) * | 2021-09-15 | 2023-03-23 | 주식회사 한내포티 | 탈질폐촉매 함유 유가금속의 추출방법 |
| CN113860364B (zh) * | 2021-09-29 | 2023-03-03 | 李礼 | 一种调控纳米二氧化钛转晶过程的方法 |
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-
2000
- 2000-02-14 US US09/503,365 patent/US6440383B1/en not_active Expired - Lifetime
- 2000-06-14 EP EP00982051A patent/EP1194380B9/en not_active Expired - Lifetime
- 2000-06-14 WO PCT/US2000/016355 patent/WO2001012555A2/en not_active Ceased
- 2000-06-14 DE DE60015763T patent/DE60015763T2/de not_active Expired - Lifetime
- 2000-06-14 JP JP2001516860A patent/JP4653916B2/ja not_active Expired - Lifetime
- 2000-06-14 CA CA002375623A patent/CA2375623C/en not_active Expired - Lifetime
- 2000-06-14 AU AU19128/01A patent/AU769225B2/en not_active Expired
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