JP4653916B2 - 塩化チタン水溶液から超微細二酸化チタンを製造する方法 - Google Patents
塩化チタン水溶液から超微細二酸化チタンを製造する方法 Download PDFInfo
- Publication number
- JP4653916B2 JP4653916B2 JP2001516860A JP2001516860A JP4653916B2 JP 4653916 B2 JP4653916 B2 JP 4653916B2 JP 2001516860 A JP2001516860 A JP 2001516860A JP 2001516860 A JP2001516860 A JP 2001516860A JP 4653916 B2 JP4653916 B2 JP 4653916B2
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- Prior art keywords
- solution
- titanium
- salts
- range
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
- C01G23/047—Titanium dioxide
- C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
- C01G23/047—Titanium dioxide
- C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
- C01G23/0536—Producing by wet processes, e.g. hydrolysing titanium salts by hydrolysing chloride-containing salts
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/36—Compounds of titanium
- C09C1/3607—Titanium dioxide
- C09C1/3615—Physical treatment, e.g. grinding, treatment with ultrasonic vibrations
- C09C1/363—Drying, calcination
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/30—Particle morphology extending in three dimensions
- C01P2004/32—Spheres
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/30—Particle morphology extending in three dimensions
- C01P2004/32—Spheres
- C01P2004/34—Spheres hollow
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/80—Particles consisting of a mixture of two or more inorganic phases
- C01P2004/82—Particles consisting of a mixture of two or more inorganic phases two phases having the same anion, e.g. both oxidic phases
- C01P2004/84—Particles consisting of a mixture of two or more inorganic phases two phases having the same anion, e.g. both oxidic phases one phase coated with the other
- C01P2004/86—Thin layer coatings, i.e. the coating thickness being less than 0.1 time the particle radius
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Inorganic Chemistry (AREA)
- Environmental & Geological Engineering (AREA)
- Nanotechnology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Composite Materials (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Materials Engineering (AREA)
- Crystallography & Structural Chemistry (AREA)
- Physics & Mathematics (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Applications Claiming Priority (9)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US14105799P | 1999-06-24 | 1999-06-24 | |
| US14111499P | 1999-06-24 | 1999-06-24 | |
| US60/141,114 | 1999-06-24 | ||
| US60/141,057 | 1999-06-24 | ||
| US09/500,207 | 2000-02-07 | ||
| US09/500,207 US6375923B1 (en) | 1999-06-24 | 2000-02-07 | Processing titaniferous ore to titanium dioxide pigment |
| US09/503,365 | 2000-02-14 | ||
| US09/503,365 US6440383B1 (en) | 1999-06-24 | 2000-02-14 | Processing aqueous titanium chloride solutions to ultrafine titanium dioxide |
| PCT/US2000/016355 WO2001012555A2 (en) | 1999-06-24 | 2000-06-14 | Processing aqueous titanium chloride solutions to ultrafine titanium dioxide |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2003507300A JP2003507300A (ja) | 2003-02-25 |
| JP2003507300A5 JP2003507300A5 (enExample) | 2007-08-02 |
| JP4653916B2 true JP4653916B2 (ja) | 2011-03-16 |
Family
ID=27495454
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2001516860A Expired - Lifetime JP4653916B2 (ja) | 1999-06-24 | 2000-06-14 | 塩化チタン水溶液から超微細二酸化チタンを製造する方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US6440383B1 (enExample) |
| EP (1) | EP1194380B9 (enExample) |
| JP (1) | JP4653916B2 (enExample) |
| AU (1) | AU769225B2 (enExample) |
| CA (1) | CA2375623C (enExample) |
| DE (1) | DE60015763T2 (enExample) |
| WO (1) | WO2001012555A2 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113860364A (zh) * | 2021-09-29 | 2021-12-31 | 李礼 | 一种调控纳米二氧化钛转晶过程的方法 |
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| JP3611303B2 (ja) * | 1997-09-02 | 2005-01-19 | 石原産業株式会社 | 中空状微粉末、該中空状微粉末を粉砕してなる薄片状酸化チタン微粉末およびそれらの製造方法 |
| NZ505774A (en) * | 2000-07-17 | 2002-12-20 | Ind Res Ltd | Oxalate stabilised titania solutions and coating compositions and catalysts formed therefrom |
| AU2001290650A1 (en) | 2000-09-05 | 2002-03-22 | Altair Nanomaterials Inc | Method for producing mixed metal oxides and metal oxide compounds |
| AU2002224394A1 (en) | 2000-10-17 | 2002-04-29 | Altair Nanomaterials Inc. | Method for producing catalyst structures |
| KR100420275B1 (ko) * | 2001-04-06 | 2004-03-02 | (주)아해 | 무기산을 이용한 사염화티타늄 수용액으로부터 TiO2 초미립 분말의 제조방법 |
| DE60202373T2 (de) * | 2001-07-20 | 2005-12-08 | Altair Nanomaterials Inc., Reno | Verfahren zur herstellung von lithiumtitanat |
| EP1282180A1 (en) * | 2001-07-31 | 2003-02-05 | Xoliox SA | Process for producing Li4Ti5O12 and electrode materials |
| US6982073B2 (en) | 2001-11-02 | 2006-01-03 | Altair Nanomaterials Inc. | Process for making nano-sized stabilized zirconia |
| EP1483206B1 (en) * | 2002-03-08 | 2010-10-20 | Altair Nanomaterials Inc. | Process for making nano-sized and sub-micron-sized lithium-transition metal oxides |
| CN1298790C (zh) * | 2002-08-07 | 2007-02-07 | 石原产业株式会社 | 二氧化钛颜料、其生产方法及包含该颜料的树脂组合物 |
| KR100475551B1 (ko) * | 2002-10-08 | 2005-03-10 | (주)아해 | 사염화티타늄과 염산수용액을 이용한 나노크기의 브루카이트상 이산화티타늄 분말의 제조방법 |
| US7140567B1 (en) * | 2003-03-11 | 2006-11-28 | Primet Precision Materials, Inc. | Multi-carbide material manufacture and use as grinding media |
| US20050100965A1 (en) | 2003-11-12 | 2005-05-12 | Tariq Ghayur | IL-18 binding proteins |
| US20050232851A1 (en) * | 2003-11-13 | 2005-10-20 | Jan Prochazka | Process to make rutile pigment from aqueous titanium solutions |
| US7482304B2 (en) | 2003-12-10 | 2009-01-27 | Altair Nanomaterials Inc. | Method for producing structures |
| US7407690B2 (en) * | 2004-03-23 | 2008-08-05 | Altair Nanomaterials Inc. | Process for surface modifications of TiO2 particles and other ceramic materials |
| US7368523B2 (en) | 2004-11-12 | 2008-05-06 | Eastman Chemical Company | Polyester polymer and copolymer compositions containing titanium nitride particles |
| CN101005833A (zh) * | 2004-08-20 | 2007-07-25 | 3M创新有限公司 | 具有半透明保护膜的透皮药物递送装置 |
| CN101006016A (zh) * | 2004-08-26 | 2007-07-25 | 三井化学株式会社 | 金红石型氧化钛超微粒子 |
| US20060051542A1 (en) * | 2004-09-03 | 2006-03-09 | Zhiyong Xia | Polyester polymer and copolymer compositions containing metallic molybdenum particles |
| US7662880B2 (en) * | 2004-09-03 | 2010-02-16 | Eastman Chemical Company | Polyester polymer and copolymer compositions containing metallic nickel particles |
| US20060110557A1 (en) * | 2004-09-03 | 2006-05-25 | Zhiyong Xia | Polyester polymer and copolymer compositions containing metallic tungsten particles |
| WO2006049831A1 (en) * | 2004-10-14 | 2006-05-11 | Tokusen U.S.A., Inc. | Method of production of high purity silver particles |
| WO2006044495A1 (en) * | 2004-10-14 | 2006-04-27 | Tokusen U.S.A., Inc. | Method for synthesizing nano-sized titanium dioxide particles |
| JP5241994B2 (ja) * | 2004-11-05 | 2013-07-17 | 戸田工業株式会社 | 酸化チタン粒子粉末及び光触媒 |
| CA2586893A1 (en) * | 2004-11-09 | 2006-05-18 | Monogen, Inc. | Vial assembly, sampling apparatus and method for processing liquid-based specimens |
| EP1807352A1 (en) * | 2004-11-11 | 2007-07-18 | Basell Poliolefine Italia S.r.l. | Preparation of tio2 powders from a waste liquid containing titanium compounds |
| JP2008519750A (ja) * | 2004-11-11 | 2008-06-12 | バーゼル・ポリオレフィン・イタリア・ソチエタ・ア・レスポンサビリタ・リミタータ | チタン化合物を含有する廃液からTiO2粉末の製造 |
| US7300967B2 (en) * | 2004-11-12 | 2007-11-27 | Eastman Chemical Company | Polyester polymer and copolymer compositions containing metallic titanium particles |
| KR100627621B1 (ko) * | 2004-11-19 | 2006-09-25 | 한국화학연구원 | 루타일형 티타니아 나노 졸의 제조방법 |
| US20060122300A1 (en) * | 2004-12-07 | 2006-06-08 | Zhiyong Xia | Polyester polymer and copolymer compositions containing steel particles |
| US20060177614A1 (en) * | 2005-02-09 | 2006-08-10 | Zhiyong Xia | Polyester polymer and copolymer compositions containing metallic tantalum particles |
| DE102005022076A1 (de) * | 2005-02-25 | 2006-09-07 | Heubach Gmbh | Pastellweißes, feinteiliges, hochdeckendes und dotiertes Rutilpigment mit verminderter Photoaktivität, ein Verfahren zu dessen Herstellung und dessen Verwendung |
| US20060210798A1 (en) * | 2005-03-16 | 2006-09-21 | Clemens Burda | Doped metal oxide nanoparticles and methods for making and using same |
| US7326399B2 (en) * | 2005-04-15 | 2008-02-05 | Headwaters Technology Innovation, Llc | Titanium dioxide nanoparticles and nanoparticle suspensions and methods of making the same |
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| CN109354062A (zh) * | 2018-11-26 | 2019-02-19 | 昆明冶金研究院 | 一种锐钛型纳米二氧化钛及其制备方法与应用 |
| CN119372485A (zh) | 2018-12-14 | 2025-01-28 | 阿瓦塔纳有限公司 | 从含钛材料中提取产品的方法 |
| US11673812B2 (en) | 2019-08-15 | 2023-06-13 | Scandium International Mining Corporation | Countercurrent process for recovering high purity copper sulfate values from low grade ores |
| US12338509B2 (en) | 2019-08-20 | 2025-06-24 | Scandium International Mining Corporation | Byproduct scandium recovery from low grade primary metal oxide ores |
| US11821057B2 (en) | 2020-03-06 | 2023-11-21 | Scandium Internatlonal Mlning Corporatlon | Recovery of critical metals from SX-EW copper raffinate and other solutions derived from leaching ores with sulfuric acid |
| KR102411275B1 (ko) * | 2021-09-15 | 2022-06-23 | 주식회사 한내포티 | 타이타늄 함유 염산용액을 이용한 아나타제형 이산화타이타늄 제조 방법 및 타이타늄 함유 염산용액을 이용한 이산화타이타늄 결정 제어 방법 |
| WO2023043095A1 (ko) * | 2021-09-15 | 2023-03-23 | 주식회사 한내포티 | 탈질폐촉매 함유 유가금속의 추출방법 |
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-
2000
- 2000-02-14 US US09/503,365 patent/US6440383B1/en not_active Expired - Lifetime
- 2000-06-14 EP EP00982051A patent/EP1194380B9/en not_active Expired - Lifetime
- 2000-06-14 WO PCT/US2000/016355 patent/WO2001012555A2/en not_active Ceased
- 2000-06-14 DE DE60015763T patent/DE60015763T2/de not_active Expired - Lifetime
- 2000-06-14 JP JP2001516860A patent/JP4653916B2/ja not_active Expired - Lifetime
- 2000-06-14 CA CA002375623A patent/CA2375623C/en not_active Expired - Lifetime
- 2000-06-14 AU AU19128/01A patent/AU769225B2/en not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113860364A (zh) * | 2021-09-29 | 2021-12-31 | 李礼 | 一种调控纳米二氧化钛转晶过程的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2001012555A3 (en) | 2001-10-11 |
| EP1194380B9 (en) | 2005-06-08 |
| JP2003507300A (ja) | 2003-02-25 |
| DE60015763D1 (de) | 2004-12-16 |
| US6440383B1 (en) | 2002-08-27 |
| AU769225B2 (en) | 2004-01-22 |
| DE60015763T2 (de) | 2005-03-31 |
| EP1194380B1 (en) | 2004-11-10 |
| AU1912801A (en) | 2001-03-13 |
| CA2375623A1 (en) | 2001-02-22 |
| WO2001012555A2 (en) | 2001-02-22 |
| EP1194380A2 (en) | 2002-04-10 |
| CA2375623C (en) | 2009-05-12 |
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