DE60133405D1 - Verfahren zur herstellung von lithiummetallverbindungen, die zur verwendung als kathodenaktivmasse geeignet sind - Google Patents

Verfahren zur herstellung von lithiummetallverbindungen, die zur verwendung als kathodenaktivmasse geeignet sind

Info

Publication number
DE60133405D1
DE60133405D1 DE60133405T DE60133405T DE60133405D1 DE 60133405 D1 DE60133405 D1 DE 60133405D1 DE 60133405 T DE60133405 T DE 60133405T DE 60133405 T DE60133405 T DE 60133405T DE 60133405 D1 DE60133405 D1 DE 60133405D1
Authority
DE
Germany
Prior art keywords
metal
lithium
active compound
lithium metal
metal compounds
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60133405T
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English (en)
Other versions
DE60133405T2 (de
Inventor
Jeremy Barker
Saidi M Yazid
Jeffrey L Swoyer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Valence Technology Inc
Original Assignee
Valence Technology Inc
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Filing date
Publication date
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First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=24908921&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DE60133405(D1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Valence Technology Inc filed Critical Valence Technology Inc
Application granted granted Critical
Publication of DE60133405D1 publication Critical patent/DE60133405D1/de
Publication of DE60133405T2 publication Critical patent/DE60133405T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/45—Phosphates containing plural metal, or metal and ammonium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/455—Phosphates containing halogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G31/00—Compounds of vanadium
    • C01G31/006—Compounds containing, besides vanadium, two or more other elements, with the exception of oxygen or hydrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G37/00—Compounds of chromium
    • C01G37/006—Compounds containing, besides chromium, two or more other elements, with the exception of oxygen or hydrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G49/00—Compounds of iron
    • C01G49/009—Compounds containing, besides iron, two or more other elements, with the exception of oxygen or hydrogen
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/485—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028—Positive electrodes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Secondary Cells (AREA)
DE60133405T 2000-11-28 2001-11-19 Verfahren zur herstellung von lithiummetallverbindungen, die zur verwendung als kathodenaktivmasse geeignet sind Expired - Lifetime DE60133405T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US09/724,085 US6645452B1 (en) 2000-11-28 2000-11-28 Methods of making lithium metal cathode active materials
US724085 2000-11-28
PCT/US2001/043633 WO2002044084A2 (en) 2000-11-28 2001-11-19 Methods of making lithium metal compounds useful as cathode active materials

Publications (2)

Publication Number Publication Date
DE60133405D1 true DE60133405D1 (de) 2008-05-08
DE60133405T2 DE60133405T2 (de) 2009-04-09

Family

ID=24908921

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60133405T Expired - Lifetime DE60133405T2 (de) 2000-11-28 2001-11-19 Verfahren zur herstellung von lithiummetallverbindungen, die zur verwendung als kathodenaktivmasse geeignet sind

Country Status (12)

Country Link
US (2) US6645452B1 (de)
EP (3) EP1343720B1 (de)
JP (2) JP4248876B2 (de)
KR (4) KR100851484B1 (de)
CN (1) CN100411977C (de)
AT (1) ATE390385T1 (de)
AU (1) AU2002217799A1 (de)
CA (4) CA2636694C (de)
DE (1) DE60133405T2 (de)
RU (1) RU2003119145A (de)
TW (1) TW544967B (de)
WO (1) WO2002044084A2 (de)

Families Citing this family (123)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1094533A1 (de) * 1999-04-06 2001-04-25 Sony Corporation Aktives material für positive platte, nichtwässrige sekundäre elektrolytische zelle und verfahren zur herstellung aktiven materials für positive platte
US6528033B1 (en) * 2000-01-18 2003-03-04 Valence Technology, Inc. Method of making lithium-containing materials
US6387568B1 (en) * 2000-04-27 2002-05-14 Valence Technology, Inc. Lithium metal fluorophosphate materials and preparation thereof
US8057769B2 (en) 2000-04-27 2011-11-15 Valence Technology, Inc. Method for making phosphate-based electrode active materials
US6964827B2 (en) 2000-04-27 2005-11-15 Valence Technology, Inc. Alkali/transition metal halo- and hydroxy-phosphates and related electrode active materials
US7524584B2 (en) 2000-04-27 2009-04-28 Valence Technology, Inc. Electrode active material for a secondary electrochemical cell
US6777132B2 (en) * 2000-04-27 2004-08-17 Valence Technology, Inc. Alkali/transition metal halo—and hydroxy-phosphates and related electrode active materials
US8367036B2 (en) 2000-04-27 2013-02-05 Valence Technology, Inc. Alkali/transition metal halo-and hydroxy-phosphates and related electrode active materials
US6794084B2 (en) * 2002-07-26 2004-09-21 Valence Technology, Inc. Alkali metal hydrogen phosphates as precursors for phosphate-containing electrochemical active materials
US7371338B2 (en) * 2002-10-01 2008-05-13 Rutgers, The State University Metal fluorides as electrode materials
DE10255124A1 (de) * 2002-11-26 2004-06-03 Degussa Ag Pyrogenes Oxidpulver, Verfahren zu seiner Herstellung und seine Verwendung in einem Separator für eine elektrochemische Zelle
WO2005031954A2 (en) 2003-09-22 2005-04-07 Valence Technology, Inc. Electrical systems, power supply apparatuses, and power supply operations methods
CA2543851C (en) * 2003-10-27 2014-05-06 Mitsui Engineering & Shipbuilding Co., Ltd. Cathode material for secondary battery and method for producing the material for secondary battery
CA2791156C (en) 2003-12-23 2015-12-15 Universite De Montreal Process for preparing electroactive insertion compounds and electrode materials obtained therefrom
US7719227B2 (en) 2004-02-13 2010-05-18 Valence Technology, Inc. Electrical energy supply methods and electrical energy power supplies
US7060238B2 (en) * 2004-03-04 2006-06-13 Valence Technology, Inc. Synthesis of metal phosphates
US7824800B1 (en) 2004-04-08 2010-11-02 Electrochemical Systems, Inc. Lithium-ion cell with a wide operating temperature range
US7582380B1 (en) 2004-04-08 2009-09-01 Electrochemical Systems, Inc. Lithium-ion cell with a wide operating temperature range
US7960057B2 (en) * 2004-05-17 2011-06-14 Toyota Motor Engineering & Manufacturing North America, Inc. Battery with molten salt electrolyte and phosphorus-containing cathode
US7338647B2 (en) * 2004-05-20 2008-03-04 Valence Technology, Inc. Synthesis of cathode active materials
US7629080B1 (en) 2004-07-23 2009-12-08 The United States Of America As Represented By The Secretary Of The Army Electrode materials for electrochemical cells
TWI459616B (zh) * 2004-08-16 2014-11-01 Showa Denko Kk Lithium batteries with positive and the use of its lithium batteries
US20060091362A1 (en) * 2004-11-02 2006-05-04 Wixom Michael R Composite electrochemical material
US20070160519A1 (en) * 2005-03-28 2007-07-12 Jeremy Barker Method Of Making Active Materials For Use In Secondary Electrochemical Cells
US7700236B2 (en) * 2005-09-09 2010-04-20 Aquire Energy Co., Ltd. Cathode material for manufacturing a rechargeable battery
TWI254031B (en) * 2005-05-10 2006-05-01 Aquire Energy Co Ltd Manufacturing method of LixMyPO4 compound with olivine structure
JP4869629B2 (ja) * 2005-05-30 2012-02-08 住友大阪セメント株式会社 リチウム電池用正極活物質の製造方法及びリチウム電池用正極活物質並びにリチウム電池
US8158090B2 (en) 2005-08-08 2012-04-17 A123 Systems, Inc. Amorphous and partially amorphous nanoscale ion storage materials
US7939201B2 (en) * 2005-08-08 2011-05-10 A123 Systems, Inc. Nanoscale ion storage materials including co-existing phases or solid solutions
US8323832B2 (en) * 2005-08-08 2012-12-04 A123 Systems, Inc. Nanoscale ion storage materials
US7524529B2 (en) * 2005-09-09 2009-04-28 Aquire Energy Co., Ltd. Method for making a lithium mixed metal compound having an olivine structure
CN101361210B (zh) * 2005-12-02 2014-11-26 A123系统公司 非晶态或部分非晶态的纳米级离子贮存材料
CN100388535C (zh) * 2005-12-19 2008-05-14 南开大学 锂离子二次电池正极材料氟化磷酸钒锂的制备方法
KR20130106440A (ko) 2006-02-28 2013-09-27 프리메트 프리시젼 머테리알스, 인크. 리튬계 화합물 나노입자 조성물 및 이의 제조 방법
FR2898885B1 (fr) * 2006-03-27 2008-05-30 Commissariat Energie Atomique Compose a base de disphosphate de titane et de carbone, procede de preparation et utilisation comme materiau actif d'une electrode pour accumulateur au lithium.
US7723958B2 (en) 2006-03-31 2010-05-25 Valence Technology, Inc. Battery charge indication methods, battery charge monitoring devices, rechargeable batteries, and articles of manufacture
CN101506094B (zh) * 2006-08-21 2011-12-28 株式会社Lg化学 制备锂金属磷酸盐的方法
US20090061314A1 (en) * 2007-08-30 2009-03-05 Ming Dong Method of Processing Active Materials For Use In Secondary Electrochemical Cells
CN101542787A (zh) 2006-09-25 2009-09-23 德克萨斯州立大学董事会 用于锂离子电池的阳离子取代的尖晶石氧化物和氟氧化物阴极
EP2266160A4 (de) 2006-10-17 2010-12-29 Valence Technology Inc Verfahren und vorrichtung zum überwachen und steuern einer elektrochemischen zelle
CN100435390C (zh) * 2007-01-12 2008-11-19 中南大学 溶胶凝胶法合成锂离子电池正极材料氟磷酸钒锂
JP4983356B2 (ja) * 2007-04-10 2012-07-25 株式会社豊田中央研究所 水系リチウム二次電池
JP4336372B2 (ja) * 2007-04-27 2009-09-30 Ｔｄｋ株式会社 電極用複合粒子及びその製造方法、並びに、電気化学デバイス
WO2008141422A1 (en) * 2007-05-21 2008-11-27 Transfert Plus, S.E.C. Processes for preparing inorganic phosphates
US20080305256A1 (en) * 2007-06-08 2008-12-11 Conocophillips Company Method for producing lithium vanadium polyanion powders for batteries
US20080303004A1 (en) * 2007-06-08 2008-12-11 Conocophillips Company Method for producing lithium transition metal polyanion powders for batteries
WO2009015565A1 (en) * 2007-07-31 2009-02-05 Byd Company Limited Method for preparing lithium iron phosphate as positive electrode active material for lithium ion secondary battery
US20090035661A1 (en) * 2007-08-01 2009-02-05 Jeffrey Swoyer Synthesis of cathode active materials
US20090068080A1 (en) * 2007-09-06 2009-03-12 Valence Technology, Inc. Method of Making Active Materials For Use in Secondary Electrochemical Cells
CN101399343B (zh) * 2007-09-25 2011-06-15 比亚迪股份有限公司 锂离子二次电池正极活性物质磷酸铁锂的制备方法
CN101420048A (zh) * 2007-10-26 2009-04-29 比亚迪股份有限公司 一种锂离子二次电池的制备方法
KR101188069B1 (ko) * 2007-11-14 2012-10-04 천-유 창 리튬 이온 배터리 분야용 공기 민감성 전극 물질을 생산하는 방법 및 장치
CN101453019B (zh) * 2007-12-07 2011-01-26 比亚迪股份有限公司 含磷酸亚铁锂的正极活性物质及其制备方法和正极及电池
US20090148377A1 (en) * 2007-12-11 2009-06-11 Moshage Ralph E Process For Producing Electrode Active Material For Lithium Ion Cell
CN101471432B (zh) * 2007-12-27 2012-11-21 比亚迪股份有限公司 一种隔膜及其制备方法及锂离子电池
CN101494305B (zh) * 2008-01-25 2011-05-18 比亚迪股份有限公司 锂离子电池电解液和含有该电解液的电池及电池组
US8088305B2 (en) * 2008-02-22 2012-01-03 Byd Company Limited Lithium iron phosphate cathode material
US8057711B2 (en) * 2008-02-29 2011-11-15 Byd Company Limited Composite compound with mixed crystalline structure
US8062560B2 (en) * 2008-02-29 2011-11-22 Byd Company Limited Composite compound with mixed crystalline structure
US20090220858A1 (en) * 2008-02-29 2009-09-03 Byd Company Limited Composite Compound With Mixed Crystalline Structure
US8062559B2 (en) * 2008-02-29 2011-11-22 Byd Company Limited Composite compound with mixed crystalline structure
US8052897B2 (en) * 2008-02-29 2011-11-08 Byd Company Limited Composite compound with mixed crystalline structure
US8148015B2 (en) * 2008-03-21 2012-04-03 Byd Company Limited Cathode materials for lithium batteries
US8951668B2 (en) 2010-11-19 2015-02-10 Rutgers, The State University Of New Jersey Iron oxyfluoride electrodes for electrochemical energy storage
WO2009143324A1 (en) * 2008-05-23 2009-11-26 Rutgers, The State University Iron oxyfluoride electrodes for electochemcial energy storage
CN101597089A (zh) * 2008-06-06 2009-12-09 比亚迪股份有限公司 一种过渡金属氢氧化物及其氧化物和正极材料的制备方法
CN101640288B (zh) * 2008-07-30 2012-03-07 比亚迪股份有限公司 一种锂离子电池电解液及含有该电解液的锂离子电池
WO2010023129A2 (en) * 2008-08-29 2010-03-04 Basf Se New alkali transition metal fluorophosphates
CN105322166B (zh) 2008-10-22 2020-06-12 株式会社Lg化学 橄榄石型锂铁磷酸盐、包含其的正极混合物及其分析方法
US20100154206A1 (en) * 2008-12-19 2010-06-24 Conocophillips Company Process for making composite lithium powders for batteries
KR20170064562A (ko) * 2008-12-19 2017-06-09 파이로텍, 인크. 전지용 플루오르화 리튬 바나듐 폴리음이온 분말의 제조 방법
US8022009B2 (en) * 2009-01-16 2011-09-20 Intematix Corporation Process for synthesizing LixFeMZO4/ carbon and LixMZO4/ carbon composite materials
DE102009001204A1 (de) * 2009-02-26 2010-09-02 Chemische Fabrik Budenheim Kg Herstellung von Eisenorthophosphat
US20100266474A1 (en) * 2009-04-16 2010-10-21 Titus Faulkner Method of Making Active Materials for Use in Secondary Electrochemical Cells
US8372540B2 (en) * 2009-04-16 2013-02-12 Valence Technology, Inc. Electrode active material for secondary electrochemical cell
US9682861B2 (en) * 2009-05-04 2017-06-20 Meecotech, Inc. Electrode active composite materials and methods of making thereof
KR101748406B1 (ko) 2009-08-07 2017-06-16 가부시키가이샤 한도오따이 에네루기 켄큐쇼 양극 활물질의 제작 방법
FR2952367B1 (fr) * 2009-11-10 2012-09-28 Commissariat Energie Atomique Synthese d'un fluorophosphate metallique et utilisation comme materiau actif d'electrode pour accumulateur
KR101134511B1 (ko) 2009-12-21 2012-04-13 한국과학기술원 망간을 기초로 하는 올리빈 복합고용체 및 이의 제조 방법
EP2355214B1 (de) * 2010-01-28 2013-12-25 Prayon Lithium-Akku auf Lithiumeisenphosphat und Kohlenstoffbasis
US9318741B2 (en) 2010-04-28 2016-04-19 Semiconductor Energy Laboratory Co., Ltd. Positive electrode active material of power storage device, power storage device, electrically propelled vehicle, and method for manufacturing power storage device
CN102263235A (zh) * 2010-05-27 2011-11-30 群顺绿能股份有限公司 含锂电极材料烧结方法
DE102010022883A1 (de) * 2010-06-07 2011-12-08 Harmony Brother Co., Ltd. Verfahren zum Sintern eines Lithium enthaltenden Elektrodenmaterials
JP5609485B2 (ja) * 2010-09-22 2014-10-22 Tdk株式会社 活物質、活物質の製造方法、電極及びリチウムイオン二次電池
CN106229475B (zh) 2010-10-08 2019-12-17 株式会社半导体能源研究所 储能装置用正极活性材料的制造方法及储能装置
JP2012204322A (ja) * 2011-03-28 2012-10-22 Gs Yuasa Corp 非水電解質二次電池用活物質の製造方法
KR101219401B1 (ko) * 2011-05-31 2013-01-15 전자부품연구원 이차전지용 양극재료 및 이의 제조방법
CN102315439A (zh) * 2011-09-14 2012-01-11 耿世达 一种锰酸钒锂正极材料及其制造方法
JP2013069456A (ja) 2011-09-21 2013-04-18 Fuji Heavy Ind Ltd 正極活物質の製造方法、正極、および蓄電デバイス
JP2013093316A (ja) * 2011-10-04 2013-05-16 Semiconductor Energy Lab Co Ltd 二次粒子の作製方法と蓄電装置の電極の作製方法
CN102354754A (zh) * 2011-10-26 2012-02-15 张爱萍 硼、钡活化磷酸铁锂正极材料
US10128491B2 (en) * 2011-12-01 2018-11-13 Nanoscale Components, Inc. Method for alkaliating electrodes
DE102011056815A1 (de) * 2011-12-21 2013-08-01 Chemische Fabrik Budenheim Kg Nährstoffzusammensetzung für biologische Systeme
JP5821877B2 (ja) * 2012-03-27 2015-11-24 Tdk株式会社 リチウムイオン二次電池
JP5621869B2 (ja) * 2012-03-27 2014-11-12 Tdk株式会社 リチウムイオン二次電池
RU2506668C1 (ru) * 2012-06-05 2014-02-10 Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Самарский государственный технический университет" Расплавляемый электролит для химического источника тока
US9692039B2 (en) 2012-07-24 2017-06-27 Quantumscape Corporation Nanostructured materials for electrochemical conversion reactions
US20140147586A1 (en) * 2012-11-27 2014-05-29 Universite De Montreal Process for making an alkali metal oxyanion comprising iron
GB201221425D0 (en) 2012-11-28 2013-01-09 Faradion Ltd Metal-containing compound
KR101400593B1 (ko) * 2012-12-06 2014-05-27 삼성정밀화학 주식회사 양극 활물질, 이의 제조방법 및 이를 포함하는 리튬 이차 전지
KR101489779B1 (ko) * 2013-01-21 2015-02-04 포항공과대학교 산학협력단 고상 반응을 이용한 리튬 이차전지의 양극 활물질용 불소 화합물의 제조방법, 양극 및 이 양극을 포함하는 리튬 이차전지
ES2870712T3 (es) * 2013-02-01 2021-10-27 Emd Acquisition Llc Composiciones mejoradas de óxido de litio manganeso
JP6111118B2 (ja) * 2013-03-29 2017-04-05 Fdk株式会社 リチウム二次電池用電極活物質の製造方法
GB201308654D0 (en) 2013-05-14 2013-06-26 Faradion Ltd Metal-containing compounds
RU2542721C1 (ru) * 2013-09-27 2015-02-27 Общество с ограниченной ответственностью "Научный центр "Автономные источники тока" (ООО "Научный центр "АИТ") Композитный катодный материал литий-ионного аккумулятора на основе li3v2(po4)3со структурой насикон и способ его получения
WO2015130831A1 (en) 2014-02-25 2015-09-03 Quantumscape Corporation Hybrid electrodes with both intercalation and conversion materials
US10326135B2 (en) 2014-08-15 2019-06-18 Quantumscape Corporation Doped conversion materials for secondary battery cathodes
JP6326366B2 (ja) * 2014-12-25 2018-05-16 信越化学工業株式会社 リチウムリン系複合酸化物炭素複合体及びその製造方法並びに、電気化学デバイス及びリチウムイオン二次電池
KR20160112665A (ko) * 2015-03-20 2016-09-28 자동차부품연구원 리튬이차전지, 리튬이차전지 전극 소재 및 그 제조방법
EP3314686A4 (de) 2015-06-26 2019-08-07 A123 Systems LLC Kathode mit nanoskaliger porenstruktur für hochleistungsanwendungen und materialsyntheseverfahren
RU2619600C2 (ru) * 2015-09-28 2017-05-17 Федеральное государственное бюджетное образовательное учреждение высшего образования "Московский государственный университет имени М.В. Ломоносова" (МГУ) Электродный материал для металл-ионных аккумуляторов, способ его получения, электрод и аккумулятор на основе электродного материала
KR20180032988A (ko) 2016-09-23 2018-04-02 삼성전자주식회사 양극활물질, 양극활물질의 제조방법 및 이를 포함한 전고체형 전지
FR3067709B1 (fr) * 2017-06-16 2020-06-19 Rhodia Operations Procede de preparation d'un phosphate de vanadium
US11380879B2 (en) 2017-07-10 2022-07-05 Nanoscale Components, Inc. Method for forming an SEI layer on an anode
JP7048266B2 (ja) * 2017-11-13 2022-04-05 大陽日酸株式会社 正極活物質の製造方法
US11251430B2 (en) 2018-03-05 2022-02-15 The Research Foundation For The State University Of New York ϵ-VOPO4 cathode for lithium ion batteries
TWI719496B (zh) * 2019-06-06 2021-02-21 台灣立凱電能科技股份有限公司 二次電池用正極材料之製造方法
RU2727620C1 (ru) * 2019-11-27 2020-07-22 Общество с ограниченной ответственностью "РУСТОР" Способ получения активного материала катода на основе литий-обогащенного фосфата Li1+xFe1-yPO4 со структурой оливина, электродная масса и катод литий-ионного аккумулятора
CN110950315A (zh) * 2019-12-24 2020-04-03 广东石油化工学院 一种复合离子掺杂的磷酸铁锂材料的制备方法
RU2748159C1 (ru) * 2020-12-11 2021-05-20 Автономная некоммерческая образовательная организация высшего образования "Сколковский институт науки и технологий" (Сколковский институт науки и технологий) Электродный материал для натрий-ионных аккумуляторов, способ его получения, электрод и аккумулятор на основе электродного материала
KR102369513B1 (ko) * 2021-03-29 2022-03-04 국민대학교산학협력단 플루오르인산염 기반 이차전지 양극활물질의 제조 방법, 이를 통하여 제조된 플루오르인산염 기반 이차전지 양극활물질 및 이차전지
CN113178615A (zh) * 2021-03-30 2021-07-27 深圳市新创材料科技有限公司 一种latp固态电解质的制备方法
WO2022215582A1 (ja) * 2021-04-07 2022-10-13 株式会社豊田自動織機 正極活物質、正極及びリチウムイオン二次電池

Family Cites Families (77)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2508878A (en) 1945-03-24 1950-05-23 Dow Chemical Co Process for the production of carbothermal magnesium furnace charge
US2570232A (en) 1945-06-26 1951-10-09 North Carolina Magnesium Dev C Continuous process for recovery of magnesium
US3865745A (en) 1971-01-15 1975-02-11 Grace W R & Co Process for the preparation of metal carbide and metal oxide microspheres
US3736184A (en) 1972-03-29 1973-05-29 Mallory & Co Inc P R Metal phosphate and metal arsenate organic electrolyte cells
US4009092A (en) 1976-02-27 1977-02-22 E. I. Du Pont De Nemours And Company Substituted lithium phosphates and solid electrolytes therefrom
US4049891A (en) 1976-06-21 1977-09-20 Massachusetts Institute Of Technology Compositions for fast alkali-metal-ion transport
GB1565065A (en) 1976-08-23 1980-04-16 Tetronics Res & Dev Co Ltd Carbothermal production of aluminium
US4194062A (en) 1978-07-27 1980-03-18 Bell Telephone Laboratories, Incorporated Rechargeable dichalcogenide cell
US4246253A (en) 1978-09-29 1981-01-20 Union Carbide Corporation MnO2 derived from LiMn2 O4
FR2457018A1 (fr) 1979-02-16 1980-12-12 Accumulateurs Fixes Matiere active positive pour generateur electrochimique a electrolyte non aqueux et methode de preparation de celle-ci
IT1131478B (it) 1980-05-13 1986-06-25 Consiglio Nazionale Ricerche Pile ricaricabili ad elevata energia specifica con anodo e catodo a intercalazione
JPS56162477A (en) 1980-05-20 1981-12-14 Nippon Telegr & Teleph Corp <Ntt> Battery
US4434216A (en) 1980-10-24 1984-02-28 Rayovac Corporation Solid state electrolyte
US4427652A (en) * 1980-12-31 1984-01-24 Colgate-Palmolive Company Antigingivitis composition
NO158361C (no) * 1981-07-03 1988-08-31 Intradal Nv Tannpleiemiddel med antikaries-virkning.
US4512905A (en) 1982-05-18 1985-04-23 The Texas A&M University System Method of making sodium zirconium silico-phosphates
US4707422A (en) 1983-06-27 1987-11-17 Voltaix, Inc. Composite coating for electrochemical electrode and method
FR2563382B1 (fr) 1984-04-24 1986-05-30 Elf Aquitaine Nouveau generateur electrochimique a electrode composite
FR2576712B1 (fr) 1985-01-30 1988-07-08 Accumulateurs Fixes Generateur electrochimique a electrolyte non aqueux
CA1265580A (en) 1985-05-10 1990-02-06 Akira Yoshino Secondary battery
JPS61263069A (ja) 1985-05-17 1986-11-21 Matsushita Electric Ind Co Ltd 電池
JPS62176054A (ja) 1986-01-30 1987-08-01 Nippon Telegr & Teleph Corp <Ntt> リチウム電池
GB2196785B (en) 1986-10-29 1990-05-23 Sony Corp Organic electrolyte secondary cell
US4792504A (en) 1987-09-18 1988-12-20 Mhb Joint Venture Liquid containing polymer networks as solid electrolytes
US4830939B1 (en) 1987-10-30 1996-10-08 Mhb Joint Venture Radiation cured solid electrolytes and electrochemical devices employing the same
US5037712A (en) 1987-10-30 1991-08-06 Ultracell, Inc. Preparation of radiation cured solid electrolytes and electrochemical devices employing the same
US4828833A (en) * 1987-12-08 1989-05-09 Colgate-Palmolive Company Dentifrice having decreased abrasivity
US4985317A (en) 1988-11-30 1991-01-15 Japan Synthetic Rubber Co., Ltd. Lithium ion-conductive solid electrolyte containing lithium titanium phosphate
US4990413A (en) 1989-01-18 1991-02-05 Mhb Joint Venture Composite solid electrolytes and electrochemical devices employing the same
US4935317A (en) 1989-06-21 1990-06-19 Mhb Joint Venture Method for producing solid state electrochemical laminar cell utilizing cathode rolling step
US5262548A (en) 1990-05-21 1993-11-16 Scientific Design Company, Inc. Phosphorous/vanadium oxidation catalyst
US5130211A (en) 1990-10-24 1992-07-14 Her Majesty The Queen In Right Of The Provence Of British Columbia Electrolyte solution sequestering agents for electrochemical cells having carbonaceous electrodes
CA2057946A1 (en) 1990-12-20 1992-06-21 Michael M. Thackeray Electrochemical cell
US5173215A (en) 1991-02-21 1992-12-22 Atraverda Limited Conductive titanium suboxide particulates
JPH06505955A (ja) 1991-03-22 1994-07-07 ザ・ダウ・ケミカル・カンパニー 非酸化物セラミック粉末の移動床炭熱合成方法
US5135732A (en) 1991-04-23 1992-08-04 Bell Communications Research, Inc. Method for preparation of LiMn2 O4 intercalation compounds and use thereof in secondary lithium batteries
US5232794A (en) 1991-10-17 1993-08-03 The United States Of America As Represented By The United States Department Of Energy Ionic conductors for solid oxide fuel cells
CA2096386A1 (en) * 1992-05-18 1993-11-19 Masahiro Kamauchi Lithium secondary battery
US5262253A (en) 1992-07-22 1993-11-16 Valence Technology, Inc. Solid electrolytes derived by polymerization of vinyl sulfonate polyalkylene oxides
ZA936168B (en) 1992-08-28 1994-03-22 Technology Finance Corp Electrochemical cell
US5300373A (en) 1992-09-11 1994-04-05 Valence Technology, Inc. Electrochemical cell stack and method of making an electrochemical cell stack
ATE163686T1 (de) 1992-11-16 1998-03-15 Mineral Dev Int As Verfahren zur herstellung metallischen magnesiums, magnesiumoxid oder refraktären materials
RU2038395C1 (ru) 1992-12-17 1995-06-27 Дальневосточный государственный технический университет Способ обезвреживания хромсодержащих отходов гальванического производства
US5296436A (en) 1993-01-08 1994-03-22 Scientific Design Company, Inc. Phosphorous/vanadium oxidation catalyst
US5418090A (en) 1993-02-17 1995-05-23 Valence Technology, Inc. Electrodes for rechargeable lithium batteries
US5418091A (en) 1993-03-05 1995-05-23 Bell Communications Research, Inc. Polymeric electrolytic cell separator membrane
US5540741A (en) 1993-03-05 1996-07-30 Bell Communications Research, Inc. Lithium secondary battery extraction method
US5460904A (en) 1993-08-23 1995-10-24 Bell Communications Research, Inc. Electrolyte activatable lithium-ion rechargeable battery cell
WO1994021560A1 (en) 1993-03-17 1994-09-29 Ultralife Batteries (Uk) Limited Lithiated manganese oxide
US5512214A (en) 1993-03-30 1996-04-30 Koksbang; Rene Lithium battery electrode compositions
US5411820A (en) 1993-06-08 1995-05-02 Valence Technology, Inc. Solid, glyme-containing electrolytes including ion salt derivatives and electrolytic cells produced therefrom
US5384291A (en) 1993-06-25 1995-01-24 The Dow Chemical Company Carbothermal synthesis precursors
JP2966261B2 (ja) 1993-11-02 1999-10-25 三菱電線工業株式会社 リチウム電池用正極材及びその製造方法
US5435054A (en) 1993-11-15 1995-07-25 Valence Technology, Inc. Method for producing electrochemical cell
US5463179A (en) 1993-12-06 1995-10-31 Chaloner-Gill; Benjamin Solid electrolyte obtained by the polymerization of diacrylate monomer having a rigid alkane segment
US5399447A (en) 1993-12-06 1995-03-21 Valence Technology, Inc. Acidity reduction of adhesion promoter layer and electrolytic cells produced therefrom
US5482795A (en) 1994-05-25 1996-01-09 Chaloner-Gill; Benjamin Solid electrolyte utilizing a polymeric matrix obtained by the polymerization of a substituted allylic chloroformate
US5514490A (en) 1994-08-30 1996-05-07 Industrial Technology Research Institute Secondary lithium battery using a new layered anode material
US5643695A (en) 1995-09-26 1997-07-01 Valence Technology, Inc. Carbonaceous electrode and compatible electrolyte
JP3484003B2 (ja) 1995-11-07 2004-01-06 日本電信電話株式会社 非水電解質二次電池
JP3523397B2 (ja) 1995-11-07 2004-04-26 日本電信電話株式会社 非水電解質二次電池
US5910382A (en) 1996-04-23 1999-06-08 Board Of Regents, University Of Texas Systems Cathode materials for secondary (rechargeable) lithium batteries
US6447951B1 (en) * 1996-09-23 2002-09-10 Valence Technology, Inc. Lithium based phosphates, method of preparation, and uses thereof
US5871866A (en) 1996-09-23 1999-02-16 Valence Technology, Inc. Lithium-containing phosphates, method of preparation, and use thereof
US6085015A (en) 1997-03-25 2000-07-04 Hydro-Quebec Lithium insertion electrode materials based on orthosilicate derivatives
US6136472A (en) 1998-06-26 2000-10-24 Valence Technology, Inc. Lithium-containing silicon/phosphates, method of preparation, and uses thereof including as electrodes for a battery
US6153333A (en) * 1999-03-23 2000-11-28 Valence Technology, Inc. Lithium-containing phosphate active materials
JP4710136B2 (ja) * 1999-04-06 2011-06-29 ソニー株式会社 正極活物質の製造方法及び非水電解質二次電池の製造方法
EP1094533A1 (de) 1999-04-06 2001-04-25 Sony Corporation Aktives material für positive platte, nichtwässrige sekundäre elektrolytische zelle und verfahren zur herstellung aktiven materials für positive platte
CA2270771A1 (fr) 1999-04-30 2000-10-30 Hydro-Quebec Nouveaux materiaux d'electrode presentant une conductivite de surface elevee
JP3246480B2 (ja) 1999-06-17 2002-01-15 独立行政法人 農業技術研究機構 造粒方法及び装置
JP3618257B2 (ja) 1999-06-23 2005-02-09 株式会社クボタ 耕耘装置の昇降制御装置
JP3504195B2 (ja) 1999-09-16 2004-03-08 日本電信電話株式会社 リチウム二次電池正極活物質およびリチウム二次電池
JP2001110414A (ja) 1999-10-04 2001-04-20 Nippon Telegr & Teleph Corp <Ntt> リチウム二次電池正極活物質およびリチウム二次電池
US6528033B1 (en) 2000-01-18 2003-03-04 Valence Technology, Inc. Method of making lithium-containing materials
US7001690B2 (en) 2000-01-18 2006-02-21 Valence Technology, Inc. Lithium-based active materials and preparation thereof
US6387568B1 (en) * 2000-04-27 2002-05-14 Valence Technology, Inc. Lithium metal fluorophosphate materials and preparation thereof

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US20040126300A1 (en) 2004-07-01
US6960331B2 (en) 2005-11-01
EP2277829A2 (de) 2011-01-26
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KR20070112297A (ko) 2007-11-22
JP4991662B2 (ja) 2012-08-01
CA2428201C (en) 2008-10-28
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CN100411977C (zh) 2008-08-20
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US6645452B1 (en) 2003-11-11
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