CN1262582C - 具有改进抗刮性的固化涂层、涂覆基材及其有关方法 - Google Patents
具有改进抗刮性的固化涂层、涂覆基材及其有关方法 Download PDFInfo
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- CN1262582C CN1262582C CNB008133549A CN00813354A CN1262582C CN 1262582 C CN1262582 C CN 1262582C CN B008133549 A CNB008133549 A CN B008133549A CN 00813354 A CN00813354 A CN 00813354A CN 1262582 C CN1262582 C CN 1262582C
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Abstract
Description
颗粒材料 | 莫氏硬度(原始标度) |
氮化硅 | 21 |
石墨 | 0.5-12 |
二硫化钼 | 13 |
滑石 | 1-1.54 |
云母 | 2.8-3.25 |
高岭土 | 2.0-2.56 |
石膏 | 1.6-27 |
方解石(碳酸钙) | 38 |
氟化钙 | 49 |
氧化锌 | 4.510 |
铝 | 2.511 |
铜 | 2.5-312 |
铁 | 4-513 |
金 | 2.5-314 |
镍 | 515 |
钯 | 4.816 |
铂 | 4.317 |
银 | 2.5-418 |
硫化锌 | 3.5-419 |
成分 | 当量 | 当量数 | 重量份(kg) |
进料I | |||
三羟甲基丙烷单烯丙醚 | 174.0 | 756.0 | 131.54 |
进料II | |||
MASILWAX BASE1 | 156.72 | 594.8 | 93.21 |
进料III | |||
氯铂酸 | 10ppm | ||
甲苯 | 0.23 | ||
异丙醇 | 0.07 |
成分 | 比较例1 | 比较例2 | 比较例3 | 实施例4 | 实施例5 | 实施例6 | 实施例7 | 实施例8 | 实施例9 | 实施例10 |
甲基戊基酮 | 35.0 | 35.0 | 35.0 | 35.0 | 35.0 | 35.0 | 35.0 | 35.0 | 35.0 | 40.0 |
TINUVIN 9281 | 2.0 | 2.0 | 2.0 | 2.0 | 2.0 | 2.0 | 2.0 | 2.0 | 2.0 | 3.0 |
TINUVIN 1232 | 0.50 | 0.50 | 0.50 | 0.50 | 0.50 | 0.50 | 0.50 | 0.50 | 0.50 | 1.00 |
RESIMENE 7573 | 41.24 | 41.24 | 41.24 | 41.24 | 41.24 | 41.24 | 41.24 | 41.24 | 41.24 | 41.24 |
流动添加剂4 | 0.50 | 0.50 | 0.50 | 0.50 | 0.50 | 0.50 | 0.50 | 0.50 | 0.50 | 0.50 |
催化剂5 | 1.43 | 1.43 | 1.43 | 1.43 | 1.43 | 1.43 | 1.43 | 1.43 | 1.43 | - |
催化剂6 | - | - | - | - | - | - | - | - | - | 2.50 |
氨基甲酸酯官能的丙烯酸类树脂 | 93.75 | 70.17 | 93.34 | 69.91 | 46.73 | 70.31 | 70.31 | 70.31 | 65.63 | 70.31 |
实施例AA的二氧化硅分散液 | - | 23.87 | - | - | 23.87 | - | - | - | - | - |
实施例BB的二氧化硅分散液 | - | - | 10.40 | 10.40 | - | - | - | - | - | - |
实施例CC的二氧化硅分散液 | - | - | - | - | - | 15.09 | - | - | - | - |
实施例DD的二氧化硅分散液 | - | - | - | - | - | - | - | - | 9.23 | - |
实施例EE的二氧化硅分散液 | - | - | - | - | - | - | - | - | - | 33.33 |
实施例B的氨基甲酸酯官能聚硅氧烷 | - | - | - | 18.75 | 18.75 | 4.53 | 18.75 | - | 18.75 | 4.91 |
实施例C的氨基甲酸酯官能聚硅氧烷 | - | - | - | - | - | - | - | 27.53 | - | - |
实施例 | 20°光泽(初始) | 划伤/划痕试验后%初始20°光泽 | 天候老化后划伤/划痕试验后保留的%初始20°光泽 | 努氏硬度 | Byk雾度 |
1 | 89 | 26% | 25% | 10.9 | 14 |
2 | 89 | 58% | 30% | 12.1 | 18 |
3 | 88 | 82% | 86% | 11.2 | 19 |
4 | 50 | 82% | 62% | 12.1 | 294雾度 |
5 | 89 | 85% | 28% | 11.8 | 19 |
6 | 87 | 95% | 94% | 12.1 | 14 |
7 | 89 | 80% | 22% | 11.9 | 14 |
8 | 91 | 69% | 31% | 10.9 | 14 |
9 | 88 | 95% | 93% | 11.2 | 14 |
10 | 86 | 97% | 92% | - | - |
成分 | 比较例11 | 比较例12 | 比较例13 | 比较例14 | 实施例15 | 实施例16 | 实施例17 | 实施例18 |
甲基戊基酮 | 20.0 | 20.0 | 20.0 | 20.0 | 20.0 | 20.0 | 20.0 | 40.0 |
丙烯酸类多醇1 | 89.6 | 89.6 | 89.6 | 89.9 | 43.3 | 43.3 | - | 43.3 |
CYMEL 2022 | - | - | 18.8 | 18.8 | 18.8 | 18.8 | 18.8 | 18.8 |
酸催化剂3 | - | 1.3 | - | 1.3 | - | 1.3 | 1.3 | 1.3 |
实施例4的聚硅氧烷多醇 | - | - | - | - | 23.4 | 23.4 | 20.9 | 13.4 |
二氧化硅分散液4 | - | - | - | - | - | - | 7.7 | 30.8 |
DESMODUR N-33905 | 41.4 | 41.4 | 24.8 | 24.8 | 33.3 | 33.3 | 33.3 | 33.3 |
实施例 | 200光泽(初始) | 划伤/划痕试验后%初始20°光泽 | 天候老化后划伤/划痕试验后保留的%初始20°光泽 | 努氏硬度 | Byk雾度 |
11 | 88 | 17% | 22% | 10.9 | 11 |
12 | 88 | 15% | 19% | 10.0 | 11 |
13 | 90 | 30% | 21% | 10.9 | 10 |
14 | 92 | 57% | 48% | 13.9 | 11 |
15 | 88 | 47% | 14% | 10.0 | 14 |
16 | 89 | 88% | 66% | 9.8 | 15 |
17 | 86 | 98% | 97% | 11.8 | 18 |
18 | 84 | 98% | 98% | 10.5 | 18 |
成分 | 树脂固体 | 二氧化硅固体 | 重量(g) |
乙酸2-甲氧基丙酯 | 2.7 | ||
甲基戊基酮 | 40.0 | ||
TINUVIN 928 | 3.0 | 3.0 | |
TINUVIN 123 | 0.5 | 0.5 | |
氨基甲酸酯官能的丙烯酸类1 | 21.5 | 33.6 | |
氨基甲酸酯官能的聚酯2 | 21.5 | 30.7 | |
氨基甲酸酯官能的聚醚3 | 10.0 | 10.3 | |
二氧化硅分散液4 | 7.0 | 3.0 | 12.8 |
RESIMENE 757 | 40.0 | 41.2 | |
比较例1的流动添加剂 | 0.3 | 0.5 | |
催化剂溶液5 | 1.0 | 2.5 |
成分 | 树脂固体 | 二氧化硅固体 | 重量(g) |
甲基戊基酮 | 35.0 | ||
3-乙氧基丙酸乙酯 | 11.9 | ||
实施例19的二氧化硅分散液 | 4.7 | 2.0 | 8.6 |
TINUVIN 928 | 3.0 | 3.0 | |
CYMEL 202 | 15.0 | 18.8 | |
丙烯酸类多醇1 | 23.6 | 47.2 | |
聚酯多醇2 | 20.3 | 25.3 | |
实施例19的含羟基聚硅氧烷的二氧化硅分散液 | 10.4 | 10.4 | |
TINUVIN 2923 | 0.5 | 0.5 | |
实施例1的流动添加剂 | 0.3 | 0.5 | |
下列两个组分在施涂涂料前加至上述混合物中 | |||
DESMODUR N-3390 | 26.0 | 28.9 | |
实施例12的催化剂 | 1.0 | 1.3 |
实施例 | 20°光(初始) | 划伤/划痕试验后保留的%初始20°光泽 | 天候老化后保留的%初始20°光泽 | 挠性级别 |
实施例19 | 86 | 83 | 55 | 8 |
*市售挠性1K透明涂层 | 88 | 46 | 11 | 8 |
实施例20 | 85 | 69 | 35 | 10 |
*市售挠性2K透明涂层 | 87 | 17 | 8 | 9 |
成分 | 比较例21A(g) | 比较例21B(g) | 实施例21C(g) | 实施例21D(g) | 实施例21E(g) |
甲基戊基酮 | 40.0 | 40.0 | 40.0 | 40.0 | 40.0 |
CYMEL 202 | 2.50 | - | - | - | - |
二氧化硅分散液1 | - | - | 0.03 | 0.08 | 0.17 |
CYLINK 20002 | - | 28.30 | 28.30 | 28.30 | 28.30 |
聚丙烯酸丁酯 | 0.50 | 0.50 | 0.50 | 0.50 | 0.50 |
N,N-二甲基十二烷基胺 | 0.30 | 0.30 | 0.30 | 0.30 | 0.30 |
丙烯酸类树脂3 | 87.89 | 87.89 | 87.89 | 87.89 | 87.89 |
交联剂4 | 63.69 | 63.69 | 63.69 | 63.69 | 63.69 |
实施例12的催化剂 | - | 1.30 | 1.30 | 1.30 | 1.30 |
实施例 | 初始20°光泽 | 划伤/划痕试验后保留的%初始20°光泽 | 天候老化后划痕(划伤)试验后保留的%初始20°光泽 |
21A* | 84 | 14 | 12 |
21B* | 86 | 27 | 23 |
21C | 86 | 49 | 42 |
21D | 86 | 67 | 58 |
21E | 85 | 80 | 68 |
硅氧烷代码 | 羟基当量 | 说明 |
实施例A的聚硅氧烷 | 190 | 含Si-H的戊硅氧烷与三羟甲基丙烷单烯丙醚的反应产物 |
KR2001 | 252 | 购自Shin-Etsu Chemical Co.的羟基官能的甲基和苯基硅氧烷 |
BYK 370 | 1600 | 购自BYK Chemie的聚酯改性的羟基官能的二甲基聚硅氧烷 |
BYK 373 | 701 | 购自BYK Chemie的聚醚改性的羟基官能的二甲基聚硅氧烷 |
BYK 375 | 1870 | 购自BYK Chemie的聚醚-聚酯改性的羟基官能的二甲基聚硅氧烷 |
BYK 325 | 0 | 购自BYK Chemie的聚醚改性的甲基烷基聚硅氧烷 |
BYK 310 | 0 | 购自BYK Chemie的聚酯改性的二甲基聚硅氧烷 |
成分 | 固体重量(g) | 制剂重量(g) |
甲基戊基酮 | - | 31.2 |
CYMEL 202 | 15.0 | 18.8 |
丙烯酸类多醇1 | 61.5 | 102.1 |
聚丙烯酸丁酯 | 0.3 | 0.5 |
DESMODUR N-3390 | 22.4 | 24.9 |
酸式磷酸苯酯催化剂 | 1.0 | 1.3 |
实施例 | %胶体二氧化硅 | %硅氧烷 | 硅氧烷类型 | 初始20°光泽 | 划伤/划痕试验后保留的%初始20°光泽 | 磨擦系数(μ) |
22A | 0 | 0 | - | 86 | 38% | 0.19 |
22B | 2 | 0 | - | 86 | 44% | 0.18 |
22C | 2 | 1.1 | 实施例A的聚硅氧烷 | 84 | 89% | 0.17 |
22D | 2 | 1.5 | KR-2001 | 85 | 51% | 0.12 |
22E | 2 | 1.0 | Byk-370 | 85 | 58% | 0.07 |
22F | 2 | 1.0 | Byk-373 | 起粒(seedy)太多难以试验 | ||
22G | 2 | 1.0 | Byk-375 | 76 | 57% | 0.04 |
22H | 2 | 1.0 | Byk-325 | 起粒太多难以试验 | ||
22I | 2 | 1.0 | Byk-310 | 84 | 52% | 0.09 |
名称 | 固体 | 总重量 |
甲基戊基酮 | - | 66.6 |
Tinuvin 928 | 3.0 | 3.0 |
胶体二氧化硅1 | 5.0 | 16.7 |
Cymel 202 | 15.0 | 18.8 |
实施例A的聚硅氧烷多醇 | 2.0 | 2.0 |
丙烯酸类多醇2 | 63.0 | 106.1 |
Tinuvin 123 | 1.0 | 1.0 |
聚丙烯酸丁酯 | 0.3 | 0.5 |
实施例12的催化剂 | 1.0 | 1.3 |
Desmodur N-33903 | 20.0 | 22.2 |
名称 | 固体 | 总重量 |
甲基戊基酮 | - | 66.2 |
Tinuvin 928 | 3.0 | 3.0 |
ORGANOSILICASOL MT-ST | 5.0 | 16.7 |
Cymel 202 | 15.0 | 18.8 |
实施例23A的丙烯酸类多醇 | 65.7 | 110.7 |
Tinuvin 123 | 1.0 | 1.0 |
聚丙烯酸丁酯 | 0.3 | 0.5 |
实施例12的催化剂 | 1.0 | 1.3 |
Desmodur N-3390 | 19.3 | 21.4 |
名称 | 固体 | 总重量 |
甲基戊基酮 | - | 25.0 |
二氧化硅分散液1 | 6.7 | 8.6 |
Tinuvin 928 | 3.0 | 3.0 |
丙烯酸类多醇2 | 35.9 | 65.3 |
Tinuvin 292 | 0.5 | 0.5 |
聚丙烯酸丁酯 | 0.3 | 0.5 |
实施例A的聚硅氧烷多醇 | 15.3 | 15.3 |
Cymel 202 | 15.0 | 18.5 |
实施例12的催化剂 | 0.5 | 0.7 |
Desmodur N-33003 | 29.1 | 29.1 |
成分 | 固体 | 总重量(g) |
甲基戊基酮 | - | 25.0 |
实施例23C的二氧化硅分散液 | 6.7 | 8.6 |
TINUVIN 928 | 3.0 | 3.0 |
实施例23C的丙烯酸类多醇 | 40.9 | 74.4 |
TINUVIN 292 | 0.5 | 0.5 |
聚丙烯酸丁酯流动添加剂 | 0.3 | 0.5 |
实施例A的聚硅氧烷多醇 | 10.3 | 10.3 |
CYMEL 202 | 15.0 | 18.8 |
实施例12的催化剂 | 0.5 | 0.7 |
DESMODUR N-3300 | 29.1 | 29.1 |
成分 | 固体(g) | 总重量(g) |
PROPASOL B1 | - | 45.0 |
CYMEL 3272 | 35.0 | 38.9 |
TINUVIN 11303 | 3.2 | 3.2 |
磷酸化的环氧树脂4 | 0.5 | 0.8 |
二甲基乙醇胺(50%在水中) | - | 2.0 |
胶乳5 | 46.5 | 109.4 |
矿油精 | - | 8.0 |
可水还原的聚氨酯6 | 10.0 | 42.6 |
黑色颜料分散液7 | 11.5 | 47.6 |
二甲基乙醇胺(50%在水中) | - | 1.0 |
去离子水 | - | 57.5 |
实施例25 | %二氧化硅** | 初始抗刮性 | 148小时QUV辐照后的抗刮性 | ||
20°光泽 | 保留的%初始光泽 | 20°光泽 | 保留的%初始光泽 | ||
A* | 0 | 88 | 79% | 89 | 51% |
B | 0.25 | 88 | 89% | 86 | 90% |
C | 0.5 | 86 | 95% | 88 | 91% |
D | 1.0 | 86 | 95% | 87 | 93% |
E | 2.0 | 85 | 93% | 86 | 95% |
F | 4.0 | 85 | 91% | 86 | 95% |
G | 8.5 | 86 | 88% | 87 | 95% |
成分 | 实施例26A | 实施例26B | 实施例26C | 实施例26D |
环氧官能的丙烯酸类1 | 69.05 | 69.05 | 68.98 | 49.11 |
十二烷二酸 | 22.68 | 22.68 | 22.65 | 22.04 |
苯偶姻 | 0.20 | 0.20 | 0.20 | 0.20 |
WAX C MICROPOWDER2 | 0.60 | 0.60 | 0.60 | 0.60 |
TINUVIN 1443 | 2.00 | 2.00 | 2.00 | 2.00 |
CGL-15454 | 2.00 | 2.00 | 2.00 | 2.00 |
HCA-15 | 2.00 | 2.00 | 2.00 | 2.00 |
ARMEEN M2C | 0.37 | 0.37 | 0.37 | 0.37 |
表面活性剂A7 | - | 1.10 | - | - |
表面活性剂B8 | 1.10 | - | - | - |
氧化铝分散体A9 | - | - | 1.20 | - |
氧化铝分散体B10 | - | - | - | 20.58 |
总计 | 100.00 | 100.00 | 100.00 | 100.00 |
抗刮(划伤)级别 | |
比较例A | 对照 |
实施例B | + |
实施例C | ++ |
实施例D | 0 |
成分 | 树脂固体(%) | 总重量(g) |
甲基戊基酮 | - | 45.0 |
TINUVIN 928 | 3.0 | 3.0 |
实施例23C的二氧化硅分散液 | 4.67 | 8.8 |
实施例A的聚硅氧烷多醇 | 10.33 | 10.33 |
Cymel 202 | 15.0 | 18.75 |
实施例23C的丙烯酸类多醇 | 43.10 | 69.68 |
Tinuvin 292 | 0.5 | 0.5 |
实施例12的催化剂 | 0.5 | 0.67 |
DESMODUR N3300 | 23.4 | 23.4 |
DESMODUR Z4470 | 3.5 | 5.0 |
成分 | 当量 | 当量数 | 重量份(kg) |
进料I | |||
三羟甲基丙烷单烯丙醚 | 174.0 | 756.0 | 131.54 |
进料II | |||
MASILWAX BASE1 | 156.72 | 594.8 | 93.21 |
进料III | |||
氯铂酸 | 10ppm | ||
甲苯 | 0.23 | ||
异丙醇 | 0.07 |
成分 | 重量份(g) | 固体重量(g) |
甲基正戊基酮 | 18.0 | - |
Butyl Cellosolye乙酸酯1 | 18.0 | - |
Butyl Carbitol乙酸酯2 | 4.0 | - |
TINUVIN 3843 | 1.58 | 1.50 |
TINUVIN 4004 | 1.76 | 1.50 |
TINUVIN 2925 | 0.40 | 0.40 |
二氧化硅分散液 | 13.2 | 10.0 |
RESIMENE 7576 | 27.1 | 26.3 |
LUWIPAL 0187 | 11.9 | 8.7 |
成分 | 重量份(g) | 固体重量(g) |
氨基甲酰化的丙烯酸类1 | 79.4 | 50.0 |
氨基甲酰化的聚酯2 | 69.4 | 50.0 |
成分 | 重量份(g) | 固体重量(g) |
甲基正戊基酮 | 5.1 | - |
Butyl Cellosolve乙酸酯1 | 10.8 | - |
Butyl Carbitol乙酸酯2 | 1.8 | - |
TINUVIN 9283 | 3.00 | 3.00 |
TINUVIN 2924 | 0.40 | 0.40 |
TINUVIN 1235 | 0.60 | 0.60 |
CYMEL 11306 | 29.9 | 29.9 |
RESIMENE 7417 | 11.3 | 9.9 |
成分 | 重量份(g) | 固体重量(g) |
甲基正戊基酮 | 7.5 | - |
Butyl Cellosolye乙酸酯1 | 15.0 | - |
Butyl Carbitol乙酸酯2 | 2.50 | - |
TINUVIN 9283 | 3.00 | 3.00 |
TINUVIN 2924 | 0.40 | 0.40 |
TINUVIN 1235 | 0.60 | 0.60 |
二氧化硅分散液 | 26.4 | 20.0 |
聚硅氧烷多醇 | 1.00 | 1.00 |
CYMEL11306 | 29.9 | 29.9 |
RESIMENE 7417 | 11.3 | 9.9 |
成分 | 涂料组合物 | ||||
5 | 6 | 7 | 8 | 9 | |
预混物1 | 95.9(48.4) | 95.9(48.4) | - | - | - |
预混物2 | 86.3(58.0) | 57.4(38.6) | - | - | - |
预混物3 | - | - | 63.2(43.8) | 63.2(43.8) | 63.2(43.8) |
二氧化硅分散液 | - | - | - | 13.2(10.0) | 26.4(20.0) |
聚硅氧烷多醇 | - | - | - | 8.0(8.0) | 1.0(1.0) |
树脂A | - | 20.1(19.4) | 62.5(60.2) | 46.9(45.2) | 46.9(45.2) |
Multiflow1 | - | - | 0.60(0.30) | - | - |
聚丙烯酸丁酯2 | 0.50(0.30) | 0.50(0.30) | 0.67(0.40) | 0.67(0.40) | 0.67(0.40) |
封端的酸催化剂3 | 2.50(1.00) | 2.50(1.00) | - | - | - |
酸催化剂4 | - | - | 1.43(1.00) | 1.43(1.00) | 1.43(1.00) |
简要信息 | |||||
甲基正戊基酮 | 3.49 | - | 3.60 | 2.89 | 2.10 |
Butyl Cellosolve乙酸酯5 | 3.49 | - | 7.2 | 5.8 | 4.20 |
Butyl Carbitol乙酸酯6 | 0.76 | - | 1.2 | 0.96 | 0.7 |
喷雾粘度7(秒) | 28 | 28 | 37 | 38 | 38 |
涂料温度(°F) | 73 | 73 | 72 | 72 | 72 |
230°F(110℃)%固体8 | 52 | 58 | 64 | 66 | 68 |
成分 | 涂料组合物 | |||
10 | 11 | 12 | 13 | |
预混物1 | 95.9(48.4) | 95.9(48.4) | 95.9(48.4) | 95.9(48.4) |
预混物2 | 86.3(58.0) | 57.4(38.6) | 57.4(38.6) | 71.9(48.3) |
树脂A | - | 20.1(19.4) | - | - |
树脂B | - | - | 23.1(19.4) | 11.5(9.7) |
聚丙烯酸丁酯1 | 0.50(0.30) | 0.50(0.30) | 0.50(0.30) | 0.50(0.30) |
封端的酸催化剂2 | 2.50(1.00) | 2.50(1.00) | 2.50(1.00) | 2.50(1.00) |
简要信息 | ||||
甲基正戊基酮 | 3.51 | - | - | 1.80 |
Butyl Cellosolve乙酸酯3 | 3.51 | - | - | 1.80 |
Butyl Carbitol乙酸酯4 | 0.78 | - | - | 0.40 |
喷雾粘度7(秒) | 28 | 29 | 28 | 28 |
涂料温度(°F) | 73 | 73 | 74 | 74 |
230°F(110℃)%固体6 | 53 | 58 | 57 | 56 |
成分 | 涂料组合物 | ||
14 | 15 | 16 | |
预混物4 | 97.6(64.8) | 97.6(64.8) | 97.6(64.8) |
预混物2 | - | 33.6(22.6) | 16.8(11.3) |
树脂B | 53.8(45.2) | 26.9(22.6) | 40.4(33.9) |
聚丙烯酸丁酯1 | 0.67(0.40) | 0.67(0.40) | 0.67(0.40) |
酸催化剂2 | 1.43(1.00) | 1.43(1.00) | 1.43(1.00) |
简要信息 | |||
甲基正戊基酮 | 0.62 | 2.7 | 1.48 |
Butyl Cellosolve乙酸酯3 | 1.25 | 5.4 | 2.95 |
Butyl Carbitol乙酸酯4 | 0.21 | 0.90 | 0.49 |
喷雾粘度5(秒) | 27 | 28 | 28 |
涂料温度(°F) | 74 | 74 | 74 |
230°F(110℃)%固体6 | 66 | 63 | 63 |
成分 | 重量份(g) | 固体重量(g) |
Hexyl Cellosolye1 | 20.0 | - |
2-丁氧基乙醇 | 20.0 | - |
磷酸化的环氧树脂2 | 1.00 | 0.60 |
TINUVIN 11303 | 3.00 | 3.00 |
CYMEL 11564 | 25.0 | 25.0 |
VISCOLAM 3305 | 3.33 | 1.00 |
去离子水 | 100.0 | - |
无气味的矿油精6 | 20.0 | - |
BYK-0327 | 3.90 | 2.00 |
丙烯酸类胶乳8 | 125.3 | 51.5 |
SETALUX 6802 AQ-249 | 61.2 | 15.0 |
胺10 | 3.00 | - |
黑色调的糊浆11 | 47.6 | 11.5 |
实施例 | 初始20°光泽1 | 划痕试验后保留的%20°光泽2 | 努氏硬度4 | 再涂覆粘合性5 | |||
初始 | 天候老化3后 | B/C//B/C | B/C//C | ||||
286小时 | 618小时 | ||||||
5 | 85 | 79 | 82 | 84 | 10.3 | 0 | 0 |
6 | 85 | 18 | 25 | 58 | 4.0 | 0 | 0 |
7 | 84 | 1 | 5 | 8 | <2.0 | 0 | 4+ |
8 | 84 | 6 | 14 | 20 | <2.0 | 0 | 4 |
9 | 83 | 1 | 13 | 18 | <2.0 | 0 | 4 |
实施例 | 初始20°光泽1 | 划痕试验后保留的%20°光泽2 | 努氏硬度4 | 再涂覆粘合性5 | |||
初始 | 天候老化3后 | B/C//B/C | B/C//C | ||||
286小时 | 618小时 | ||||||
5 | 87 | 91 | 84 | 71 | 12.7 | 0 | 0 |
6 | 87 | 78 | 80 | 64 | 9.9 | 4+ | 0 |
7 | 87 | 27 | 20 | 20 | 13.8 | 5 | 4+ |
8 | 88 | 81 | 28 | 26 | 11.5 | 4+ | 4 |
9 | 88 | 71 | 53 | 44 | 9.9 | 4+ | 4 |
10 | 87 | 91 | - | - | 10.9 | 1 | 0 |
11 | 86 | 67 | - | - | 7.7 | 4+ | 0 |
12 | 87 | 67 | - | - | 8.1 | 4+ | 0 |
13 | 85 | 91 | - | - | 10.4 | 4 | 0 |
14 | 87 | 49 | - | - | 5.8 | 4+ | 4+ |
15 | 85 | 67 | - | - | 6.7 | 4 | 1+ |
16 | 87 | 59 | - | - | 6.6 | 4+ | 3+ |
组分 | 说明 | 固体 | 重量 |
SR3551 | 二(三羟甲基丙烷)四丙烯酸酯 | 27.3 | 27.3 |
ClariantHIGHLINK OG108-32 | 在三丙二醇二丙烯酸酯中的胶体二氧化硅 | 41.9 | 41.9 |
DAROCURE 42653 | 光引发剂 | 2.0 | 2.0 |
TINUVIN 4003 | UV吸收剂 | 3.0 | 3.0 |
TINUVIN 2923 | 位阻胺光稳定剂 | 0.8 | 0.8 |
RC-68-14972 | 丙烯酸类多醇树脂 | 15.6 | 23.3 |
DESMODUR N-33004 | HDI的异氰脲酸酯 | 9.4 | 9.4 |
总计 | 100.0 | 107.7 |
透明涂层 | 初始20°光泽 | 划痕试验后的20°光泽 | %保留光泽 |
UV/热双重固化 | 82 | 79 | 96 |
成分 | 当量 | 当量数 | 重量份(kg) |
进料I | |||
三羟甲基丙烷单烯丙醚 | 174.0 | 756.0 | 131.54 |
进料II | |||
MASILWAX BASE1 | 156.72 | 594.8 | 93.21 |
进料III | |||
氯铂酸 | 10ppm | ||
甲苯 | 0.23 | ||
异丙醇 | 0.07 |
组分 | 重量份(g) | 固体重量(g) |
甲基正戊基酮 | 18.0 | - |
Butyl Cellosolve乙酸酯1 | 18.0 | - |
Butyl Carbitol乙酸酯2 | 4.0 | - |
TINUVIN9283 | 3.0 | 3.0 |
TINUVIN2924 | 0.40 | 0.40 |
组分 | 实施例2(99-346-93A) | 实施例3(99-346-93B) |
实施例1的预混物 | 43.4(3.4) | 43.4(3.4) |
二氧化硅分散液AA | 10.0(7.0) | 10.0(7.0) |
RESIMENE 7571 | 11.8(11.4) | 11.8(11.4) |
丙烯酸2 | 100.8(65.5) | 74.9(48.7) |
聚丙烯酸丁酯3 | 0.50(0.30) | 0.50(0.30) |
封端的酸催化剂4 | 2.50(1.00) | 2.50(1.00) |
CYLINK20005 | 37.1(19.1) | - |
TRIXENE DP9B/14946 | - | 51.3(35.9) |
简要信息 | ||
甲基正戊基酮 | 2.39 | - |
Butyl Cellosolye乙酸酯7 | 2.39 | - |
Butyl Carbitol乙酸酯8 | 0.53 | - |
喷雾粘度9(秒) | 29 | 26 |
涂料温度(°F) | 73 | 74 |
成分 | 重量份(g) | 固体重量(g) |
正丁氧基丙醇,PNB1 | 45.0 | - |
CYMEL 3272 | 38.9 | 35.0 |
TINUVIN 11303 | 3.20 | 3.20 |
磷酸化的环氧树脂4 | 0.80 | 0.50 |
胺5 | 2.00 | - |
丙烯酸类胶乳6 | 109.4 | 46.5 |
无气味的矿油精7 | 8 | - |
聚氨酯丙烯酸类8 | 42.6 | 10.0 |
黑色调的糊浆9 | 47.6 | 11.5 |
胺5 | 1.00 | - |
去离子水 | 67.7 | - |
实施例 | 初始20°光泽1 | 划痕试验后保留的%20°光泽2 | |||
初始 | 天候老化3 | ||||
240小时 | 504小时 | 1028小时 | |||
2 | 92 | 92 | 84 | 51 | 32 |
3 | 90 | 79 | 85 | 49 | 29 |
成分 | 树脂固体(%) | 总重量(g) |
乙酸丁酯 | - | 11.1 |
DOWANOL PM乙酸酯 | - | 28.6 |
Butyl Cellusolye乙酸酯 | - | 4.1 |
Tinuvin 928 | 3.0 | 3.0 |
实施例23C的二氧化硅分散液 | 6.7 | 8.8 |
实施例A的聚硅氧烷多醇 | 10.3 | 10.3 |
Cymel 202 | 15.0 | 18.8 |
丙烯酸类多醇1 | 22.48 | 31.5 |
Tinuvin 292 | 0.5 | 0.5 |
实施例12的催化剂 | 0.5 | 0.67 |
DESMODUR N3300 | 23.4 | 23.4 |
DESMODUR Z4470 | 3.5 | 5.0 |
成分 | 树脂固体(%) | 总重量(g) |
3-乙氧基丙酸乙酯 | - | 38.7 |
Tinuvin 928 | 3.0 | 3.0 |
实施例23C的二氧化硅分散液 | 6.7 | 8.8 |
实施例A的聚硅氧烷多醇 | 10.3 | 10.3 |
Cymel 202 | 7.5 | 9.4 |
丙烯酸类多醇1 | 39.0 | 57.9 |
Tinuvin 292 | 1.0 | 1.0 |
实施例12的催化剂 | 0.5 | 0.7 |
DESMODUR N3300 | 16.6 | 16.6 |
DESMODUR Z4470 | 21.9 | 31.3 |
Claims (128)
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Application Number | Priority Date | Filing Date | Title |
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US36506999A | 1999-07-30 | 1999-07-30 | |
US09/365,069 | 1999-07-30 | ||
US17189999P | 1999-12-23 | 1999-12-23 | |
US60/171,899 | 1999-12-23 | ||
US48904300A | 2000-01-21 | 2000-01-21 | |
US09/489,043 | 2000-01-21 |
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-
2000
- 2000-07-31 WO PCT/US2000/020836 patent/WO2001009231A1/en active IP Right Grant
- 2000-07-31 ES ES00950897T patent/ES2249285T3/es not_active Expired - Lifetime
- 2000-07-31 DE DE2000622765 patent/DE60022765T2/de not_active Expired - Lifetime
- 2000-07-31 EP EP20000950897 patent/EP1204701B1/en not_active Revoked
- 2000-07-31 CN CNB008133549A patent/CN1262582C/zh not_active Expired - Lifetime
- 2000-07-31 AU AU63927/00A patent/AU770696B2/en not_active Ceased
- 2000-07-31 US US09/629,423 patent/US6387519B1/en not_active Expired - Fee Related
- 2000-07-31 CA CA 2380403 patent/CA2380403C/en not_active Expired - Lifetime
- 2000-07-31 KR KR1020027001349A patent/KR100745875B1/ko active IP Right Grant
- 2000-07-31 MX MXPA02001019 patent/MX238958B/es active IP Right Grant
- 2000-07-31 JP JP2001521985A patent/JP4284020B2/ja not_active Expired - Fee Related
- 2000-07-31 AT AT00950897T patent/ATE305019T1/de not_active IP Right Cessation
- 2000-07-31 BR BR0012882A patent/BR0012882A/pt not_active Application Discontinuation
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2006
- 2006-03-10 JP JP2006066801A patent/JP2006213925A/ja active Pending
Also Published As
Publication number | Publication date |
---|---|
AU770696B2 (en) | 2004-02-26 |
CN1376175A (zh) | 2002-10-23 |
KR100745875B1 (ko) | 2007-08-02 |
MX238958B (es) | 2006-07-27 |
EP1204701B1 (en) | 2005-09-21 |
WO2001009231A1 (en) | 2001-02-08 |
CA2380403A1 (en) | 2001-02-08 |
JP2003508595A (ja) | 2003-03-04 |
MXPA02001019A (es) | 2003-07-21 |
WO2001009231A9 (en) | 2002-09-06 |
AU6392700A (en) | 2001-02-19 |
US6387519B1 (en) | 2002-05-14 |
DE60022765D1 (de) | 2006-02-02 |
JP2006213925A (ja) | 2006-08-17 |
EP1204701A1 (en) | 2002-05-15 |
ES2249285T3 (es) | 2006-04-01 |
BR0012882A (pt) | 2002-04-09 |
ATE305019T1 (de) | 2005-10-15 |
DE60022765T2 (de) | 2006-06-29 |
JP4284020B2 (ja) | 2009-06-24 |
CA2380403C (en) | 2009-12-08 |
KR20020056881A (ko) | 2002-07-10 |
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