CN117916279A

CN117916279A - 组合物、树脂、膜及光传感器

组合物、树脂、膜及光传感器 Download PDF

Info

Publication number: CN117916279A
Authority: CN; China
Prior art keywords: resin; group; particles; formula; mass
Prior art date: 2021-09-29
Legal status : Pending

Application number

CN202280060166.5A

Other languages

English (en)

Chinese (zh)

Inventor

大井翔太

荒山恭平

泷下大贵

Current Assignee

Fujifilm Corp

Original Assignee

Fujifilm Corp

Priority date

2021-09-29

Filing date

2022-09-22

Publication date

2024-04-19

2022-09-22 Application filed by Fujifilm Corp filed Critical Fujifilm Corp

2024-04-19 Publication of CN117916279A publication Critical patent/CN117916279A/zh

Status Pending legal-status Critical Current

Links

229920005989 resin Polymers 0.000 title claims abstract description 404
239000011347 resin Substances 0.000 title claims abstract description 404
239000000203 mixture Substances 0.000 title claims abstract description 185
230000003287 optical effect Effects 0.000 title abstract description 14
239000002245 particle Substances 0.000 claims abstract description 256
239000000178 monomer Substances 0.000 claims abstract description 66
239000011164 primary particle Substances 0.000 claims abstract description 26
230000036961 partial effect Effects 0.000 claims abstract description 24
239000002904 solvent Substances 0.000 claims abstract description 24
239000002253 acid Substances 0.000 claims description 80
125000005647 linker group Chemical group 0.000 claims description 73
125000001424 substituent group Chemical group 0.000 claims description 60
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 56
229920000642 polymer Polymers 0.000 claims description 51
125000000217 alkyl group Chemical group 0.000 claims description 49
238000005191 phase separation Methods 0.000 claims description 40
125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 39
OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 38
125000003118 aryl group Chemical group 0.000 claims description 35
239000002270 dispersing agent Substances 0.000 claims description 30
239000011230 binding agent Substances 0.000 claims description 24
238000010438 heat treatment Methods 0.000 claims description 16
229920000728 polyester Polymers 0.000 claims description 16
239000010954 inorganic particle Substances 0.000 claims description 15
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 10
XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 8
TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims description 8
RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 claims description 6
229910001928 zirconium oxide Inorganic materials 0.000 claims description 5
TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 4
VEALVRVVWBQVSL-UHFFFAOYSA-N strontium titanate Chemical compound [Sr+2].[O-][Ti]([O-])=O VEALVRVVWBQVSL-UHFFFAOYSA-N 0.000 claims description 4
239000011787 zinc oxide Substances 0.000 claims description 4
239000005083 Zinc sulfide Substances 0.000 claims description 3
WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 3
JRPBQTZRNDNNOP-UHFFFAOYSA-N barium titanate Chemical compound [Ba+2].[Ba+2].[O-][Ti]([O-])([O-])[O-] JRPBQTZRNDNNOP-UHFFFAOYSA-N 0.000 claims description 3
229910002113 barium titanate Inorganic materials 0.000 claims description 3
239000000395 magnesium oxide Substances 0.000 claims description 3
CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 3
AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims description 3
229910052984 zinc sulfide Inorganic materials 0.000 claims description 3
DRDVZXDWVBGGMH-UHFFFAOYSA-N zinc;sulfide Chemical compound [S-2].[Zn+2] DRDVZXDWVBGGMH-UHFFFAOYSA-N 0.000 claims description 3
238000003786 synthesis reaction Methods 0.000 description 157
230000015572 biosynthetic process Effects 0.000 description 148
239000010408 film Substances 0.000 description 146
150000001875 compounds Chemical class 0.000 description 141
239000000126 substance Substances 0.000 description 109
125000004432 carbon atom Chemical group C* 0.000 description 87
-1 methacryloyl Chemical group 0.000 description 87
238000000034 method Methods 0.000 description 77
239000000047 product Substances 0.000 description 41
239000004094 surface-active agent Substances 0.000 description 40
238000002834 transmittance Methods 0.000 description 38
239000003999 initiator Substances 0.000 description 33
238000000149 argon plasma sintering Methods 0.000 description 31
239000010410 layer Substances 0.000 description 31
229910052731 fluorine Inorganic materials 0.000 description 29
239000007787 solid Substances 0.000 description 29
NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 28
125000002947 alkylene group Chemical group 0.000 description 26
239000002994 raw material Substances 0.000 description 25
150000003254 radicals Chemical class 0.000 description 24
239000011521 glass Substances 0.000 description 23
239000000243 solution Substances 0.000 description 23
YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 22
239000011737 fluorine Substances 0.000 description 22
239000003505 polymerization initiator Substances 0.000 description 21
CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 20
239000006185 dispersion Substances 0.000 description 19
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 19
238000006243 chemical reaction Methods 0.000 description 17
LLHKCFNBLRBOGN-UHFFFAOYSA-N propylene glycol methyl ether acetate Chemical compound COCC(C)OC(C)=O LLHKCFNBLRBOGN-UHFFFAOYSA-N 0.000 description 17
229920002845 Poly(methacrylic acid) Polymers 0.000 description 16
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 16
125000003545 alkoxy group Chemical group 0.000 description 16
238000000576 coating method Methods 0.000 description 16
239000003112 inhibitor Substances 0.000 description 16
230000005540 biological transmission Effects 0.000 description 15
125000004122 cyclic group Chemical group 0.000 description 15
125000002887 hydroxy group Chemical group [H]O* 0.000 description 15
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230000008569 process Effects 0.000 description 15
239000004793 Polystyrene Substances 0.000 description 14
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 14
125000001931 aliphatic group Chemical group 0.000 description 14
AOJOEFVRHOZDFN-UHFFFAOYSA-N benzyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OCC1=CC=CC=C1 AOJOEFVRHOZDFN-UHFFFAOYSA-N 0.000 description 14
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 14
239000011248 coating agent Substances 0.000 description 14
125000003700 epoxy group Chemical group 0.000 description 14
125000000623 heterocyclic group Chemical group 0.000 description 14
229910052757 nitrogen Inorganic materials 0.000 description 14
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239000006087 Silane Coupling Agent Substances 0.000 description 13
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 13
125000000524 functional group Chemical group 0.000 description 13
239000007788 liquid Substances 0.000 description 13
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 13
239000001301 oxygen Substances 0.000 description 13
229910052760 oxygen Inorganic materials 0.000 description 13
238000003860 storage Methods 0.000 description 13
239000004721 Polyphenylene oxide Substances 0.000 description 12
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238000004519 manufacturing process Methods 0.000 description 12
229920000570 polyether Polymers 0.000 description 12
125000000732 arylene group Chemical group 0.000 description 11
230000008859 change Effects 0.000 description 11
238000004040 coloring Methods 0.000 description 11
230000000694 effects Effects 0.000 description 11
230000005484 gravity Effects 0.000 description 11
239000000463 material Substances 0.000 description 11
239000003960 organic solvent Substances 0.000 description 11
NCAVPEPBIJTYSO-UHFFFAOYSA-N 4-hydroxybutyl prop-2-enoate;2-(oxiran-2-ylmethoxymethyl)oxirane Chemical compound C1OC1COCC1CO1.OCCCCOC(=O)C=C NCAVPEPBIJTYSO-UHFFFAOYSA-N 0.000 description 10
125000003647 acryloyl group Chemical group O=C([*])C([H])=C([H])[H] 0.000 description 10
125000003277 amino group Chemical group 0.000 description 10
230000018109 developmental process Effects 0.000 description 10
239000000758 substrate Substances 0.000 description 10
IRQWEODKXLDORP-UHFFFAOYSA-N 4-ethenylbenzoic acid Chemical compound OC(=O)C1=CC=C(C=C)C=C1 IRQWEODKXLDORP-UHFFFAOYSA-N 0.000 description 9
238000011161 development Methods 0.000 description 9
150000002430 hydrocarbons Chemical group 0.000 description 9
239000000049 pigment Substances 0.000 description 9
ARXJGSRGQADJSQ-UHFFFAOYSA-N 1-methoxypropan-2-ol Chemical compound COCC(C)O ARXJGSRGQADJSQ-UHFFFAOYSA-N 0.000 description 8
OZJPLYNZGCXSJM-UHFFFAOYSA-N 5-valerolactone Chemical compound O=C1CCCCO1 OZJPLYNZGCXSJM-UHFFFAOYSA-N 0.000 description 8
238000005481 NMR spectroscopy Methods 0.000 description 8
WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 8
125000004104 aryloxy group Chemical group 0.000 description 8
238000011156 evaluation Methods 0.000 description 8
238000001914 filtration Methods 0.000 description 8
125000001153 fluoro group Chemical group F* 0.000 description 8
125000005843 halogen group Chemical group 0.000 description 8
125000004433 nitrogen atom Chemical group N* 0.000 description 8
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238000006116 polymerization reaction Methods 0.000 description 8
TXBCBTDQIULDIA-UHFFFAOYSA-N 2-[[3-hydroxy-2,2-bis(hydroxymethyl)propoxy]methyl]-2-(hydroxymethyl)propane-1,3-diol Chemical compound OCC(CO)(CO)COCC(CO)(CO)CO TXBCBTDQIULDIA-UHFFFAOYSA-N 0.000 description 7
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RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical group [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 7
125000004391 aryl sulfonyl group Chemical group 0.000 description 7
125000002091 cationic group Chemical group 0.000 description 7
238000005516 engineering process Methods 0.000 description 7
125000001072 heteroaryl group Chemical group 0.000 description 7
ZQMHJBXHRFJKOT-UHFFFAOYSA-N methyl 2-[(1-methoxy-2-methyl-1-oxopropan-2-yl)diazenyl]-2-methylpropanoate Chemical compound COC(=O)C(C)(C)N=NC(C)(C)C(=O)OC ZQMHJBXHRFJKOT-UHFFFAOYSA-N 0.000 description 7
238000002156 mixing Methods 0.000 description 7
150000002989 phenols Chemical class 0.000 description 7
125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 7
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125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 6
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 6
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SJECZPVISLOESU-UHFFFAOYSA-N 3-trimethoxysilylpropan-1-amine Chemical compound CO[Si](OC)(OC)CCCN SJECZPVISLOESU-UHFFFAOYSA-N 0.000 description 3
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