CN107028803B - 包括化妆品组合物浸渍的聚氨酯泡沫的化妆品 - Google Patents

包括化妆品组合物浸渍的聚氨酯泡沫的化妆品 Download PDF

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CN107028803B
CN107028803B CN201610900009.7A CN201610900009A CN107028803B CN 107028803 B CN107028803 B CN 107028803B CN 201610900009 A CN201610900009 A CN 201610900009A CN 107028803 B CN107028803 B CN 107028803B
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金京南
崔汀善
沈珉敬
崔庚浩
崔荣镇
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Abstract

本发明提供了一种化妆品，其包括浸渍化妆品组合物的聚氨酯泡沫，其中所述聚氨酯泡沫具有网状结构。

Description

包括化妆品组合物浸渍的聚氨酯泡沫的化妆品
本申请是基于申请日为2012年3月23日、申请号为201280002267.3的中国专利申请的分案申请。
【技术领域】
本发明涉及用于浸渍化妆品组合物中的聚氨酯泡沫.
【背景技术】
在过去，化妆品组合物主要在室内使用。然而，由于最近休闲活动已经普及，并且相应地已经改变了现代生活方式，化妆品组合物已经频繁地在室外使用。特别是，在过去，UV防护化妆品组合物大多在夏季使用。然而，当现代人享受户外活动并越来越认识到紫外线的危害时，对于UV防护化妆品组合物的趋势是除夏季外还在所有季节都频繁使用。因此，更加需要方便使用和容易携带的化妆品组合物。
基于聚酯的聚氨酯泡沫偶然由德国技术专家在十九世纪四十年代后期开发，在此期间塑料材料的发展处于其中。由于所述聚氨酯泡沫基于聚酯，其也被称为酯泡沫。制备这样的聚氨酯泡沫不要求先进的技术。因此，基于聚酯的聚氨酯泡沫已经被广泛地制造，并在不同的工业领域使用，尤其是要求强拉伸力的领域。
然而，基于聚酯的聚氨酯泡沫在湿性环境下趋于容易破裂。另外，其具有微孔结构和低空气透过性，并因此显示了低柔软感觉、柔性和挠性。结果，基于聚酯的聚氨酯泡沫不适合用于浸渍化妆品组合物，尤其不适于液体化妆品组合物。在这些情况下，对于开发适合用于浸渍化妆品组合物的聚氨酯泡沫具有迫切的需要。
【公开】
【技术问题】
本公开旨在提供在浸渍化妆品组合物中使用的聚氨酯泡沫，所述聚氨酯泡沫能够保持所浸渍的化妆品组合物的高稳定性以及高浸渍后的稳定性。
【技术方案】
在一个总体方面，提供了在浸渍化妆品组合物中使用的基于聚醚的聚氨酯泡沫.
【有益效果】
本文所公开的基于聚醚的聚氨酯泡沫即使在用化妆品组合物进行浸渍后也保持高稳定性，并且改进了化妆品组合物的可携带性和手感。
【附图说明】
图1是湿性的基于聚醚的聚氨酯泡沫的微观视图；
图2所示为包装的化妆产品，其中包封有用W/O型乳液化妆组合物浸渍的聚氨酯泡沫；
图3是表2所列的聚氨酯泡沫的微观视图，每个放大10×0.3；
图4是表3所列的聚氨酯泡沫的微观视图，每个放大10×0.3；以及
图5所示是实施例1、对比例1和对比例2在50℃储存2小时后的照片。
【具体实施方式】
在一个方面，提供了在浸渍化妆品组合物中使用的基于聚醚的聚氨酯泡沫。在另一方面，基于聚醚的聚氨酯泡沫可作为载体，在该载体中承载并保留化妆品组合物。
本文中所用术语“聚氨酯泡沫”意指发泡并固化的聚氨酯树脂，也称作“发泡聚氨酯”。
在一个方面，与基于聚酯的聚氨酯泡沫相比，基于聚醚的聚氨酯泡沫更耐湿气，因此在高湿度条件下不容易破裂，并显示高稳定性。另外，与基于聚酯的聚氨酯泡沫相比，基于聚醚的聚氨酯泡沫具有更大的孔结构，从而具有改进的空气透过性、柔软感觉、柔性和挠性。再者，基于聚醚的聚氨酯泡沫需要减少的生产成本，因而比基于聚酯的聚氨酯泡沫具有更高的成本效率。
在一个方面，聚氨酯泡沫可包括干性聚氨酯泡沫或湿性聚氨酯泡沫。特别地，湿性基于聚醚的聚氨酯泡沫具有以下表1所示的性能。
[表1]
Figure GDA0001231369180000031
通常，湿性基于聚醚的聚氨酯泡沫比干性基于聚醚的聚氨酯泡沫具有更小的孔径和更致密结构。干性基于聚醚的聚氨酯泡沫具有亲油的表面性能，而作为湿发泡的结果，湿性基于聚醚的聚氨酯泡沫具有亲水表面性能。湿性基于聚醚的聚氨酯泡沫是具有均匀高孔隙率的连续微孔聚氨酯泡沫，显示高水/油可吸收性。图1是湿性基于聚醚的聚氨酯泡沫的微观视图。
在一方面，聚氨酯泡沫可具有淬硬或网状结构。另一方面，聚氨酯泡沫可具有这样的网状结构，该网状结构允许均匀且容易地用化妆品组合物浸渍，并提供高浸渍比。
一方面，聚氨酯泡沫的密度可以为1-3磅/立方英尺(pcf)，特别是1-2pcf。当聚氨酯泡沫的密度小于1pcf时，化妆品组合物可被过量释放，并且因此不方便使用。当聚氨酯泡沫的密度大于3pcf时，则不可能提供足够数量的浸渍化妆品组合物的孔，从而难以有效浸渍化妆品组合物。
一方面，聚氨酯泡沫的孔数可以为70-120孔/英寸(ppi)，特别是75-95ppi。当聚氨酯泡沫的孔数小于70ppi时，其具有差的弹性，不方便使用，也不易控制化妆品组合物的可流动性。当聚氨酯泡沫的孔数大于120ppi时，其在使用期间提供化妆品组合物以低耐久性和差的手感。
一方面，聚氨酯泡沫的ASKER硬度可以为10-70，特别是20-60，更特别是30-50，所述硬度通过由ASKER得到的DUROMETER HARDNESS TESTER(F型)测得。当聚氨酯泡沫太软使得其硬度小于10时，当其被用于包装容器中包封的化妆组合物的化妆工具如丁腈橡胶(NBR)粉扑或手所取用时，浸渍在聚氨酯泡沫中的化妆品组合物可被过量释放。当聚氨酯泡沫太硬使得其硬度大于70时，化妆品组合物可能不容易释放。
一方面，聚氨酯泡沫可以具有开孔结构。当聚氨酯泡沫具有闭合孔结构时，气泡被保持在聚氨酯中，使得低密度乳液型化妆品组合物可能不容易浸渍在其中。因此，可专门使用具有开孔结构的聚氨酯泡沫。
一方面，待浸渍在聚氨酯泡沫中的化妆品组合物包括液体化妆品组合物，特别是乳液型化妆品组合物，更特别是油包水(W/O)型或水包油(O/W)型乳液化妆品组合物。
一方面，乳液化妆品组合物可具有低粘度，特别是5000-15000厘泊(cp)，更特别是6000-10000cp。当乳液化妆品组合物的粘度低于5000cp时，其可以分开为油相和水相，从而难以用组合物均匀地浸渍聚氨酯泡沫。当乳液化妆品组合物的粘度高于15000cp时，当施用到皮肤上时，其可提供不希望的粘稠和重手感。
一方面，化妆品组合物包括皮肤护理组合物和化妆组合物。化妆品组合物的非限制性实例可以包括化妆打底霜、隔离霜、粉底、粉末、二合一粉饼、口红、润唇膏、眼影、眉笔、遮瑕产品、唇线、腮红、紫外线保护剂、露、霜或精油。更特别地，化妆品组合物可配制为化妆打底霜、化妆隔离霜、液体或固体粉底、粉末、二合一粉饼、口红、润唇膏、眼影、眉笔、遮瑕产品或腮红，但不限于此。
一方面，提供了化妆产品，其中包封了浸渍有化妆品组合物的基于聚醚的聚氨酯泡沫。所述化妆产品包括施用于本文公开的基于聚醚的聚氨酯泡沫的化妆品组合物，从而容许化妆品组合物的高质量包装。另外，所述化妆产品容许化妆品组合物长时间均一地负载在聚氨酯泡沫中，并当使用者取用该化妆品组合物时能够以足够的量释放。进一步地，所述化妆产品保持了高长期耐用性和稳定性。本文公开的化妆产品可被提供作为包装的容器，通常简写为“pact”，其通常包括下部和上部，下部中装有基于聚醚的聚氨酯泡沫，上部具有盖，该盖上可结合有镜子或类似物。图2显示了在包装容器中提供的基于聚醚的聚氨酯泡沫的示例图。
现在将描述实施例、对比例、制备例和测试例。以下实施例仅用于说明目的，并不试图限制本发明的范围。
【测试例1】聚氨酯泡沫的性能测定
为了选择适于用W/O型或O/W低粘度乳液化妆品组合物浸渍的聚氨酯泡沫，对于各种类型的聚氨酯泡沫的性能进行了测定。下表2和3显示每种类型的聚氨酯泡沫和相应性能。另外，图3和图4是每种类型的聚氨酯泡沫的微观图，放大10x 0.3。
[表2]
Figure GDA0001231369180000051
[表3]
Figure GDA0001231369180000052
Figure GDA0001231369180000061
在表3中，基于聚醚的聚氨酯泡沫1是干性基于聚醚的聚氨酯泡沫.
[测试例2]配制品稳定性的评价
在表2和表3中所列的不同种类的聚氨酯泡沫中，选择基于聚醚的聚氨酯泡沫1(实施例1)、基于聚酯的聚氨酯泡沫2(对比例1)和基于聚酯的聚氨酯泡沫3(对比例2)，并用W/O型乳液化妆组合物浸渍。然后，评价他们随温度和时间的稳定性。结果显示在下表4和图5中。图5显示了实施例1、对比例1和对比例2在它们于50℃储存2小时后的照片。
[表4]
Figure GDA0001231369180000062
从以上结果可以看出，当每种泡沫用W/O型乳液化妆组合物浸渍时，根据对比例1和2的每种聚氨酯泡沫都破损，导致化妆组合物在高温或温度严重变化下随时间分层和产生气泡，从而显示非常不稳定。相反，实施例1基本上保持了其原始状态，并显示了高稳定性。
因此，可以看出，在用化妆品组合物浸渍时，聚醚-聚氨酯泡沫比基于聚酯的聚氨酯泡沫显示了更高的稳定性，从事更适于浸渍化妆品组合物。
[制备例1和2]UV防护化妆品组合物的制备
在制备例1和2中，根据下表5的配方制备W/O型乳液UV防护化妆品组合物
特别地，UV防护剂被引入油性成分中，并在其中溶解和乳化。接下来，油性组分与表面活性剂混合，并加热到80℃，在此温度下搅动，使得混合物均匀化。然后，进一步向其中加入颜料，随后搅拌和均匀化，从而提供油性部分。在单独的混合器中，水性组分被混合，并加热到80℃，在此温度下搅动，从而提供完全溶解的水性部分。所制备的水性部分逐渐加入到油性部分中，并使用均质混合器进行乳化。在冷却到50℃后，皮肤防护成分和香料加入其中，随后冷却，从而提供低粘度W/O型乳液UV防护化妆品组合物。
[表5]
Figure GDA0001231369180000071
在表5中，二硬脂二甲铵锂蒙脱石起增稠剂的作用，聚甲基丙烯酸甲酯用作纯粹本体颜料，二氧化钛/氢氧化铝/硬脂酸用作无机UV防护剂。
【测试例3】取决于聚氨酯泡沫的硬度的优选性评价
具有不同硬度值的不同类型的基于聚醚的聚氨酯泡沫用制备例1和2浸渍，测定每个情况下的使用者优选性。特别地，将50个女性分为两组(每组25人)。使她们用NBR粉扑在两天内在皮肤上涂敷浸渍在具有不同硬度值的基于聚醚的聚氨酯泡沫中的每个制备例1和2。然后，在每种情况下评价全部使用者优选性，包括手感和涂布质量。结果显示于表6和7中。
[表6]
Figure GDA0001231369180000081
[表7]
Figure GDA0001231369180000082
由以上结果可以看出，当用于使用根据制备例1和2的组合物浸渍的基于聚醚的聚氨酯泡沫的Asker硬度值为40时，是最优选的。
本领域技术人员将知道，前述说明书中公开的概念和具体实施方案可以容易用作改变或设计其他实施方案来实现与本公开相同的目标的基础。本领域技术人员也将知道，这样的等价实施方案不会背离所附权利要求所限定的本公开的精神和范围。

Claims (3)

1.一种化妆品，其包括浸渍化妆品组合物的聚氨酯泡沫，
其中所述聚氨酯泡沫具有网状结构，
其中所述化妆品组合物是油包水(W/O)型乳液化妆品组合物，
其中所述聚氨酯泡沫具有1-3pcf的密度，
其中所述聚氨酯泡沫具有70-120孔/英寸(ppi)的孔数，
其中所述聚氨酯泡沫具有10-70的ASKER硬度，
其中所述乳液化妆品组合物的粘度为5,000-15,000cp。
2.一种化妆品，其包括浸渍化妆品组合物的聚氨酯泡沫，
其中所述聚氨酯泡沫具有开孔结构，
其中所述化妆品组合物是油包水(W/O)型乳液化妆品组合物，
其中所述聚氨酯泡沫具有1-3pcf的密度，
其中所述聚氨酯泡沫具有70-120孔/英寸(ppi)的孔数，
其中所述聚氨酯泡沫具有10-70的ASKER硬度，
其中所述乳液化妆品组合物的粘度为5,000-15,000cp。
3.根据权利要求1或2所述的化妆品，其包括浸渍化妆品组合物的聚氨酯泡沫，
其中所述化妆品组合物被提供用作化妆打底霜、隔离霜、粉底、粉末、二合一粉饼、口红、润唇膏、眼影、眉笔、遮瑕产品或腮红。
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