CN100448838C - 结晶形态的酚类抗氧化剂 - Google Patents

结晶形态的酚类抗氧化剂 Download PDF

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Publication number
CN100448838C
CN100448838C CNB2003801041780A CN200380104178A CN100448838C CN 100448838 C CN100448838 C CN 100448838C CN B2003801041780 A CNB2003801041780 A CN B2003801041780A CN 200380104178 A CN200380104178 A CN 200380104178A CN 100448838 C CN100448838 C CN 100448838C
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CN
China
Prior art keywords
weak
moderate
tert
butyl
strong
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Expired - Fee Related
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CNB2003801041780A
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English (en)
Chinese (zh)
Other versions
CN1717385A (zh
Inventor
D·雷姆
J·谢夫特
P·A·范德沙夫
C·古克尔
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BASF Schweiz AG
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Ciba Spezialitaetenchemie Holding AG
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Publication of CN1717385A publication Critical patent/CN1717385A/zh
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Publication of CN100448838C publication Critical patent/CN100448838C/zh
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/22—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/22—Separation; Purification; Stabilisation; Use of additives
    • C07C231/24—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/66—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety
    • C07C69/73—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety of unsaturated acids
    • C07C69/732—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety of unsaturated acids of unsaturated hydroxy carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/04—Oxygen-containing compounds
    • C08K5/13—Phenols; Phenolates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/16—Nitrogen-containing compounds
    • C08K5/20—Carboxylic acid amides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/002—Physical properties
    • C08K2201/005—Additives being defined by their particle size in general

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Anti-Oxidant Or Stabilizer Compositions (AREA)
CNB2003801041780A 2002-11-26 2003-11-17 结晶形态的酚类抗氧化剂 Expired - Fee Related CN100448838C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP02406023.8 2002-11-26
EP02406023 2002-11-26

Publications (2)

Publication Number Publication Date
CN1717385A CN1717385A (zh) 2006-01-04
CN100448838C true CN100448838C (zh) 2009-01-07

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ID=32338231

Family Applications (1)

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CNB2003801041780A Expired - Fee Related CN100448838C (zh) 2002-11-26 2003-11-17 结晶形态的酚类抗氧化剂

Country Status (11)

Country Link
US (1) US7262319B2 (cg-RX-API-DMAC7.html)
EP (1) EP1575895A1 (cg-RX-API-DMAC7.html)
JP (1) JP2006507337A (cg-RX-API-DMAC7.html)
KR (1) KR20050085019A (cg-RX-API-DMAC7.html)
CN (1) CN100448838C (cg-RX-API-DMAC7.html)
AU (1) AU2003300566B2 (cg-RX-API-DMAC7.html)
BR (1) BR0316567A (cg-RX-API-DMAC7.html)
MY (1) MY136146A (cg-RX-API-DMAC7.html)
RU (1) RU2362764C2 (cg-RX-API-DMAC7.html)
TW (1) TWI308145B (cg-RX-API-DMAC7.html)
WO (1) WO2004048312A1 (cg-RX-API-DMAC7.html)

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WO2006014605A2 (en) * 2004-07-23 2006-02-09 Polnox Corporation Anti-oxidant macromonomers and polymers and methods of making and using the same
KR101189589B1 (ko) 2004-07-27 2012-10-12 시바 홀딩 인코포레이티드 페놀 산화방지제의 고형 입자의 제조 방법
WO2006060800A1 (en) 2004-12-03 2006-06-08 Polnox Corporation Synthesis of aniline and phenol-based antioxidant macromonomers and corresponding polymers
WO2006091705A2 (en) 2005-02-22 2006-08-31 Polnox Corporation Nitrogen and hindered phenol containing dual functional macromolecular antioxidants: synthesis , performances and applications
WO2006104957A2 (en) 2005-03-25 2006-10-05 Polnox Corporation Alkylated and polymeric macromolecular antioxidants and methods of making and using the same
US7705176B2 (en) 2005-10-27 2010-04-27 Polnox Corporation Macromolecular antioxidants based on sterically hindered phenols and phosphites
EP1966293A1 (en) 2005-10-27 2008-09-10 Polnox Corporation Stabilized polyolefin compositions
WO2007064843A1 (en) 2005-12-02 2007-06-07 Polnox Corporation Lubricant oil compositions
WO2008005358A2 (en) 2006-07-06 2008-01-10 Polnox Corporation Novel macromolecular antioxidants comprising differing antioxidant moieties: structures, methods of making and using the same
US7767853B2 (en) 2006-10-20 2010-08-03 Polnox Corporation Antioxidants and methods of making and using the same
WO2008055832A2 (en) * 2006-11-09 2008-05-15 Ciba Holding Inc. Process using liquid phenolic antioxidants
KR101211231B1 (ko) * 2008-08-21 2012-12-11 주식회사 엘지화학 산화방지제 유성 분산액과 이의 제조방법 및 이로부터 제조된 염화비닐계 수지 중합체
JP5330904B2 (ja) * 2009-06-12 2013-10-30 住友化学株式会社 粒状物質の製造方法
RU2602066C2 (ru) * 2011-03-14 2016-11-10 ДАУ ГЛОБАЛ ТЕКНОЛОДЖИЗ ЭлЭлСи Композиции на основе этилена
JP5542289B2 (ja) * 2012-01-23 2014-07-09 トヨタ自動車株式会社 オイル添加物およびオイルフィルター
EP3071544B1 (en) 2013-11-22 2022-07-06 Polnox Corporation Macromolecular antioxidants based on dual type moiety per molecule: structures methods of making and using the same
US20180251695A1 (en) 2017-03-01 2018-09-06 Polnox Corporation Macromolecular Corrosion (McIn) Inhibitors: Structures, Methods Of Making And Using The Same
WO2018189016A1 (en) 2017-04-10 2018-10-18 Basf Se Low volatile organic anti-oxidation stabilisers for polymeric systems, their production and use
CN107417528A (zh) * 2017-05-02 2017-12-01 沈阳化工大学 一种抗氧剂1076在甲醇溶剂中得到针状晶形结晶的方法
CN111495312B (zh) * 2020-05-22 2023-07-28 河南心连心化学工业集团股份有限公司 一种草酰胺合成装置以及合成方法
KR102771644B1 (ko) * 2022-06-21 2025-02-26 금호석유화학 주식회사 산화방지제의 제조방법

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US3867414A (en) * 1969-12-04 1975-02-18 Yamanouchi Pharma Co Ltd Process for the preparation of suspensions of microcrystals of chloramphenicol palmitate
US4547585A (en) * 1981-05-28 1985-10-15 Mitsui Petrochemical Industries, Ltd. Process for preparing tetrakis [3-(3,5-dibutyl-4-hydroxyphenyl)propionyloxymethyl] methane
US4683326A (en) * 1985-07-19 1987-07-28 Ciba-Geigy Corporation Solvent-free crystallization of pentaerythritol tetrakis-[3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate] and the novel alpha-crystalline form thereof
US4708979A (en) * 1985-05-02 1987-11-24 Ciba-Geigy Corporation Process for the stabilization of spherically polymerized polyolefins
EP0498620A1 (en) * 1991-02-04 1992-08-12 Polyplastics Co. Ltd. Colored polyacetal resin composition
EP0562856A2 (en) * 1992-03-26 1993-09-29 Polyplastics Co. Ltd. Polyoxymethylene composition
EP0563906A1 (en) * 1992-03-31 1993-10-06 Union Carbide Chemicals & Plastics Technology Corporation Dispersions of polymer additives in fatty acid esters

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US3644482A (en) 1961-10-30 1972-02-22 Geigy Ag J R (4-hydroxy-5-alkylphenyl) alkanoic acid esters of polyols
US3666809A (en) 1969-10-08 1972-05-30 Mitsubishi Chem Ind Method for the production of acrylamide crystals
AT303971B (de) 1969-12-04 1972-12-27 Yamanouchi Pharma Co Ltd Verfahren zur Herstellung einer Suspension von Chloramphenicol-palmitat in mikrokristalliner Form
JPS6013018B2 (ja) * 1980-04-01 1985-04-04 三井化学株式会社 新規な結晶構造を有するテトラキス〔３−（３，５−ジ−ｔ−ブチル−４−ヒドロキシフエニル）プロピオニルオキシメチル〕メタン
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3543293A (en) * 1966-01-10 1970-11-24 Sankyo Co Method for the production of microcrystallines of chloramphenicol
US3867414A (en) * 1969-12-04 1975-02-18 Yamanouchi Pharma Co Ltd Process for the preparation of suspensions of microcrystals of chloramphenicol palmitate
US4547585A (en) * 1981-05-28 1985-10-15 Mitsui Petrochemical Industries, Ltd. Process for preparing tetrakis [3-(3,5-dibutyl-4-hydroxyphenyl)propionyloxymethyl] methane
US4708979A (en) * 1985-05-02 1987-11-24 Ciba-Geigy Corporation Process for the stabilization of spherically polymerized polyolefins
US4683326A (en) * 1985-07-19 1987-07-28 Ciba-Geigy Corporation Solvent-free crystallization of pentaerythritol tetrakis-[3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate] and the novel alpha-crystalline form thereof
EP0498620A1 (en) * 1991-02-04 1992-08-12 Polyplastics Co. Ltd. Colored polyacetal resin composition
EP0562856A2 (en) * 1992-03-26 1993-09-29 Polyplastics Co. Ltd. Polyoxymethylene composition
EP0563906A1 (en) * 1992-03-31 1993-10-06 Union Carbide Chemicals & Plastics Technology Corporation Dispersions of polymer additives in fatty acid esters

Also Published As

Publication number Publication date
EP1575895A1 (en) 2005-09-21
US7262319B2 (en) 2007-08-28
KR20050085019A (ko) 2005-08-29
TW200415234A (en) 2004-08-16
AU2003300566B2 (en) 2010-01-21
US20060189820A1 (en) 2006-08-24
BR0316567A (pt) 2005-10-04
CN1717385A (zh) 2006-01-04
WO2004048312A1 (en) 2004-06-10
RU2005120164A (ru) 2006-04-27
AU2003300566A1 (en) 2004-06-18
RU2362764C2 (ru) 2009-07-27
TWI308145B (en) 2009-04-01
JP2006507337A (ja) 2006-03-02
MY136146A (en) 2008-08-29

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