CN100439320C - 用于制备二嗪的中间体 - Google Patents

用于制备二嗪的中间体 Download PDF

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Publication number
CN100439320C
CN100439320C CNB031579167A CN03157916A CN100439320C CN 100439320 C CN100439320 C CN 100439320C CN B031579167 A CNB031579167 A CN B031579167A CN 03157916 A CN03157916 A CN 03157916A CN 100439320 C CN100439320 C CN 100439320C
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CN
China
Prior art keywords
compound
milliliters
gram
mixture
reaction
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Expired - Lifetime
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CNB031579167A
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English (en)
Chinese (zh)
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CN1607200A (zh
Inventor
G·D·安尼斯
S·F·麦坎
R·沙皮罗
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EIDP Inc
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EI Du Pont de Nemours and Co
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Publication of CN1607200A publication Critical patent/CN1607200A/zh
Application granted granted Critical
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D273/00—Heterocyclic compounds containing rings having nitrogen and oxygen atoms as the only ring hetero atoms, not provided for by groups C07D261/00 - C07D271/00
    • C07D273/02—Heterocyclic compounds containing rings having nitrogen and oxygen atoms as the only ring hetero atoms, not provided for by groups C07D261/00 - C07D271/00 having two nitrogen atoms and only one oxygen atom
    • C07D273/04—Six-membered rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C271/00—Derivatives of carbamic acids, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups
    • C07C271/62—Compounds containing any of the groups, X being a hetero atom, Y being any atom, e.g. N-acylcarbamates
    • C07C271/66—Y being a hetero atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C281/00—Derivatives of carbonic acid containing functional groups covered by groups C07C269/00 - C07C279/00 in which at least one nitrogen atom of these functional groups is further bound to another nitrogen atom not being part of a nitro or nitroso group
    • C07C281/02—Compounds containing any of the groups, e.g. carbazates
    • C07C281/04—Compounds containing any of the groups, e.g. carbazates the other nitrogen atom being further doubly-bound to a carbon atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C63/00—Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
    • C07C63/68—Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings containing halogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C65/00—Compounds having carboxyl groups bound to carbon atoms of six—membered aromatic rings and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
    • C07C65/21—Compounds having carboxyl groups bound to carbon atoms of six—membered aromatic rings and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups containing ether groups, groups, groups, or groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/74—Esters of carboxylic acids having an esterified carboxyl group bound to a carbon atom of a ring other than a six-membered aromatic ring
    • C07C69/757—Esters of carboxylic acids having an esterified carboxyl group bound to a carbon atom of a ring other than a six-membered aromatic ring having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
    • C07C69/84—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring of monocyclic hydroxy carboxylic acids, the hydroxy groups and the carboxyl groups of which are bound to carbon atoms of a six-membered aromatic ring
    • C07C69/92—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring of monocyclic hydroxy carboxylic acids, the hydroxy groups and the carboxyl groups of which are bound to carbon atoms of a six-membered aromatic ring with etherified hydroxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/07—Optical isomers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2602/00—Systems containing two condensed rings
    • C07C2602/02—Systems containing two condensed rings the rings having only two atoms in common
    • C07C2602/04—One of the condensed rings being a six-membered aromatic ring
    • C07C2602/08—One of the condensed rings being a six-membered aromatic ring the other ring being five-membered, e.g. indane

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
CNB031579167A 1994-04-20 1995-04-17 用于制备二嗪的中间体 Expired - Lifetime CN100439320C (zh)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US23056894A 1994-04-20 1994-04-20
US08/230568 1994-04-20
US29890994A 1994-08-31 1994-08-31
US08/298909 1994-08-31

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
CNB001036327A Division CN1142922C (zh) 1994-04-20 1995-04-17 用于制备噁二嗪的中间体及其制法

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN2006101006848A Division CN101007763B (zh) 1994-04-20 1995-04-17 用于制备噁二嗪的中间体

Publications (2)

Publication Number Publication Date
CN1607200A CN1607200A (zh) 2005-04-20
CN100439320C true CN100439320C (zh) 2008-12-03

Family

ID=26924355

Family Applications (3)

Application Number Title Priority Date Filing Date
CN95192654A Expired - Lifetime CN1059901C (zh) 1994-04-20 1995-04-17 杀节肢动物的二嗪的制备
CNB031579167A Expired - Lifetime CN100439320C (zh) 1994-04-20 1995-04-17 用于制备二嗪的中间体
CNB001036327A Expired - Lifetime CN1142922C (zh) 1994-04-20 1995-04-17 用于制备噁二嗪的中间体及其制法

Family Applications Before (1)

Application Number Title Priority Date Filing Date
CN95192654A Expired - Lifetime CN1059901C (zh) 1994-04-20 1995-04-17 杀节肢动物的二嗪的制备

Family Applications After (1)

Application Number Title Priority Date Filing Date
CNB001036327A Expired - Lifetime CN1142922C (zh) 1994-04-20 1995-04-17 用于制备噁二嗪的中间体及其制法

Country Status (21)

Country Link
US (1) US5869657A (de)
EP (5) EP1048647A1 (de)
JP (2) JP3882195B2 (de)
KR (1) KR100249448B1 (de)
CN (3) CN1059901C (de)
AT (3) ATE214380T1 (de)
AU (2) AU687547B2 (de)
BR (1) BR9507845A (de)
CA (3) CA2582172C (de)
CZ (1) CZ306096A3 (de)
DE (4) DE69535654T2 (de)
ES (4) ES2248663T3 (de)
HU (2) HU221609B (de)
IL (3) IL113412A (de)
MX (1) MX209131B (de)
NZ (1) NZ283961A (de)
PL (1) PL316849A1 (de)
PT (3) PT756594E (de)
RU (1) RU2138489C1 (de)
TW (1) TW477790B (de)
WO (1) WO1995029171A1 (de)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103033573A (zh) * 2012-12-13 2013-04-10 黄河三角洲京博化工研究院有限公司 一种n-氯甲酰基-n-[4-(三氟甲氧基)苯基]氨基甲酸甲酯含量分析方法
CN105111164A (zh) * 2013-10-11 2015-12-02 浙江大学 精茚虫威的晶型

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* Cited by examiner, † Cited by third party
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CN101391953B (zh) * 1994-04-20 2012-06-06 纳幕尔杜邦公司 用于制备*二嗪的中间体
BR9708025A (pt) * 1996-03-15 1999-07-27 Du Pont Mistura inseticida composição inseticida e método para controlar insetos
USH1950H1 (en) * 1996-08-05 2001-03-06 E. I. Du Pont De Nemours And Company Processes for preparing indeno[1,2-E][1,3,4]oxadiazine-dicarboxylates
DE19736921A1 (de) 1997-08-25 1999-03-04 Bayer Ag Verfahren zur Herstellung von 2-Cyanoindan-1-onen
AU4553999A (en) * 1998-06-10 1999-12-30 E.I. Du Pont De Nemours And Company Arthropodicidal carboxanilides
DE19837069C1 (de) * 1998-08-17 2000-01-05 Bayer Ag Substituierte Zimtsäuren und Zimtsäureester, Verfahren zu ihrer Herstellung und ihre Verwendung zur Herstellung von substituierten Indanoncarbonsäureestern
US6956129B2 (en) * 2001-02-16 2005-10-18 Bayer Aktiengesellschaft Polyhalogen-substituted cinnamic acids and cinnamic acid derivatives and a process for the preparation of polyhalogen-substituted cinnamic acids and cinnamic acid derivatives
US7414157B2 (en) 2001-06-29 2008-08-19 E. I. Du Pont De Nemours And Company Hydroxylation of β-dicarbonyls with zirconium catalysts
WO2003040083A1 (en) * 2001-11-07 2003-05-15 E.I. Du Pont De Nemours And Company Enantioselective hydroxylation of beta-dicarbonyls catalyzed by cinchona alkaloid derivatives
US6916946B2 (en) 2003-08-20 2005-07-12 Daicel Chemical Industries, Ltd. Acid halide derivatives, their production, and production of indanonecarboxylic acid esters using the same
JP2005170803A (ja) 2003-12-08 2005-06-30 Daicel Chem Ind Ltd 新規なマロン酸モノメチル誘導体とその製造法
IN241255B (de) * 2005-05-02 2010-06-25
ES2823760T3 (es) 2006-09-01 2021-05-10 Fmc Corp Formulaciones para administración tópica local que contienen indoxacarb
CN101503358B (zh) * 2009-03-10 2012-01-25 大连理工大学 高乌甲素作为催化剂制备手性α-羟基-β-二羰基化合物的方法
JP2011246436A (ja) 2010-04-28 2011-12-08 Sumitomo Chemical Co Ltd 有害生物防除組成物
CN102391261A (zh) * 2011-10-14 2012-03-28 上海交通大学 一种n-取代噁二嗪类化合物及其制备方法和应用
CN103371168B (zh) * 2012-04-28 2017-02-22 马国丰 一种高效杀虫剂组合物
CN104262285B (zh) * 2014-07-24 2016-08-17 浙江大学 农用杀虫剂茚虫威中间体的合成法
CN104193696A (zh) * 2014-08-26 2014-12-10 常州大学 一种新型杀虫剂茚虫威的制备方法
CN104230838B (zh) * 2014-09-11 2016-03-30 浙江大学 农用杀虫剂茚虫威高纯度关键中间体的制备方法
CN104311502B (zh) * 2014-09-15 2016-08-24 南通施壮化工有限公司 从茚虫威混合体中分离提纯s体茚虫威的方法
CN106928062B (zh) * 2015-12-31 2020-05-12 江苏扬农化工股份有限公司 一种α-羟基-β-二羰基化合物手性富集的方法
CN106106504A (zh) * 2016-06-27 2016-11-16 江苏新农化工有限公司 含甲基毒死蜱的杀虫组合物及其制剂和应用
CN106397351B (zh) * 2016-08-31 2018-10-30 京博农化科技股份有限公司 一种茚虫威中间体的制备方法
CN107043360B (zh) * 2017-03-22 2019-07-12 京博农化科技股份有限公司 一种茚虫威杀虫剂的制备方法
CN107915692A (zh) * 2017-10-30 2018-04-17 安徽富田农化有限公司 一种茚虫威的制备方法
CN108586292A (zh) * 2018-01-24 2018-09-28 湖南国发精细化工科技有限公司 N-氯甲酰基-n-[(4-三氟甲氧基)苯基]氨基甲酸甲酯的精制方法
CN108997254A (zh) * 2018-08-27 2018-12-14 湖南国发精细化工科技有限公司 茚并噁二嗪化合物的合成方法
CN109704994A (zh) * 2018-12-26 2019-05-03 山东华阳农药化工集团有限公司 一种合成茚虫威中间体氯甲酰基[4-(三氟甲氧基)苯基]氨基甲酸甲酯的改进方法
CN109651288A (zh) * 2018-12-29 2019-04-19 京博农化科技有限公司 一种茚虫威中间体的制备方法
WO2022200364A1 (en) 2021-03-25 2022-09-29 Syngenta Crop Protection Ag Insect, acarina and nematode pest control
EP4337016A1 (de) 2021-05-14 2024-03-20 Syngenta Crop Protection AG Zusammensetzungen zur saatgutbehandlung
JP2024516912A (ja) 2021-05-14 2024-04-17 シンジェンタ クロップ プロテクション アクチェンゲゼルシャフト 昆虫、ダニ目及び線虫有害生物の防除
WO2022268813A1 (en) 2021-06-24 2022-12-29 Syngenta Crop Protection Ag Insect, acarina and nematode pest control
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CN117940402A (zh) 2021-07-13 2024-04-26 安道麦马克西姆有限公司 制备杀节肢动物的噁二嗪中间体的方法
WO2023105065A1 (en) 2021-12-10 2023-06-15 Syngenta Crop Protection Ag Insect, acarina and nematode pest control
WO2023105064A1 (en) 2021-12-10 2023-06-15 Syngenta Crop Protection Ag Insect, acarina and nematode pest control
WO2023131943A1 (en) 2022-01-04 2023-07-13 Adama Makhteshim Ltd. Process of preparation of indoxacarb and its intermediates
WO2023148735A1 (en) 2022-02-02 2023-08-10 Adama Makhteshim Ltd. Novel solid state forms of indoxacarb

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WO1992011249A1 (en) * 1990-12-21 1992-07-09 E.I. Du Pont De Nemours And Company Arthropodicidal carboxanilides

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103033573A (zh) * 2012-12-13 2013-04-10 黄河三角洲京博化工研究院有限公司 一种n-氯甲酰基-n-[4-(三氟甲氧基)苯基]氨基甲酸甲酯含量分析方法
CN103033573B (zh) * 2012-12-13 2014-05-21 黄河三角洲京博化工研究院有限公司 一种n-氯甲酰基-n-[4-(三氟甲氧基)苯基]氨基甲酸甲酯含量分析方法
CN105111164A (zh) * 2013-10-11 2015-12-02 浙江大学 精茚虫威的晶型

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ES2171537T3 (es) 2002-09-16
DE69535630T2 (de) 2008-08-28
EP1623980A1 (de) 2006-02-08
EP1357107A1 (de) 2003-10-29
CA2582172C (en) 2008-07-08
EP1598332A3 (de) 2005-12-21
TW477790B (en) 2002-03-01
CN1059901C (zh) 2000-12-27
ATE214380T1 (de) 2002-03-15
PT1598332E (pt) 2008-01-11
EP1048647A1 (de) 2000-11-02
KR100249448B1 (ko) 2000-04-01
CA2188400C (en) 2006-08-01
PL316849A1 (en) 1997-02-17
EP1623980B1 (de) 2007-11-21
EP1598332A2 (de) 2005-11-23
PT756594E (pt) 2002-06-28
EP0756594A1 (de) 1997-02-05
CN1282739A (zh) 2001-02-07
DE69535654D1 (de) 2008-01-03
IL155210A (en) 2010-06-30
ATE303983T1 (de) 2005-09-15
EP1357107B1 (de) 2005-09-07
IL113412A0 (en) 1995-07-31
CN1607200A (zh) 2005-04-20
CA2546165C (en) 2007-12-11
HU221609B (hu) 2002-11-28
AU2243295A (en) 1995-11-16
CN1146205A (zh) 1997-03-26
AU714304B2 (en) 1999-12-23
HUT75052A (en) 1997-03-28
HU9801346D0 (en) 1998-08-28
ATE376541T1 (de) 2007-11-15
CA2546165A1 (en) 1995-11-02
CN1142922C (zh) 2004-03-24
EP0756594B1 (de) 2002-03-13
DE69534440D1 (de) 2005-10-13
CA2188400A1 (en) 1995-11-02
JP3882195B2 (ja) 2007-02-14
HU214902B (hu) 1998-07-28
DE69535654T2 (de) 2008-10-30
JP4263200B2 (ja) 2009-05-13
AU687547B2 (en) 1998-02-26
DE69535630D1 (de) 2007-12-06
CA2582172A1 (en) 1995-11-02
NZ283961A (en) 1997-11-24
US5869657A (en) 1999-02-09
MX209131B (es) 2002-07-23
ES2296010T3 (es) 2008-04-16
CZ306096A3 (en) 1997-03-12
AU5216898A (en) 1998-04-23
JP2006273867A (ja) 2006-10-12
BR9507845A (pt) 1997-09-23
RU2138489C1 (ru) 1999-09-27
PT1623980E (pt) 2008-02-12
ES2297591T3 (es) 2008-05-01
JPH09512533A (ja) 1997-12-16
EP1598332B1 (de) 2007-10-24
ES2248663T3 (es) 2006-03-16
IL113412A (en) 2003-10-31
HU9602885D0 (en) 1996-12-30
IL155210A0 (en) 2003-11-23
WO1995029171A1 (en) 1995-11-02
DE69525840T2 (de) 2002-10-02
MX9604881A (es) 1998-01-31
DE69534440T2 (de) 2006-07-13
DE69525840D1 (de) 2002-04-18

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