WO2009115506A2 - Nanoparticules métalliques stabilisées avec des polyéthylène imines ou des polyvinyle amines dérivées - Google Patents

Nanoparticules métalliques stabilisées avec des polyéthylène imines ou des polyvinyle amines dérivées Download PDF

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Publication number
WO2009115506A2
WO2009115506A2 PCT/EP2009/053114 EP2009053114W WO2009115506A2 WO 2009115506 A2 WO2009115506 A2 WO 2009115506A2 EP 2009053114 W EP2009053114 W EP 2009053114W WO 2009115506 A2 WO2009115506 A2 WO 2009115506A2
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WO
WIPO (PCT)
Prior art keywords
reaction
silver
acid
polyvinylamines
solution
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PCT/EP2009/053114
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German (de)
English (en)
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WO2009115506A3 (fr
Inventor
Gerrit Luinstra
Wolfgang Schrof
Udo Goedert
Robert Feuerhake
Tobias Joachim Koplin
Imme Domke
Original Assignee
Basf Se
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Publication date
Application filed by Basf Se filed Critical Basf Se
Priority to CN2009801180013A priority Critical patent/CN102036773A/zh
Priority to JP2011500188A priority patent/JP2011517728A/ja
Priority to EP09722099A priority patent/EP2274123A2/fr
Priority to US12/933,397 priority patent/US20110020170A1/en
Publication of WO2009115506A2 publication Critical patent/WO2009115506A2/fr
Publication of WO2009115506A3 publication Critical patent/WO2009115506A3/fr

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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/62—Metallic pigments or fillers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05—Metallic powder characterised by the size or surface area of the particles
    • B22F1/054—Nanosized particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/10—Metallic powder containing lubricating or binding agents; Metallic powder containing organic material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G29/00—Compounds of bismuth
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G3/00—Compounds of copper
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G5/00—Compounds of silver
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G55/00—Compounds of ruthenium, rhodium, palladium, osmium, iridium, or platinum
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G7/00—Compounds of gold
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G9/00—Compounds of zinc
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/01—Crystal-structural characteristics depicted by a TEM-image
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/84—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by UV- or VIS- data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties

Abstract

L’invention concerne des nanoparticules métalliques et leur procédé de fabrication dans lequel une solution de sels métalliques est réduite en présence de la polyéthylène imine ou de la polyvinyle amine dérivée avec un agent de réduction. Des solutions de sels métalliques de deux ou plusieurs métaux différents peuvent être réduites simultanément ou successivement, des nanoparticules métalliques étant obtenues à partir de deux ou plusieurs métaux différents. Les métaux préférés sont l’argent, le palladium et le platine. Des agents de réduction appropriés sont par exemple l’acide formique, le formaldéhyde, la diéthanolamine, l’acide pentène-5-oïque et le borohydrure de sodium. L’argent peut être utilisé sous la forme d’oxyde d’argent et/ou de nitrate d’argent, le palladium sous la forme de tétrachloropalladate de métal alcalin ou de nitrate de palladium (ll) et le platine sous la forme de tétrachloroplatinate de métal alcalin ou de nitrate de tétraamino-platine (ll).
PCT/EP2009/053114 2008-03-19 2009-03-17 Nanoparticules métalliques stabilisées avec des polyéthylène imines ou des polyvinyle amines dérivées WO2009115506A2 (fr)

Priority Applications (4)

Application Number Priority Date Filing Date Title
CN2009801180013A CN102036773A (zh) 2008-03-19 2009-03-17 经衍生的聚乙烯亚胺或聚乙烯胺稳定的金属纳米颗粒
JP2011500188A JP2011517728A (ja) 2008-03-19 2009-03-17 誘導体化されたポリエチレンイミン又はポリビニルアミンで安定化された金属ナノ粒子
EP09722099A EP2274123A2 (fr) 2008-03-19 2009-03-17 Nanoparticules métalliques stabilisées avec des polyéthylène imines ou des polyvinyle amines dérivées
US12/933,397 US20110020170A1 (en) 2008-03-19 2009-03-17 Metal nanoparticles stabilized with derivatized polyethyleneimines or polyvinylamines

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP08152996.8 2008-03-19
EP08152996 2008-03-19

Publications (2)

Publication Number Publication Date
WO2009115506A2 true WO2009115506A2 (fr) 2009-09-24
WO2009115506A3 WO2009115506A3 (fr) 2010-05-06

Family

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PCT/EP2009/053114 WO2009115506A2 (fr) 2008-03-19 2009-03-17 Nanoparticules métalliques stabilisées avec des polyéthylène imines ou des polyvinyle amines dérivées

Country Status (5)

Country Link
US (1) US20110020170A1 (fr)
EP (1) EP2274123A2 (fr)
JP (1) JP2011517728A (fr)
CN (1) CN102036773A (fr)
WO (1) WO2009115506A2 (fr)

Cited By (9)

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WO2011073120A1 (fr) 2009-12-17 2011-06-23 Basf Se Matériau de support d'oxyde de métal contenant des particules métalliques du groupe fer-platine à l'échelle nanométrique
JP2011153362A (ja) * 2010-01-28 2011-08-11 Harima Chemicals Inc 銀ナノ粒子の製造方法
JP2011168806A (ja) * 2010-02-16 2011-09-01 Shinko Kagaku Kogyosho:Kk 金属ナノ粒子およびその製造方法
DE102011082332A1 (de) 2010-09-15 2012-03-15 Basf Se Heterogenkatalysator
DE102011085903A1 (de) 2010-11-19 2012-05-24 Basf Se Festkörper, insbesondere Katalysator
DE102011083510A1 (de) 2010-09-28 2012-05-24 Basf Se Verfahren zur Herstellung einer Hülle auf einem Templat mittels Versprühen reaktiver Ausgangsstoffe
CN101829563B (zh) * 2010-05-14 2012-07-04 中国科学技术大学 乙烯还原制备纳米钯催化剂的方法
JP2014198908A (ja) * 2014-06-09 2014-10-23 株式会社新光化学工業所 金属ナノ粒子およびその製造方法
WO2016062880A3 (fr) * 2014-10-24 2016-06-16 Basf Se Polymères non ampholytes quaternarisables hydrosolubles pour modifier la charge superficielle de particules solides

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EP2305402B1 (fr) * 2008-06-26 2017-11-29 DIC Corporation Procédé de production de poudre contenant de l'argent et pâte conductrice l utilisant
TWI403373B (zh) * 2009-07-16 2013-08-01 Univ Nat Taiwan 應用乙醇胺以製造奈米銀粒子之方法
FR2971167B1 (fr) * 2011-02-03 2013-03-15 Commissariat Energie Atomique Procede de separation d'au moins un element platinoide d'une solution aqueuse acide comprenant, outre cet element platinoide, un ou plusieurs autres elements chimiques
CN102179525B (zh) * 2011-04-15 2013-05-08 北京航空航天大学 一种室温条件制备镍铂双层纳米碗的可控合成方法
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KR101316298B1 (ko) * 2011-09-05 2013-10-08 숭실대학교산학협력단 수불용성 할로겐화은으로부터 은나노 콜로이드 제조방법
WO2013063161A2 (fr) * 2011-10-25 2013-05-02 Lockheed Martin Corporation Procédés dont l'échelle peut être agrandie pour la formation de nanoparticules d'étain, compositions contenant des nanoparticules d'étain et applications les utilisant
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KR20140097981A (ko) * 2013-01-29 2014-08-07 주식회사 엘지화학 태양전지용 금속 나노 입자의 제조 방법, 그 금속 나노 입자를 포함하는 잉크 조성물 및 이를 사용한 박막의 제조 방법
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Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011073120A1 (fr) 2009-12-17 2011-06-23 Basf Se Matériau de support d'oxyde de métal contenant des particules métalliques du groupe fer-platine à l'échelle nanométrique
US8574520B2 (en) 2009-12-17 2013-11-05 BASF SE Ludwigshafen Metal oxide support material containing nanoscaled iron platinum group metal
JP2011153362A (ja) * 2010-01-28 2011-08-11 Harima Chemicals Inc 銀ナノ粒子の製造方法
JP2011168806A (ja) * 2010-02-16 2011-09-01 Shinko Kagaku Kogyosho:Kk 金属ナノ粒子およびその製造方法
CN101829563B (zh) * 2010-05-14 2012-07-04 中国科学技术大学 乙烯还原制备纳米钯催化剂的方法
DE102011082332A1 (de) 2010-09-15 2012-03-15 Basf Se Heterogenkatalysator
DE102011083510A1 (de) 2010-09-28 2012-05-24 Basf Se Verfahren zur Herstellung einer Hülle auf einem Templat mittels Versprühen reaktiver Ausgangsstoffe
DE102011085903A1 (de) 2010-11-19 2012-05-24 Basf Se Festkörper, insbesondere Katalysator
JP2014198908A (ja) * 2014-06-09 2014-10-23 株式会社新光化学工業所 金属ナノ粒子およびその製造方法
WO2016062880A3 (fr) * 2014-10-24 2016-06-16 Basf Se Polymères non ampholytes quaternarisables hydrosolubles pour modifier la charge superficielle de particules solides
US10899932B2 (en) 2014-10-24 2021-01-26 Basf Se Non-amphoteric, quaternisable and water-soluble polymers for modifying the surface charge of solid particles

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JP2011517728A (ja) 2011-06-16
CN102036773A (zh) 2011-04-27
US20110020170A1 (en) 2011-01-27
WO2009115506A3 (fr) 2010-05-06
EP2274123A2 (fr) 2011-01-19

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