KR960703146A - 실록산 개질된 폴리올레핀 공중합체(siloxane modified polyolefin copolymers) - Google Patents

실록산 개질된 폴리올레핀 공중합체(siloxane modified polyolefin copolymers) Download PDF

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KR960703146A
KR960703146A KR1019950705885A KR19950705885A KR960703146A KR 960703146 A KR960703146 A KR 960703146A KR 1019950705885 A KR1019950705885 A KR 1019950705885A KR 19950705885 A KR19950705885 A KR 19950705885A KR 960703146 A KR960703146 A KR 960703146A
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polyolefin
alkyl
alkylphenyl
phenyl
siloxane modified
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스티븐 대릴 스미쓰
앤드류 줄리안 누크
마가렛 수 거버
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제이코버스 코넬리스 레이서
더 프록터 앤드 갬블 캄파니
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/42—Block-or graft-polymers containing polysiloxane sequences
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
    • C08L83/04—Polysiloxanes
    • C08L83/06—Polysiloxanes containing silicon bound to oxygen-containing groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F283/00—Macromolecular compounds obtained by polymerising monomers on to polymers provided for in subclass C08G
    • C08F283/12—Macromolecular compounds obtained by polymerising monomers on to polymers provided for in subclass C08G on to polysiloxanes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/42—Block-or graft-polymers containing polysiloxane sequences
    • C08G77/442—Block-or graft-polymers containing polysiloxane sequences containing vinyl polymer sequences
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G81/00—Macromolecular compounds obtained by interreacting polymers in the absence of monomers, e.g. block polymers
    • C08G81/02—Macromolecular compounds obtained by interreacting polymers in the absence of monomers, e.g. block polymers at least one of the polymers being obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • C08G81/024—Block or graft polymers containing sequences of polymers of C08C or C08F and of polymers of C08G
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
    • C08L83/04—Polysiloxanes
    • C08L83/08—Polysiloxanes containing silicon bound to organic groups containing atoms other than carbon, hydrogen and oxygen
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/13—Hollow or container type article [e.g., tube, vase, etc.]
    • Y10T428/1352—Polymer or resin containing [i.e., natural or synthetic]
    • Y10T428/1386—Natural or synthetic rubber or rubber-like compound containing
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31652—Of asbestos
    • Y10T428/31663—As siloxane, silicone or silane
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31652—Of asbestos
    • Y10T428/31667—Next to addition polymer from unsaturated monomers, or aldehyde or ketone condensation product

Abstract

하기 일반식(Ⅰ)의 실록산 개질된 공중합체는 실질적으로 용매가 없는 환경내에서는 약 150내지 약 350℃의 온도, 50내지 350rpm에서 1시간 이하동안, 반응성 말단 그룹을 갖는 오가노실록산을 반응성 그룹을 갖는 폴리올레핀과 반응성 압축시켜(작용기의 몰비는 약 1:1 내지 약 1:1,100,000) 제조한다 :
상기식에서, X는 1 내지 1000이고; m은 2 내지 100이고; n은 0 내지 1000이고; y는 1내지 3이고; p는 1내지 200이고; R 및 R1은 독립적으로 수소, 1 내지 6개의 탄소를 갖는 알킬 그룹, 페닐, 벤질 또는 6내지 12개의 탄소를 갖는 알킬페닐로 구성되는 그룹으로부터 선택되고; R2는 C1―C6알킬, 페닐, 벤질 또는 6 내지 12개의 탄소를 갖는 알킬페닐로 구성되는 그룹으로부터 선택되고; R3는 메틸, 에틸 또는 프로필이고; Z는 O, S, NH 또는 NR′이고; R′는 페닐, C1―C4알킬 또는 C1―C3알킬페닐이다.

Description

실록산 개질된 폴리올레핀 공중합체(SILOXANE MODIFIED POLYOLEFIN COPOLYMERS)
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (11)

  1. 실질적으로 용매가 없는 환경내에서 약 150 내지 350℃의 온도, 200 내지 350rpm에서, 바람직하게는 200 내지 300rpm에서 1시간 이하동안, 반응성 말단 글부을 갖는 오가노실록산을 반응성 그룹을 갖는 폴리올레핀과 함께 반응시켜 압출(상기 작용기들의 몰비는 약 1:1 내지 1:100,000이다)시킴을 포함하는 실록산 개질된 폴리올레핀 공중합체의 제조방법.
  2. 제1항에 있어서, 실록산이 하기 일반식을 가짐을 특징으로 하는 방법 :
    상기식에서, X는 NH2, NHR′, OH 또는 SH이고; R′는 페닐, C1―C4알킬 또는 C1―C3알킬페닐이고; R, R1및 R3는 독립적으로 수소, C1―C6알킬, 페닐, 벤질 또는 6 내지 12개의 탄소를 갖는 알킬페닐이고; m은 2 내지 100이고; n은 0 내지 1000이고; y는 1 내지 3이다.
  3. 제2항에 있어서, 폴리올레핀이 에틸렌 또는 치환된 에틸렌으로부터 유도된 중합체이고, 바람직하게는 프로필렌, 스티렌, 알킬, 스티렌, 부틸렌, 부타디엔, 아크릴레이트 또는 이들의 혼합물이고; 상기 반응성 말단 그룹이 카복실산, 카복실산 무수물, 말레산 무수물, 산 염화물 또는 이소시아네이트와 반응하여 상응하는 에스테르, 아미드, 우레아 또는 우레탄을 형성하는 알콜, 티올, 1차 또는 2차 아민임을 특징으로 하는 방법.
  4. 제3항에 있어서, 폴리실록산이 하기 일반식을 가짐을 특징을 하는 방법 :
    상기식에서, n은 70이다.
  5. 제3항에 있어서, 폴리올레핀이 하기 일반식을 갖고, 바람직하게는 5 내지 20gm/10분의 용융수지를 갖는 폴리에틸렌 카복실산 유도체인 방법 :
    상기식에서 T는 OH, Cl, 무수물, 이소시아네이트, 또는 OR6이고; R6는 메틸, 에틸, 또는 프로필이고; x는 1 내지 1000이고; y는 2 또는 3이다.
  6. 실질적으로 용매가 없는 환경내에서 150 내지 350℃의 온도, 200 내지 350rpm에서 1시간 이하동안, 1000cps이상의 점도 및 반응성 말단 그룹을 갖는 오가노실록산을 반응성 그룹을 갖는 폴리올레핀과 함께 반응시켜 압출(상기 작용기들의 몰비는 1:1 내지 1:100,000 이다)시킴을 포함하며; 이때 압출기를, 하기 단계들을 포함하여 7개의 대역으로 분리함을 특징으로 하는 실록산 개질된 폴리올레핀 공중합체의 제조 방법; (1) 폴리올레킨을 호퍼(hopper)로부터 제1대역으로 궁급하고, 150℃에서 225℃로 가열하여 폴리올레핀을 가소화시키는 단계; (2) 폴리올레핀을 제2대역에서 혼련/혼합시키면서 150℃에서 225℃로 가열하는 단계; (3) 실록산 중합체를 3대역의 입구에 사출시켜 이것을 혼합하고 175℃에서 285℃로 가열하는 단계; (4) 이 혼합물을 가열하면서 제4대역을 통해 펌핑하는 단계; (5) 상기 혼합물을 제5대역에서 혼련하고 진공하에서 부산물을 배출시키는 단계; 및 (6) 공중합체를 펌핑시키고 다이를 통해 방출시키는 단계.
  7. 하기 일반식을 가짐을 특징으로 하는 실록산 폴리올레핀 공중합체 :
    상기식에서, X는 1 내지 1000이고; m은 2 내지 100이고; n은 0 내지 1000이고; 바람직하게는 70이고; y는 1 내지 3이고; p는 1 내지 200이고; R 및 R1은 독립적으로는 수소, 1 내지 6개의 탄소를 갖는 알킬 그룹, 페닐, 벤질 또는 6내지 12개의 탄소를 갖는 알킬페닐이고, 바람직하게는 메틸이고; R2는 C1―C6알킬, 페닐, 벤질 또는 6 내지 12개의 탄소를 갖는 알킬페닐이고; R3는 메틸, 에틸 또는 프로필이고; Z는 O, S, NH 또는 NR′이고, 바람직하게는 NH이고; R′는 페닐, C1―C4알킬 또는 C1―C3알킬페닐이다.
  8. 폴리실록산 분절이 5000 내지 300,000, 더욱 바람직하게는 8000 내지 200,000, 더더욱 바람직하게는 10,000 내지 30,000의 평균분자량을 가짐을 특징으로 하는, 제2항 내지 제5항 중 어느 한 항에 따른 공중합체.
  9. 제7항 또는 제8항에 따른 실록산 개질된 공중합체로부터 제조된 접착제 이형제.
  10. 제7항 또는제8항에따른 실록산 개질된 공중합체로부터 제조된 액체 소출용 포장제(liquid dispensing package).
  11. 제7항 또는 제8항에 따른 실록산 개질된 공중합체로부터 제조된 필름.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019950705885A 1993-06-24 1994-06-03 실록산개질된폴리올레핀공중합체 KR100329900B1 (ko)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US08/082,685 1993-06-24
US08/082,685 US5476901A (en) 1993-06-24 1993-06-24 Siloxane modified polyolefin copolymers
US08/082685 1993-06-24
PCT/US1994/006236 WO1995000578A1 (en) 1993-06-24 1994-06-03 Siloxane modified polyolefin copolymers

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KR960703146A true KR960703146A (ko) 1996-06-19
KR100329900B1 KR100329900B1 (ko) 2002-09-26

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US (2) US5476901A (ko)
EP (1) EP0705297B1 (ko)
JP (1) JPH08511825A (ko)
KR (1) KR100329900B1 (ko)
AT (1) ATE184295T1 (ko)
AU (2) AU6963494A (ko)
CA (1) CA2163734C (ko)
DE (1) DE69420560T2 (ko)
ES (1) ES2135584T3 (ko)
WO (1) WO1995000578A1 (ko)

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FR3124703B1 (fr) 2021-06-30 2024-03-08 Oreal Composition sous forme d’émulsion comprenant un tensioactif non ionique particulier
FR3124729B1 (fr) 2021-06-30 2024-02-16 Oreal Composition d’apparence monophasique comprenant l’association de deux tensioactifs non ioniques différents l’un de l’autre, dont un est siliconé
FR3124717B1 (fr) 2021-06-30 2024-03-01 Oreal Composition d’apparence monophasique comprenant un tensioactif anionique et un tensioactif amphotère
FR3124723B1 (fr) 2021-06-30 2024-02-16 Oreal Composition sous forme d’émulsion comprenant un tensioactif amphotère, un corps gras et un agent propulseur
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AU8313698A (en) 1998-10-22
CA2163734A1 (en) 1995-01-05
EP0705297B1 (en) 1999-09-08
US5476901A (en) 1995-12-19
WO1995000578A1 (en) 1995-01-05
ES2135584T3 (es) 1999-11-01
US5641835A (en) 1997-06-24
JPH08511825A (ja) 1996-12-10
DE69420560D1 (de) 1999-10-14
DE69420560T2 (de) 2000-04-27
EP0705297A1 (en) 1996-04-10
AU708721B2 (en) 1999-08-12
AU6963494A (en) 1995-01-17
KR100329900B1 (ko) 2002-09-26
CA2163734C (en) 2000-10-31
ATE184295T1 (de) 1999-09-15

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