KR870002117A - 2-옥소-1,3-디옥솔란의 제조방법 - Google Patents
2-옥소-1,3-디옥솔란의 제조방법 Download PDFInfo
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- KR870002117A KR870002117A KR1019860006754A KR860006754A KR870002117A KR 870002117 A KR870002117 A KR 870002117A KR 1019860006754 A KR1019860006754 A KR 1019860006754A KR 860006754 A KR860006754 A KR 860006754A KR 870002117 A KR870002117 A KR 870002117A
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- KR
- South Korea
- Prior art keywords
- epoxy
- catalyst
- group
- weight
- compound
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims 11
- KMTRUDSVKNLOMY-UHFFFAOYSA-N Ethylene carbonate Chemical compound O=C1OCCO1 KMTRUDSVKNLOMY-UHFFFAOYSA-N 0.000 title claims 2
- 239000004593 Epoxy Substances 0.000 claims 9
- 239000003054 catalyst Substances 0.000 claims 7
- 150000001875 compounds Chemical class 0.000 claims 7
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims 6
- -1 nitrogen-containing compound Chemical class 0.000 claims 4
- 239000001569 carbon dioxide Substances 0.000 claims 3
- 229910002092 carbon dioxide Inorganic materials 0.000 claims 3
- RAXXELZNTBOGNW-UHFFFAOYSA-N imidazole Natural products C1=CNC=N1 RAXXELZNTBOGNW-UHFFFAOYSA-N 0.000 claims 3
- NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Chemical compound [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 claims 3
- FVAUCKIRQBBSSJ-UHFFFAOYSA-M sodium iodide Chemical compound [Na+].[I-] FVAUCKIRQBBSSJ-UHFFFAOYSA-M 0.000 claims 3
- VHYFNPMBLIVWCW-UHFFFAOYSA-N 4-Dimethylaminopyridine Chemical compound CN(C)C1=CC=NC=C1 VHYFNPMBLIVWCW-UHFFFAOYSA-N 0.000 claims 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 2
- 150000002118 epoxides Chemical class 0.000 claims 2
- KYVBNYUBXIEUFW-UHFFFAOYSA-N 1,1,3,3-tetramethylguanidine Chemical compound CN(C)C(=N)N(C)C KYVBNYUBXIEUFW-UHFFFAOYSA-N 0.000 claims 1
- LXBGSDVWAMZHDD-UHFFFAOYSA-N 2-methyl-1h-imidazole Chemical compound CC1=NC=CN1 LXBGSDVWAMZHDD-UHFFFAOYSA-N 0.000 claims 1
- ULKLGIFJWFIQFF-UHFFFAOYSA-N 5K8XI641G3 Chemical compound CCC1=NC=C(C)N1 ULKLGIFJWFIQFF-UHFFFAOYSA-N 0.000 claims 1
- KCVHJZBJVWEDHM-UHFFFAOYSA-M CCCCC(CCCC)(CCCC)[N+](C)(CCC1=CC=CC=C1)CC(CCl)O.[Cl-] Chemical compound CCCCC(CCCC)(CCCC)[N+](C)(CCC1=CC=CC=C1)CC(CCl)O.[Cl-] KCVHJZBJVWEDHM-UHFFFAOYSA-M 0.000 claims 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims 1
- CTKINSOISVBQLD-UHFFFAOYSA-N Glycidol Chemical compound OCC1CO1 CTKINSOISVBQLD-UHFFFAOYSA-N 0.000 claims 1
- 239000005922 Phosphane Substances 0.000 claims 1
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 claims 1
- LINDOXZENKYESA-UHFFFAOYSA-N TMG Natural products CNC(N)=NC LINDOXZENKYESA-UHFFFAOYSA-N 0.000 claims 1
- 125000001931 aliphatic group Chemical group 0.000 claims 1
- 229910052783 alkali metal Inorganic materials 0.000 claims 1
- 150000001340 alkali metals Chemical class 0.000 claims 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims 1
- 150000001342 alkaline earth metals Chemical class 0.000 claims 1
- 150000001408 amides Chemical class 0.000 claims 1
- 150000001409 amidines Chemical class 0.000 claims 1
- 150000001412 amines Chemical class 0.000 claims 1
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims 1
- OEYIOHPDSNJKLS-UHFFFAOYSA-N choline Chemical compound C[N+](C)(C)CCO OEYIOHPDSNJKLS-UHFFFAOYSA-N 0.000 claims 1
- 229960001231 choline Drugs 0.000 claims 1
- GYZLOYUZLJXAJU-UHFFFAOYSA-N diglycidyl ether Chemical group C1OC1COCC1CO1 GYZLOYUZLJXAJU-UHFFFAOYSA-N 0.000 claims 1
- 125000003700 epoxy group Chemical group 0.000 claims 1
- 239000003822 epoxy resin Substances 0.000 claims 1
- 125000004185 ester group Chemical group 0.000 claims 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims 1
- 125000003055 glycidyl group Chemical group C(C1CO1)* 0.000 claims 1
- 150000002357 guanidines Chemical class 0.000 claims 1
- 150000004820 halides Chemical class 0.000 claims 1
- 125000005843 halogen group Chemical group 0.000 claims 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims 1
- 150000002460 imidazoles Chemical class 0.000 claims 1
- 239000012442 inert solvent Substances 0.000 claims 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 150000005677 organic carbonates Chemical class 0.000 claims 1
- 229910000064 phosphane Inorganic materials 0.000 claims 1
- 229920000647 polyepoxide Polymers 0.000 claims 1
- 150000003856 quaternary ammonium compounds Chemical class 0.000 claims 1
- 229920006395 saturated elastomer Polymers 0.000 claims 1
- 235000009518 sodium iodide Nutrition 0.000 claims 1
- 239000004575 stone Substances 0.000 claims 1
- HWCKGOZZJDHMNC-UHFFFAOYSA-M tetraethylammonium bromide Chemical compound [Br-].CC[N+](CC)(CC)CC HWCKGOZZJDHMNC-UHFFFAOYSA-M 0.000 claims 1
- IMNIMPAHZVJRPE-UHFFFAOYSA-N triethylenediamine Chemical compound C1CN2CCN1CC2 IMNIMPAHZVJRPE-UHFFFAOYSA-N 0.000 claims 1
- JOYRKODLDBILNP-UHFFFAOYSA-N urethane group Chemical group NC(=O)OCC JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
- C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
- C07D317/32—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D317/34—Oxygen atoms
- C07D317/36—Alkylene carbonates; Substituted alkylene carbonates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Epoxy Compounds (AREA)
- Epoxy Resins (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Secondary Cells (AREA)
- Catalysts (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (13)
- 적어도 하나의 에폭시 화합물을 불활성 용매의 존재 또는 부재하에서 적어도 하나의 촉매와 혼합하고, 상압 또는 약간 상승된 압력하에서 이산화탄소를 도입시키면소 40 내지 180℃에서 반응시켜 상응하는 유기 카보네이트를 제조함을 특징으로 하여, 촉매의 존재하에서 에폭시드와 이산화탄소의 반응으로 2-옥소-1,3-디옥솔란을 제조하는 방법.
- 제1항에 있어서, 1 내지 10바(bar), 바람직하게는 1 내지 5바, 특히 바람직하게는 1 내지 3바의 압력이 사용되는 방법.
- 제1항 또는 2항에 있어서, 촉매를 에폭시 성분에 대하여 0.02 내지 10중량%, 바람직하게는 0.05 내지 6중량%, 특히 바람직하게는 0.05 내지 3중량%의 양으로 사용하는 방법.
- 제1항 내지 3항 중의 어느 한 항에 있어서, 추가로 조 촉매를 에폭시 성분에 대하여 0.1 내지 10중량%, 바람직하게는 0.2 내지 5중량%, 특히 바람직하게는 0.4 내지 2.5중량%의 양으로 사용하는 방법.
- 제1항 내지 4항 중의 어느 한 항에 있어서, 에폭시 화합물과 이산화탄소와의 반응이 단지 부분적으로 수행되는 방법.
- 제1항 내지 5항 중의 어느 한 항에 있어서, 촉매로서 일반식(R1,R2,R3,R4)N+X-의 4급 암모늄 화합물, 일반식(R1,R2,R3) p의 포스판, 또는 아민, 구아니딘, 아미딘 및 이미다졸의 그룹중에서 선택된 질소-함유 화합물이 단독으로 또는 혼합물로 사용되는 방법.
- 제6항에 있어서, 벤질트리메젤틸암모늄 하이드록사이드, 벤질트리메틸, 벤질트리부틸-3-클로로-2-히드록시프로필 트리메틸암모늄 클로라이드, 테트라에틸암모늄 브로마이드, 콜린, 1,4-디아자비사이클로[2,2,2]-옥탄, 1,1,3,3-테트라메틸구아니딘, 4-디메틸아미노-피리딘, 트리페닐-및 트리톨릴포스판, 이미다졸, 1-메틸, 2-메틸이미다졸 또는 2-에틸-4-메틸이미다졸이 사용되는 방법.
- 제4항 내지 8항 중의 어느 한 항에 있어서, 조 촉매로서 알카리 금속 또는 알카리 토금속의 할로겐화물 또는 탄산염이 사용되는 방법.
- 제8항에 있어서, 조 촉매로서 요오드화 나트륨 또는 요오드화 칼륨이 사용되는 방법.
- 제1항 내지 9항 중의 어느 한 항에 있어서, 에폭시 화합물이 적어도 말단 1,2-에폭시 그룹을 갖는 방법.
- 제10항에 있어서, 에폭시 화합물로서, 탄소수 적어도 6인 지방족 에폭시돌, 글리시돌, 또는 일반식(2) (여기에서 Z는 수소원자, 메틸 또는 에틸그룹을 나타내고, X는 할로겐원자 또는 OH그룹을 나타낸다)의 에필할로히드린을 사용하는 방법.
- 제10항에 있어서, 대체로 적어도 하나의 , 일반식(3) (여기에서 Z는 일반식 (2)에서 정의한 바와 같다)의 치환되거나 비치환된 글리시딜 에테르그룹 또는 일반식 -OC-O-CH2-(4) (여기에서 Z는 일반식(2)에서 정의한 바와 같다)의 치환되거나 비치환된 글리시딜 에스테르 그룹을 함유하는 화합물 및 또한 다중 불포화된 에폭시와 화합물 및, 아미드와 우레탄 그룹을 함유하는 에폭시드를 에폭시 화합물로서 반응시키는 방법.
- 제10항 내지 12항 중의 어느 한 항에 있어서, 폴리글리시딜에테르, 말단 에폭시그룹을 갖는 가소화된 에폭시수지, 포화되거나 또는 에틸렌형으로 불포화된(폴리) 카복실산의 글리시딜 에스테르를 반응시키는 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DEP3529263.6 | 1985-08-16 | ||
DE19853529263 DE3529263A1 (de) | 1985-08-16 | 1985-08-16 | Verfahren zur herstellung von 2-oxo-1,3-dioxolanen |
DE3529263 | 1985-08-16 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR870002117A true KR870002117A (ko) | 1987-03-30 |
KR940008751B1 KR940008751B1 (ko) | 1994-09-26 |
Family
ID=6278572
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019860006754A KR940008751B1 (ko) | 1985-08-16 | 1986-08-16 | 2-옥소-1,3-디옥솔란의 제조방법 |
Country Status (18)
Country | Link |
---|---|
US (1) | US4892954A (ko) |
EP (1) | EP0212409B1 (ko) |
JP (1) | JP2565875B2 (ko) |
KR (1) | KR940008751B1 (ko) |
CN (1) | CN1020729C (ko) |
AR (1) | AR242201A1 (ko) |
AT (1) | ATE51225T1 (ko) |
AU (1) | AU585385B2 (ko) |
BR (1) | BR8603901A (ko) |
CA (1) | CA1334851C (ko) |
DE (2) | DE3529263A1 (ko) |
DK (1) | DK164864C (ko) |
ES (1) | ES2000286A6 (ko) |
FI (1) | FI86719C (ko) |
MX (1) | MX170907B (ko) |
NO (1) | NO863302L (ko) |
PT (1) | PT83209B (ko) |
ZA (1) | ZA866149B (ko) |
Families Citing this family (95)
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DE3600602A1 (de) * | 1986-01-11 | 1987-07-16 | Hoechst Ag | Verfahren zur herstellung von 2-oxo-1,3-dioxolanen |
DE3809840C2 (de) * | 1988-03-21 | 1993-11-11 | Dainippon Ink & Chemicals | Lagerstabile wäßrige Emulsionen Cyclocarbonatgruppen enthaltender Polymere |
US7119202B1 (en) | 1989-02-08 | 2006-10-10 | Glaxo Wellcome Inc. | Substituted-1,3-oxathiolanes and substituted-1,3-dioxolanes with antiviral properties |
US6350753B1 (en) | 1988-04-11 | 2002-02-26 | Biochem Pharma Inc. | 2-Substituted-4-substituted-1,3-dioxolanes and use thereof |
US6903224B2 (en) | 1988-04-11 | 2005-06-07 | Biochem Pharma Inc. | Substituted 1,3-oxathiolanes |
US5270315A (en) * | 1988-04-11 | 1993-12-14 | Biochem Pharma Inc. | 4-(purinyl bases)-substituted-1,3-dioxlanes |
UA45942A (uk) * | 1989-02-08 | 2002-05-15 | Біокем Фарма, Інк. | 1,3-оксатіолан, його похідні, спосіб (варіанти) його одержання та фармацевтична композиція |
GB9009861D0 (en) | 1990-05-02 | 1990-06-27 | Glaxo Group Ltd | Chemical compounds |
US5095124A (en) * | 1990-09-10 | 1992-03-10 | Isp Investments Inc. | Process for the preparation of alk-1-enyl ether cyclocarbonate |
DE4030283A1 (de) * | 1990-09-25 | 1992-03-26 | Ruetgerswerke Ag | Verfahren zur herstellung cyclischer carbonate |
US5091543A (en) * | 1990-10-15 | 1992-02-25 | Arco Chemical Technology, Inc. | Preparation of cyclic carbonates using alkylammonium and tertiary amine catalysts |
US5587480A (en) * | 1990-11-13 | 1996-12-24 | Biochem Pharma, Inc. | Substituted 1,3-oxathiolanes and substituted 1,3-dithiolanes with antiviral properties |
US6228860B1 (en) | 1990-11-13 | 2001-05-08 | Biochem Pharma Inc. | Substituted 1,3-oxathiolanes with antiviral properties |
US6369066B1 (en) | 1990-11-13 | 2002-04-09 | Biochem Pharma, Inc. | Substituted 1,3-oxathiolanes with antiviral properties |
DE4129752C2 (de) * | 1991-09-04 | 1994-01-05 | Dainippon Ink & Chemicals | Verfahren zur Herstellung von 2-Oxo-1,3-dioxolanen |
DE4129753C2 (de) * | 1991-09-04 | 1995-05-04 | Dainippon Ink & Chemicals | Verfahren zur Herstellung von Cyclocarbonatverbindungen |
US5179214A (en) * | 1991-09-23 | 1993-01-12 | Texaco Chemical Company | Process for manufacturing alkylene carbonates |
US5283356A (en) * | 1992-08-03 | 1994-02-01 | Texaco Chemical Company | Process for manufacturing alkylene carbonates using metal phthalocyanine catalysts |
DK0678105T3 (da) * | 1993-01-06 | 1998-08-10 | Akzo Nobel Nv | Oligomere, sterisk hindrede polyamintværbindere ogovertræksammensætninger indeholdende disse |
US5340889A (en) * | 1993-07-19 | 1994-08-23 | Texaco Chemical Company | Liquification of bis-carbonates of bis-glycidyl ethers |
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DE19505892C1 (de) * | 1995-02-21 | 1996-03-14 | Goldschmidt Ag Th | Verfahren zur Herstellung von Carbonatgruppen enthaltenden Organopolysiloxanen |
DE19512316A1 (de) * | 1995-04-01 | 1996-10-02 | Hoechst Ag | Härtungsmittel für elastische Epoxidharz-Systeme |
DE19625344A1 (de) * | 1996-06-25 | 1998-01-08 | Herberts Gmbh | Wäßriges Überzugsmittel und dessen Verwendung zur Herstellung von Füllerschichten |
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US5998568A (en) * | 1999-01-14 | 1999-12-07 | Reichhold, Inc. | Polyesters prepared from alkoxylated intermediates |
US5969056A (en) * | 1999-01-14 | 1999-10-19 | Reichhold, Inc. | Process for preparing esterification products from cyclic organic carbonates using catalysts comprising quaternary ammonium salts |
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US7750170B2 (en) * | 2005-12-22 | 2010-07-06 | Shell Oil Company | Process for mixing an oxidant having explosive potential with a hydrocarbon |
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-
1985
- 1985-08-16 DE DE19853529263 patent/DE3529263A1/de not_active Withdrawn
-
1986
- 1986-08-04 EP EP86110736A patent/EP0212409B1/de not_active Expired - Lifetime
- 1986-08-04 DE DE8686110736T patent/DE3669717D1/de not_active Expired - Lifetime
- 1986-08-04 AT AT86110736T patent/ATE51225T1/de not_active IP Right Cessation
- 1986-08-14 DK DK387386A patent/DK164864C/da not_active IP Right Cessation
- 1986-08-14 ES ES8601130A patent/ES2000286A6/es not_active Expired
- 1986-08-14 PT PT83209A patent/PT83209B/pt not_active IP Right Cessation
- 1986-08-14 FI FI863298A patent/FI86719C/fi not_active IP Right Cessation
- 1986-08-14 AR AR86304909A patent/AR242201A1/es active
- 1986-08-15 ZA ZA866149A patent/ZA866149B/xx unknown
- 1986-08-15 CA CA000516014A patent/CA1334851C/en not_active Expired - Fee Related
- 1986-08-15 JP JP61190730A patent/JP2565875B2/ja not_active Expired - Lifetime
- 1986-08-15 MX MX003452A patent/MX170907B/es unknown
- 1986-08-15 AU AU61506/86A patent/AU585385B2/en not_active Ceased
- 1986-08-15 BR BR8603901A patent/BR8603901A/pt not_active IP Right Cessation
- 1986-08-15 NO NO863302A patent/NO863302L/no unknown
- 1986-08-16 CN CN86105205A patent/CN1020729C/zh not_active Expired - Fee Related
- 1986-08-16 KR KR1019860006754A patent/KR940008751B1/ko not_active IP Right Cessation
-
1987
- 1987-10-21 US US07/111,979 patent/US4892954A/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
JPS6245584A (ja) | 1987-02-27 |
FI86719C (fi) | 1992-10-12 |
CN1020729C (zh) | 1993-05-19 |
FI863298A (fi) | 1987-02-17 |
DK164864B (da) | 1992-08-31 |
CN86105205A (zh) | 1987-02-11 |
AR242201A1 (es) | 1993-03-31 |
JP2565875B2 (ja) | 1996-12-18 |
AU6150686A (en) | 1987-02-19 |
NO863302L (no) | 1987-02-17 |
ES2000286A6 (es) | 1988-02-01 |
NO863302D0 (no) | 1986-08-15 |
FI863298A0 (fi) | 1986-08-14 |
DK387386D0 (da) | 1986-08-14 |
CA1334851C (en) | 1995-03-21 |
PT83209B (pt) | 1989-03-30 |
DK387386A (da) | 1987-02-17 |
DK164864C (da) | 1993-01-18 |
EP0212409A3 (en) | 1987-10-21 |
DE3669717D1 (de) | 1990-04-26 |
MX170907B (es) | 1993-09-22 |
PT83209A (en) | 1986-09-01 |
US4892954A (en) | 1990-01-09 |
KR940008751B1 (ko) | 1994-09-26 |
EP0212409B1 (de) | 1990-03-21 |
AU585385B2 (en) | 1989-06-15 |
FI86719B (fi) | 1992-06-30 |
ATE51225T1 (de) | 1990-04-15 |
EP0212409A2 (de) | 1987-03-04 |
ZA866149B (en) | 1987-04-29 |
BR8603901A (pt) | 1987-03-24 |
DE3529263A1 (de) | 1987-02-19 |
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