KR20150000412A - 토너 - Google Patents
토너 Download PDFInfo
- Publication number
- KR20150000412A KR20150000412A KR1020140072771A KR20140072771A KR20150000412A KR 20150000412 A KR20150000412 A KR 20150000412A KR 1020140072771 A KR1020140072771 A KR 1020140072771A KR 20140072771 A KR20140072771 A KR 20140072771A KR 20150000412 A KR20150000412 A KR 20150000412A
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- KR
- South Korea
- Prior art keywords
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- Prior art date
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- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 288
- 239000002245 particle Substances 0.000 claims abstract description 264
- 239000010419 fine particle Substances 0.000 claims abstract description 223
- 239000000654 additive Substances 0.000 claims abstract description 68
- 238000009792 diffusion process Methods 0.000 claims abstract description 60
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 57
- 230000000996 additive effect Effects 0.000 claims abstract description 48
- 238000011049 filling Methods 0.000 claims abstract description 29
- 229920005989 resin Polymers 0.000 claims abstract description 27
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- 239000003086 colorant Substances 0.000 claims abstract description 21
- 239000011230 binding agent Substances 0.000 claims abstract description 17
- 239000000377 silicon dioxide Substances 0.000 claims description 104
- 239000000178 monomer Substances 0.000 claims description 36
- 239000011164 primary particle Substances 0.000 claims description 35
- VEALVRVVWBQVSL-UHFFFAOYSA-N strontium titanate Chemical compound [Sr+2].[O-][Ti]([O-])=O VEALVRVVWBQVSL-UHFFFAOYSA-N 0.000 claims description 29
- 239000000203 mixture Substances 0.000 claims description 23
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 19
- 239000012736 aqueous medium Substances 0.000 claims description 14
- 229910052757 nitrogen Inorganic materials 0.000 claims description 8
- 238000001179 sorption measurement Methods 0.000 claims description 6
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- 238000004833 X-ray photoelectron spectroscopy Methods 0.000 claims description 5
- 230000000379 polymerizing effect Effects 0.000 claims description 2
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims 1
- 229910052726 zirconium Inorganic materials 0.000 claims 1
- 239000011248 coating agent Substances 0.000 abstract description 30
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- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 21
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- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 13
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 11
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- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 11
- 150000003839 salts Chemical class 0.000 description 11
- 229910052710 silicon Inorganic materials 0.000 description 11
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- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 10
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 10
- 239000000047 product Chemical class 0.000 description 10
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- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
- 238000004458 analytical method Methods 0.000 description 9
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- 229920001225 polyester resin Polymers 0.000 description 8
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- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 8
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 7
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- 125000004386 diacrylate group Chemical group 0.000 description 7
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- FFUAGWLWBBFQJT-UHFFFAOYSA-N hexamethyldisilazane Chemical compound C[Si](C)(C)N[Si](C)(C)C FFUAGWLWBBFQJT-UHFFFAOYSA-N 0.000 description 7
- 230000007774 longterm Effects 0.000 description 7
- 238000002844 melting Methods 0.000 description 7
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- 238000002360 preparation method Methods 0.000 description 7
- 239000002904 solvent Substances 0.000 description 7
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- MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 6
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-M acrylate group Chemical group C(C=C)(=O)[O-] NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 6
- 125000005907 alkyl ester group Chemical group 0.000 description 6
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- 125000000524 functional group Chemical group 0.000 description 6
- 239000007789 gas Substances 0.000 description 6
- 239000002736 nonionic surfactant Substances 0.000 description 6
- 239000011163 secondary particle Substances 0.000 description 6
- 238000010008 shearing Methods 0.000 description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 5
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 5
- 229910052782 aluminium Inorganic materials 0.000 description 5
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 5
- 239000003945 anionic surfactant Substances 0.000 description 5
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical class C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 5
- 238000004364 calculation method Methods 0.000 description 5
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- 230000005484 gravity Effects 0.000 description 5
- 235000013980 iron oxide Nutrition 0.000 description 5
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 5
- 239000011976 maleic acid Substances 0.000 description 5
- 238000000691 measurement method Methods 0.000 description 5
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 5
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- 238000003825 pressing Methods 0.000 description 5
- 238000000926 separation method Methods 0.000 description 5
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- 238000010557 suspension polymerization reaction Methods 0.000 description 5
- 239000010936 titanium Substances 0.000 description 5
- ARCGXLSVLAOJQL-UHFFFAOYSA-N trimellitic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C(C(O)=O)=C1 ARCGXLSVLAOJQL-UHFFFAOYSA-N 0.000 description 5
- 238000005406 washing Methods 0.000 description 5
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 4
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 4
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 4
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- HNEGQIOMVPPMNR-IHWYPQMZSA-N citraconic acid Chemical compound OC(=O)C(/C)=C\C(O)=O HNEGQIOMVPPMNR-IHWYPQMZSA-N 0.000 description 4
- 229940018557 citraconic acid Drugs 0.000 description 4
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- 229910052742 iron Inorganic materials 0.000 description 4
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 description 4
- 229910021506 iron(II) hydroxide Inorganic materials 0.000 description 4
- NCNCGGDMXMBVIA-UHFFFAOYSA-L iron(ii) hydroxide Chemical compound [OH-].[OH-].[Fe+2] NCNCGGDMXMBVIA-UHFFFAOYSA-L 0.000 description 4
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 description 4
- CERQOIWHTDAKMF-UHFFFAOYSA-M methacrylate group Chemical group C(C(=C)C)(=O)[O-] CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 description 4
- 239000012299 nitrogen atmosphere Substances 0.000 description 4
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- 229910052712 strontium Inorganic materials 0.000 description 4
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 4
- 229910052719 titanium Inorganic materials 0.000 description 4
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 4
- 239000012808 vapor phase Substances 0.000 description 4
- JAHNSTQSQJOJLO-UHFFFAOYSA-N 2-(3-fluorophenyl)-1h-imidazole Chemical compound FC1=CC=CC(C=2NC=CN=2)=C1 JAHNSTQSQJOJLO-UHFFFAOYSA-N 0.000 description 3
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 description 3
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- 239000005977 Ethylene Substances 0.000 description 3
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- 125000000217 alkyl group Chemical group 0.000 description 3
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 description 3
- 125000003118 aryl group Chemical group 0.000 description 3
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- ATBAMAFKBVZNFJ-UHFFFAOYSA-N beryllium atom Chemical compound [Be] ATBAMAFKBVZNFJ-UHFFFAOYSA-N 0.000 description 3
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- NYGZLYXAPMMJTE-UHFFFAOYSA-M metanil yellow Chemical group [Na+].[O-]S(=O)(=O)C1=CC=CC(N=NC=2C=CC(NC=3C=CC=CC=3)=CC=2)=C1 NYGZLYXAPMMJTE-UHFFFAOYSA-M 0.000 description 3
- LVHBHZANLOWSRM-UHFFFAOYSA-N methylenebutanedioic acid Natural products OC(=O)CC(=C)C(O)=O LVHBHZANLOWSRM-UHFFFAOYSA-N 0.000 description 3
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- RYYKJJJTJZKILX-UHFFFAOYSA-M sodium octadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 description 3
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- OZAIFHULBGXAKX-UHFFFAOYSA-N 2-(2-cyanopropan-2-yldiazenyl)-2-methylpropanenitrile Chemical compound N#CC(C)(C)N=NC(C)(C)C#N OZAIFHULBGXAKX-UHFFFAOYSA-N 0.000 description 2
- XMNIXWIUMCBBBL-UHFFFAOYSA-N 2-(2-phenylpropan-2-ylperoxy)propan-2-ylbenzene Chemical compound C=1C=CC=CC=1C(C)(C)OOC(C)(C)C1=CC=CC=C1 XMNIXWIUMCBBBL-UHFFFAOYSA-N 0.000 description 2
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- INQDDHNZXOAFFD-UHFFFAOYSA-N 2-[2-(2-prop-2-enoyloxyethoxy)ethoxy]ethyl prop-2-enoate Chemical compound C=CC(=O)OCCOCCOCCOC(=O)C=C INQDDHNZXOAFFD-UHFFFAOYSA-N 0.000 description 2
- HCLJOFJIQIJXHS-UHFFFAOYSA-N 2-[2-[2-(2-prop-2-enoyloxyethoxy)ethoxy]ethoxy]ethyl prop-2-enoate Chemical compound C=CC(=O)OCCOCCOCCOCCOC(=O)C=C HCLJOFJIQIJXHS-UHFFFAOYSA-N 0.000 description 2
- KUDUQBURMYMBIJ-UHFFFAOYSA-N 2-prop-2-enoyloxyethyl prop-2-enoate Chemical compound C=CC(=O)OCCOC(=O)C=C KUDUQBURMYMBIJ-UHFFFAOYSA-N 0.000 description 2
- ZGHFDIIVVIFNPS-UHFFFAOYSA-N 3-Methyl-3-buten-2-one Chemical compound CC(=C)C(C)=O ZGHFDIIVVIFNPS-UHFFFAOYSA-N 0.000 description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
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- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
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- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
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- 239000002202 Polyethylene glycol Substances 0.000 description 2
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Landscapes
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- Inorganic Chemistry (AREA)
- Developing Agents For Electrophotography (AREA)
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| JP2013131695 | 2013-06-24 | ||
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| JPJP-P-2014-102124 | 2014-05-16 | ||
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| JP (1) | JP6399804B2 (enExample) |
| KR (1) | KR20150000412A (enExample) |
| CN (1) | CN104238295B (enExample) |
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| US9606462B2 (en) * | 2014-08-07 | 2017-03-28 | Canon Kabushiki Kaisha | Toner and method for manufacturing toner |
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| JP6991701B2 (ja) | 2015-12-04 | 2022-01-12 | キヤノン株式会社 | トナー |
| US10228627B2 (en) | 2015-12-04 | 2019-03-12 | Canon Kabushiki Kaisha | Toner |
| DE102016116610B4 (de) | 2015-12-04 | 2021-05-20 | Canon Kabushiki Kaisha | Toner |
| JP6768423B2 (ja) | 2015-12-04 | 2020-10-14 | キヤノン株式会社 | トナーの製造方法 |
| US9804519B2 (en) | 2015-12-04 | 2017-10-31 | Canon Kabushiki Kaisha | Method for producing toner |
| JP6762706B2 (ja) | 2015-12-04 | 2020-09-30 | キヤノン株式会社 | トナー |
| US9971263B2 (en) | 2016-01-08 | 2018-05-15 | Canon Kabushiki Kaisha | Toner |
| JP6910805B2 (ja) | 2016-01-28 | 2021-07-28 | キヤノン株式会社 | トナー、画像形成装置及び画像形成方法 |
| US9897932B2 (en) * | 2016-02-04 | 2018-02-20 | Canon Kabushiki Kaisha | Toner |
| JP6859141B2 (ja) | 2016-03-24 | 2021-04-14 | キヤノン株式会社 | トナー粒子の製造方法 |
| JP6873796B2 (ja) | 2016-04-21 | 2021-05-19 | キヤノン株式会社 | トナー |
| JP6878133B2 (ja) | 2016-05-20 | 2021-05-26 | キヤノン株式会社 | トナー |
| US9946181B2 (en) | 2016-05-20 | 2018-04-17 | Canon Kabushiki Kaisha | Toner |
| JP2017223945A (ja) * | 2016-06-09 | 2017-12-21 | キヤノン株式会社 | トナー |
| JP6904801B2 (ja) | 2016-06-30 | 2021-07-21 | キヤノン株式会社 | トナー、該トナーを備えた現像装置及び画像形成装置 |
| JP6869819B2 (ja) | 2016-06-30 | 2021-05-12 | キヤノン株式会社 | トナー、現像装置及び画像形成装置 |
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| US10295921B2 (en) | 2016-12-21 | 2019-05-21 | Canon Kabushiki Kaisha | Toner |
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| JP7023721B2 (ja) * | 2017-02-28 | 2022-02-22 | キヤノン株式会社 | トナー |
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| US10451985B2 (en) * | 2017-02-28 | 2019-10-22 | Canon Kabushiki Kaisha | Toner |
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| US10241430B2 (en) | 2017-05-10 | 2019-03-26 | Canon Kabushiki Kaisha | Toner, and external additive for toner |
| US10545420B2 (en) | 2017-07-04 | 2020-01-28 | Canon Kabushiki Kaisha | Magnetic toner and image-forming method |
| JP7005328B2 (ja) * | 2017-12-20 | 2022-02-10 | キヤノン株式会社 | トナー |
| JP2019128516A (ja) * | 2018-01-26 | 2019-08-01 | キヤノン株式会社 | トナー |
| US10768540B2 (en) | 2018-02-14 | 2020-09-08 | Canon Kabushiki Kaisha | External additive, method for manufacturing external additive, and toner |
| JP7066439B2 (ja) | 2018-02-14 | 2022-05-13 | キヤノン株式会社 | トナー用外添剤、トナー用外添剤の製造方法及びトナー |
| EP3582017B1 (en) | 2018-06-13 | 2023-04-26 | Canon Kabushiki Kaisha | Toner and method for producing toner |
| EP3582020B1 (en) | 2018-06-13 | 2023-08-30 | Canon Kabushiki Kaisha | Toner |
| US10732529B2 (en) | 2018-06-13 | 2020-08-04 | Canon Kabushiki Kaisha | Positive-charging toner |
| CN110597031B (zh) | 2018-06-13 | 2024-08-13 | 佳能株式会社 | 调色剂 |
| EP3582013B1 (en) | 2018-06-13 | 2023-08-09 | Canon Kabushiki Kaisha | Toner and method for producing toner |
| US10859931B2 (en) | 2018-06-13 | 2020-12-08 | Canon Kabushiki Kaisha | Toner and two-component developer |
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| CN110597028A (zh) | 2018-06-13 | 2019-12-20 | 佳能株式会社 | 磁性调色剂和磁性调色剂的制造方法 |
| CN110597029B (zh) | 2018-06-13 | 2025-01-03 | 佳能株式会社 | 调色剂和调色剂的制造方法 |
| US10838316B2 (en) | 2018-08-28 | 2020-11-17 | Canon Kabushiki Kaisha | Image forming apparatus |
| JP7286471B2 (ja) * | 2018-08-28 | 2023-06-05 | キヤノン株式会社 | トナー |
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| JP5911235B2 (ja) * | 2011-08-29 | 2016-04-27 | キヤノン株式会社 | トナー |
| JP5442045B2 (ja) * | 2012-02-01 | 2014-03-12 | キヤノン株式会社 | 磁性トナー |
| JP6184191B2 (ja) | 2012-06-27 | 2017-08-23 | キヤノン株式会社 | トナー |
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| US9239528B2 (en) | 2016-01-19 |
| JP2015028601A (ja) | 2015-02-12 |
| US20140377696A1 (en) | 2014-12-25 |
| JP6399804B2 (ja) | 2018-10-03 |
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