JP7168704B2 - 抗菌性ガラス組成物、それを含むガラス、およびポリマー物品 - Google Patents
抗菌性ガラス組成物、それを含むガラス、およびポリマー物品 Download PDFInfo
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Description
本明細書に記載の組成物の非限定的な例を表1中に列挙する。表1中の組成物を、バッチ処理し、溶融させ、ガラスを形成した。表2は、表1の組成物および/またはそれらより形成されたガラスの選択された性質を示しており、溶融条件、アニール、溶融物の外観、密度、アニール点(Beam Bending Viscometer(BBV)により測定される)、歪点(BBVによって測定される)、軟化点(平行板粘度計(PPV)によって測定される)、ビッカース硬度、ビッカース亀裂発生、シェブロンノッチによる破壊靱性、熱膨張係数など、およびその他の性質が含まれる。表2は、ICP技術によって求められるCu酸化物の重量パーセント、および選択されたガラスのCu1+:Cu2+の比も含む。
ガラスを含む物品において、前記ガラスが、モルパーセントの単位で:
約40~約70の範囲内のSiO2、
約0~約20の範囲内のAl2O3、
約10~約50の範囲内の銅含有酸化物、
約0~約15の範囲内のCaO、
約0~約15の範囲内のMgO、
約0~約25の範囲内のP2O5、
約0~約25の範囲内のB2O3、
約0~約20の範囲内のK2O、
約0~約5の範囲内のZnO、
約0~約20の範囲内のNa2O、および
約0~約5の範囲内のFe2O3
を含み、
前記銅含有酸化物の量がAl2O3の量よりも多いことを特徴とする、物品。
ポリマー、モノマー、バインダー、または溶媒をさらに含むことを特徴とする実施形態1に記載の物品。
EPA Test Method for Efficacy of Copper Alloy as a Sanitizer試験条件下で、黄色ブドウ球菌(Staphylococcus aureus)、エンテロバクター・アエロゲネス(Enterobacter aerogenes)、緑膿菌(Pseudomomas aeruginosa)、メチシリン耐性黄色ブドウ球菌(Methicillin Resistant Staphylococcus aureus)、および大腸菌(E.coli)のいずれか1つ以上の濃度の2対数減少以上をさらに示すことを特徴とする実施形態1または実施形態2に記載の物品。
JIS Z 2801(2000)試験条件または細菌用修正JIS Z 2801試験下で、黄色ブドウ球菌(Staphylococcus aureus)、エンテロバクター・アエロゲネス(Enterobacter aerogenes)、緑膿菌(Pseudomomas aeruginosa bacteria)、メチシリン耐性黄色ブドウ球菌(Methicillin Resistant Staphylococcus aureus)、および大腸菌(E.coli)のいずれか1つ以上の濃度の4対数減少以上をさらに示すことを特徴とする実施形態1~3のいずれか一項に記載の物品。
ウイルス用修正JIS Z 2801試験下で、マウスノロウイルス(Murine Norovirus)の濃度の4対数減少以上をさらに示すことを特徴とする実施形態1~4のいずれか一項に記載の物品。
前記銅含有酸化物がCuOおよびCu2Oの少なくとも1つを含むことを特徴とする実施形態1~のいずれか一項に記載の物品。
複数のCu1+イオンをさらに含むことを特徴とする実施形態1~6のいずれか一項に記載の物品。
Cu金属をさらに含むことを特徴とする実施形態1~7のいずれか一項に記載の物品。
前記ガラスが黒銅鉱を実質的に含まないことを特徴とする実施形態1~8のいずれか一項に記載の物品。
前記組成物が約5モルパーセント以下の量のAl2O3を含むことを特徴とする実施形態1~9のいずれか一項に記載の物品。
前記組成物がAl2O3を実質的に含まないことを特徴とする実施形態1~10のいずれか一項に記載の物品。
赤銅鉱相をさらに含み、前記赤銅鉱相が、約5マイクロメートル(μm)以下の平均主要寸法を有する結晶を含むことを特徴とする実施形態1~11のいずれか一項に記載の物品。
前記平均主要寸法が約500ナノメートル(nm)以下であることを特徴とする実施形態12に記載の物品。
前記組成物が核剤を含み、前記核剤がTiO2およびZrO2のいずれか1つ以上を含むことを特徴とする実施形態1~13のいずれか一項に記載の物品。
ガラスを含む物品において、前記ガラスが
複数のCu1+イオンを含む赤銅鉱相を含み、
B2O3、P2O5、およびR2Oの少なくとも1つを含むことを特徴とする物品。
40モル%を超えるSiO2を含むガラス相をさらに含むことを特徴とする実施形態15に記載の物品。
ポリマー、モノマー、バインダー、または溶媒をさらに含むことを特徴とする実施形態15に記載の物品。
重量パーセント基準で約10:90~約90:10の範囲内のガラス対ポリマーの比をさらに示すことを特徴とする実施形態16に記載の物品。
EPA Test Method for Efficacy of Copper Alloy as a Sanitizer試験条件下で、黄色ブドウ球菌(Staphylococcus aureus)、エンテロバクター・アエロゲネス(Enterobacter aerogenes)、緑膿菌(Pseudomomas aeruginosa bacteria)、メチシリン耐性黄色ブドウ球菌(Methicillin Resistant Staphylococcus aureus)、および大腸菌(E.coli)のいずれか1つ以上の濃度の2対数減少以上をさらに示すことを特徴とする実施形態15~18のいずれか一項に記載の物品。
JIS Z 2801(2000)試験条件または細菌用修正JIS Z 2801試験下で、黄色ブドウ球菌(Staphylococcus aureus)、エンテロバクター・アエロゲネス(Enterobacter aerogenes)、緑膿菌(Pseudomomas aeruginosa bacteria)、メチシリン耐性黄色ブドウ球菌(Methicillin Resistant Staphylococcus aureus)、および大腸菌(E.coli)のいずれか1つ以上の濃度の4対数減少以上をさらに示すことを特徴とする実施形態15~19のいずれか一項に記載の物品。
ウイルス用修正JIS Z 2801試験下で、マウスノロウイルス(Murine Norovirus)の濃度の4対数減少以上をさらに示すことを特徴とする実施形態15~20のいずれか一項に記載の物品。
前記ガラス相が前記赤銅鉱相の重量を基準とした量で存在することを特徴とする実施形態16~21のいずれか一項に記載の物品。
前記赤銅鉱相が前記ガラス相中に分散していることを特徴とする実施形態16~22のいずれか一項に記載の物品。
前記赤銅鉱相および前記ガラス相のいずれか一方または両方がCu1+を含むことを特徴とする実施形態15~23のいずれか一項に記載の物品。
前記赤銅鉱相が約5マイクロメートル(μm)以下の平均主要寸法を有する結晶を含むことを特徴とする実施形態15~24のいずれか一項に記載の物品。
水の存在下で前記赤銅鉱相が分解性であり浸出することを特徴とする実施形態15~25のいずれか一項に記載の物品。
ガラスが約5ナノメートル(nm)未満の深さを有する表面部分を含み、前記表面部分が複数の銅イオンを含み、前記複数の銅イオンの少なくとも75%がCu1+であることを特徴とする実施形態15~26のいずれか一項に記載の物品。
前記複数の銅イオンの約25%未満がCu2+であることを特徴とする実施形態27に記載の物品。
前記ガラス物品がAl2O3を実質的に含まないことを特徴とする実施形態15~28のいずれか一項に記載の物品。
前記赤銅鉱相が前記ガラスの少なくとも約10重量パーセントを構成することを特徴とする実施形態15~29のいずれか一項に記載の物品。
前記赤銅鉱相が前記ガラスの少なくとも約20重量パーセントを構成することを特徴とする実施形態15~30のいずれか一項に記載の物品。
表面と、前記表面上、ならびにガラス網目およびガラスマトリックスの少なくとも1つの中に配置された複数のCu1+イオンとを含む無機材料を含むことを特徴とする物品。
ポリマー、モノマー、バインダー、または溶媒をさらに含むことを特徴とする実施形態32に記載の物品。
EPA Test Method for Efficacy of Copper Alloy as a Sanitizer試験条件下で、黄色ブドウ球菌(Staphylococcus aureus)、エンテロバクター・アエロゲネス(Enterobacter aerogenes)、緑膿菌(Pseudomomas aeruginosa)、メチシリン耐性黄色ブドウ球菌(Methicillin Resistant Staphylococcus aureus)、および大腸菌(E.coli)のいずれか1つ以上の濃度の2対数減少以上、
JIS Z 2801(2000)試験条件または細菌用修正JIS Z 2801試験下で、黄色ブドウ球菌(Staphylococcus aureus)、エンテロバクター・アエロゲネス(Enterobacter aerogenes)、緑膿菌(Pseudomomas aeruginosa)、メチシリン耐性黄色ブドウ球菌(Methicillin Resistant Staphylococcus aureus)、および大腸菌(E.coli)のいずれか1つ以上の濃度の4対数減少以上、
ウイルス用修正JIS Z 2801試験下で、マウスノロウイルス(Murine Norovirus)の濃度の4対数減少以上
のいずれか1つ以上をさらに示すことを特徴とする実施形態32または実施形態33に記載の物品。
前記ガラス網目が原子を含み、前記複数のCu1+イオンが前記原子に原子的に結合していることを特徴とする実施形態32~34のいずれか一項に記載の物品。
前記無機材料が、モルパーセントの単位で:
約40~約70の範囲内のSiO2、
約0~約20の範囲内のAl2O3、
約10~約50の範囲内の銅含有酸化物、
約0~約15の範囲内のCaO、
約0~約15の範囲内のMgO、
約0~約25の範囲内のP2O5、
約0~約25の範囲内のB2O3、
約0~約20の範囲内のK2O、
約0~約5の範囲内のZnO、
約0~約20の範囲内のNa2O、および
約0~約5の範囲内のFe2O3
を含み;
前記銅含有酸化物の量がAl2O3の量よりも多いことを特徴とする実施形態32~35のいずれか一項に記載の物品。
前記無機材料が核剤を含み、前記核剤がTiO2およびZrO2のいずれか1つ以上を含むことを特徴とする実施形態32~36のいずれか一項に記載の物品。
前記複数のCu1+イオンが、前記ガラスマトリックス中に分散している赤銅鉱結晶を含むことを特徴とする実施形態32~37のいずれか一項に記載の物品。
前記無機材料が黒銅鉱を実質的に含まないことを特徴とする実施形態32~38のいずれか一項に記載の物品。
Al2O3が約5モルパーセント以下の量で存在することを特徴とする実施形態36に記載の物品。
前記組成物がAl2O3を実質的に含まないことを特徴とする実施形態36に記載の物品。
抗菌性物品の製造方法において:
ガラス組成物を溶融させて、複数のCu1+イオンおよびガラス相を含むガラスを形成するステップと;
前記ガラスから少なくとも1つの粒子または繊維を形成するステップと、
前記少なくとも1つの粒子または繊維をポリマー中に分散させて、充填されたポリマーを得るステップと;
前記充填されたポリマーが前記抗菌性物品を形成するステップと
を有してなることを特徴とする製造方法。
前記ガラス組成物が、モルパーセントの単位で:
約40~約70の範囲内のSiO2、
約0~約20の範囲内のAl2O3、
約10~約40の範囲内の銅含有酸化物、
約0~約15の範囲内のCaO、
約0~約15の範囲内のMgO、
約0~約25の範囲内のP2O5、
約0~約25の範囲内のB2O3、
約0~約20の範囲内のK2O、
約0~約5の範囲内のZnO、
約0~約20の範囲内のNa2O、
約0~約5の範囲内のFe2O3、および
場合により約0.1~約1の核剤
を含み、
前記銅含有酸化物の量がAl2O3の量よりも多いことを特徴とする実施形態42に記載の方法。
前記ポリマーが、熱可塑性ポリマー、ポリオレフィン、硬化させたポリマー、紫外線硬化またはUV硬化させたポリマー、ポリマーエマルジョン、溶剤系ポリマー、およびそれらの組合せを含むことを特徴とする実施形態42または実施形態43に記載の方法。
前記抗菌性物品が電子デバイスのハウジングを含むことを特徴とする実施形態42~44のいずれか一項に記載の方法。
前記抗菌性物品が:
EPA Test Method for Efficacy of Copper Alloy as a Sanitizer試験条件下で、黄色ブドウ球菌(Staphylococcus aureus)、エンテロバクター・アエロゲネス(Enterobacter aerogenes)、緑膿菌(Pseudomomas aeruginosa bacteria)、メチシリン耐性黄色ブドウ球菌(Methicillin Resistant Staphylococcus aureus)、および大腸菌(E.coli)のいずれか1つ以上の濃度の2対数減少以上、
JIS Z 2801(2000)試験条件または細菌用修正JIS Z 2801試験下で、黄色ブドウ球菌(Staphylococcus aureus)、エンテロバクター・アエロゲネス(Enterobacter aerogenes)、緑膿菌(Pseudomomas aeruginosa)、メチシリン耐性黄色ブドウ球菌(Methicillin Resistant Staphylococcus aureus)、および大腸菌(E.coli)のいずれか1つ以上の濃度の4対数減少以上、
ウイルス用修正JIS Z 2801試験下で、マウスノロウイルス(Murine Norovirus)の濃度の4対数減少以上
のいずれか1つ以上を示すことを特徴とする実施形態42~45のいずれか一項に記載の方法。
前記抗菌性物品が:
EPA Test Method for Efficacy of Copper Alloy as a Sanitizer試験条件下で、黄色ブドウ球菌(Staphylococcus aureus)、エンテロバクター・アエロゲネス(Enterobacter aerogenes)、緑膿菌(Pseudomomas aeruginosa bacteria)、メチシリン耐性黄色ブドウ球菌(Methicillin Resistant Staphylococcus aureus)、および大腸菌(E.coli)のいずれか1つ以上の濃度の2対数減少以上、
JIS Z 2801(2000)試験条件または細菌用修正JIS Z 2801試験下で、黄色ブドウ球菌(Staphylococcus aureus)、エンテロバクター・アエロゲネス(Enterobacter aerogenes)、緑膿菌(Pseudomomas aeruginosa)、メチシリン耐性黄色ブドウ球菌(Methicillin Resistant Staphylococcus aureus)、および大腸菌(E.coli)のいずれか1つ以上の濃度の4対数減少以上、
ウイルス用修正JIS Z 2801試験下で、マウスノロウイルス(Murine Norovirus)の濃度の4対数減少以上
のいずれか1つ以上を3か月以上の期間示すことを特徴とする実施形態42~46のいずれか一項に記載の方法。
Claims (10)
- ガラスを含む物品であって、前記ガラスが、
複数のCu1+イオンを含む赤銅鉱相と、
B2O3、P2O5およびR2Oの少なくとも1つを含む第1の相と、
SiO2を含む第2の相と
を含む抗菌性ガラスであって、
該ガラスが、Cu総量に対して、70重量%以上で前記複数のCu1+イオンおよび30重量%以下のCu 2+ イオンを含有し、Rは、K、Na、Li、RbおよびCsのいずれか1つ以上である、物品。 - ポリマー、モノマー、バインダー、溶媒またはそれらの組み合わせを含む担体をさらに含む、請求項1に記載の物品。
- 前記物品が建築構造物品である、請求項1または2に記載の物品。
- ガラスを含む物品であって、前記ガラスが、
複数のCu1+イオンを含む赤銅鉱相と、
B2O3、P2O5およびR2Oの少なくとも1つを含む第1の相と、
SiO2を含む第2の相と
を含む抗菌性ガラスであって、
該ガラス中の前記複数のCu1+イオンのCu総量に対する比は0.7以上であり、Rは、K、Na、Li、RbおよびCsのいずれか1つ以上であり、前記赤銅鉱相が5マイクロメートル(μm)以下の平均主要寸法を有する結晶を含む、物品。 - ポリマー、モノマー、バインダー、溶媒またはそれらの組み合わせを含む担体をさらに含む、請求項4に記載の物品。
- 前記ガラス中の前記複数のCu1+イオンのCu総量に対する比が0.8以上である、請求項4または5に記載の物品。
- 前記物品が建築構造物品である、請求項4~6のいずれかに記載の物品。
- ガラスを含む物品であって、前記ガラスが、
複数のCu1+イオンを含む赤銅鉱相と、
B2O3、P2O5およびR2Oの少なくとも1つを含む第1の相と、
SiO2を含む第2の相と
を含む抗菌性ガラスであって、
該ガラスが、深さ約5ナノメートル(nm)未満の表面部分を有し、該表面部分が複数の銅イオンを含み、該複数の銅イオンの少なくとも75%がCu1+であり、Rは、K、Na、Li、RbおよびCsのいずれか1つ以上である、物品。 - ポリマー、モノマー、バインダー、溶媒またはそれらの組み合わせを含む担体をさらに含む、請求項8に記載の物品。
- 前記物品が建築構造物品である、請求項8または9に記載の物品。
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