JP6035632B2 - ポリアミド酸繊維からポリイミド繊維への高速熱転化 - Google Patents

ポリアミド酸繊維からポリイミド繊維への高速熱転化 Download PDF

Info

Publication number
JP6035632B2
JP6035632B2 JP2013532899A JP2013532899A JP6035632B2 JP 6035632 B2 JP6035632 B2 JP 6035632B2 JP 2013532899 A JP2013532899 A JP 2013532899A JP 2013532899 A JP2013532899 A JP 2013532899A JP 6035632 B2 JP6035632 B2 JP 6035632B2
Authority
JP
Japan
Prior art keywords
temperature
polyamic acid
fiber
polyimide
nanoweb
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2013532899A
Other languages
English (en)
Japanese (ja)
Other versions
JP2013539824A (ja
JP2013539824A5 (enExample
Inventor
ティー ジョセフ デンズ
ティー ジョセフ デンズ
ラクシュミー クリシュナムールティ
ラクシュミー クリシュナムールティ
グレン エドワード シモンズ
グレン エドワード シモンズ
サイモン フリスク
サイモン フリスク
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Publication of JP2013539824A publication Critical patent/JP2013539824A/ja
Publication of JP2013539824A5 publication Critical patent/JP2013539824A5/ja
Application granted granted Critical
Publication of JP6035632B2 publication Critical patent/JP6035632B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/06—Flat membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/06—Organic material
    • B01D71/58—Other polymers having nitrogen in the main chain, with or without oxygen or carbon only
    • B01D71/62—Polycondensates having nitrogen-containing heterocyclic rings in the main chain
    • B01D71/64—Polyimides; Polyamide-imides; Polyester-imides; Polyamide acids or similar polyimide precursors
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D10/00—Physical treatment of artificial filaments or the like during manufacture, i.e. during a continuous production process before the filaments have been collected
    • D01D10/02—Heat treatment
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
    • D01F6/58—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products
    • D01F6/74—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products from polycondensates of cyclic compounds, e.g. polyimides, polybenzimidazoles
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01H—SPINNING OR TWISTING
    • D01H1/00—Spinning or twisting machines in which the product is wound-up continuously
    • D01H1/14—Details
    • D01H1/42—Guards or protectors for yarns or threads, e.g. separator plates, anti-ballooning devices
    • D—TEXTILES; PAPER
    • D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02J—FINISHING OR DRESSING OF FILAMENTS, YARNS, THREADS, CORDS, ROPES OR THE LIKE
    • D02J13/00—Heating or cooling the yarn, thread, cord, rope, or the like, not specific to any one of the processes provided for in this subclass
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/4326—Condensation or reaction polymers
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/4326—Condensation or reaction polymers
    • D04H1/4334—Polyamides
    • D04H1/4342—Aromatic polyamides
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/70—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres
    • D04H1/72—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged
    • D04H1/728—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged by electro-spinning
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00—Formation of filaments, threads, or the like
    • D01D5/0007—Electro-spinning

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Textile Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
  • Artificial Filaments (AREA)
  • Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
JP2013532899A 2010-10-07 2011-10-05 ポリアミド酸繊維からポリイミド繊維への高速熱転化 Expired - Fee Related JP6035632B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US12/899,770 2010-10-07
US12/899,770 US20110144297A1 (en) 2009-12-15 2010-10-07 Rapid thermal conversion of a polyamic acid fiber to a polyimide fiber
PCT/US2011/054863 WO2012047960A2 (en) 2010-10-07 2011-10-05 Rapid thermal conversion of a polyamic acid fiber to a polyimide fiber

Publications (3)

Publication Number Publication Date
JP2013539824A JP2013539824A (ja) 2013-10-28
JP2013539824A5 JP2013539824A5 (enExample) 2014-11-20
JP6035632B2 true JP6035632B2 (ja) 2016-11-30

Family

ID=45928587

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2013532899A Expired - Fee Related JP6035632B2 (ja) 2010-10-07 2011-10-05 ポリアミド酸繊維からポリイミド繊維への高速熱転化

Country Status (6)

Country Link
US (1) US20110144297A1 (enExample)
EP (1) EP2625322B1 (enExample)
JP (1) JP6035632B2 (enExample)
KR (1) KR20130115278A (enExample)
CN (1) CN103154335B (enExample)
WO (1) WO2012047960A2 (enExample)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102168317B (zh) * 2011-03-11 2012-07-25 北京化工大学 一种聚酰亚胺纤维的制备方法
US8679200B2 (en) 2011-11-18 2014-03-25 E I Du Pont De Nemours And Company Method for reducing self discharge in an electrochemical cell
WO2013181333A1 (en) * 2012-06-01 2013-12-05 E. I. Du Pont De Nemours And Company An electrochemical cell comprising a nanoweb comprising nanofibers of a cross-linked polyimide
US9090996B2 (en) * 2012-08-15 2015-07-28 E I Du Pont De Nemours And Company Multizone electroblowing process
CN103337595B (zh) * 2013-07-04 2016-04-06 上海和辉光电有限公司 柔性封装衬底及其制造方法和使用该衬底的oled封装方法
JP5946565B1 (ja) * 2015-06-23 2016-07-06 紘邦 張本 紡糸口金及び極細繊維製造装置
CN105040276B (zh) * 2015-06-23 2017-08-01 北京化工大学常州先进材料研究院 一种具有交联形貌的聚酰亚胺纤维膜及其制备方法
WO2017007302A2 (en) * 2015-07-06 2017-01-12 Universiti Putra Malaysia Post conditioning machine
CN105040512A (zh) * 2015-09-09 2015-11-11 长春高琦聚酰亚胺材料有限公司 一种聚酰亚胺纸模塑制品及其制备方法
US11077325B2 (en) 2016-04-01 2021-08-03 Dupont Safety & Construction, Inc. Flame and particulate resistant knit article
CN105734710A (zh) * 2016-05-06 2016-07-06 江苏奥神新材料股份有限公司 一种有色聚酰亚胺纤维的制备方法
EP3491178B1 (en) * 2017-01-06 2019-11-20 SABIC Global Technologies B.V. Apparatus for continuous needleless electrospinning a nanoscale or submicron scale polymer fiber web onto a substrate
CN106958047B (zh) * 2017-04-06 2019-10-25 中国科学院长春应用化学研究所 一种热酰亚胺化制备聚酰亚胺纤维的方法
US20190330766A1 (en) * 2018-04-28 2019-10-31 Dennis Joseph Steibel, JR. Apparatus for removing moisture from a section of polymer filament
CN110681266B (zh) * 2018-07-06 2021-11-30 中国石油化工股份有限公司 分离非质子极性溶剂中小分子溶剂的方法
CN109509678A (zh) * 2018-11-22 2019-03-22 漳州雅宝电子有限公司 一种熔点为236±2℃的耐高温热敏材料
CN115989457A (zh) 2020-09-25 2023-04-18 富士胶片株式会社 固化物的制造方法、层叠体的制造方法及半导体器件的制造方法
CN119663548A (zh) * 2024-12-17 2025-03-21 井冈山大学 一种萘基聚酰亚胺复合柔性纳米纤维材料及其制备方法和应用

Family Cites Families (31)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB903272A (en) 1959-04-01 1962-08-15 Du Pont Method of preparing polyimides
US3814719A (en) * 1972-05-01 1974-06-04 Ciba Geigy Corp Zeta-triazine-imide copolymers
US4167620A (en) * 1978-02-01 1979-09-11 Standard Oil Company (Indiana) Method for heat treating shaped articles of amide-imide or amic acid polymers
US4874368A (en) * 1988-07-25 1989-10-17 Micromedics, Inc. Fibrin glue delivery system
JPH02234911A (ja) * 1988-11-07 1990-09-18 Mitsui Toatsu Chem Inc ポリイミド繊維の製造方法
CA2002147A1 (en) * 1988-11-07 1990-05-07 Shuichi Morikawa Production process for polyimide fibers
JPH0314617A (ja) * 1989-06-12 1991-01-23 Asahi Chem Ind Co Ltd 高強度、高弾性率ポリイミド成形物の製造方法
US5374708A (en) * 1989-12-22 1994-12-20 Mitsui Toatsu Chemicals, Incorporated Formed polyimide article
US5089360A (en) * 1990-02-08 1992-02-18 Tonen Chemical Corporation High-strength non-woven fabric, method of producing same and battery separator constituted thereby
JP2626827B2 (ja) * 1990-03-15 1997-07-02 宇部興産株式会社 ポリイミド延伸成形体及びその製造法
US5367046A (en) * 1992-04-10 1994-11-22 The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration Low dielectric polyimide fibers
US5518779A (en) * 1992-12-16 1996-05-21 Industrial Technology Research Institute Forming copper clad laminates
KR0161313B1 (ko) * 1994-10-31 1999-01-15 강박광 폴리이미드 아미 에스테르 화합물 및 그 제조방법
EP0751168B1 (en) * 1995-06-28 1999-02-10 Mitsui Chemicals, Inc. Linear polyamic acid, linear polyimide and thermoset polyimide
JPH11269268A (ja) * 1998-03-20 1999-10-05 Mitsui Chem Inc 線状ポリアミド酸、線状ポリイミド及び熱硬化性ポリイミド
JP2000071268A (ja) * 1998-08-31 2000-03-07 Du Pont Toray Co Ltd ポリイミドフィルムおよびその製造方法
ATA49899A (de) * 1999-03-19 2002-06-15 Immuno Ag Verfahren und vorrichtung zum mischen von komponenten
CN1216092C (zh) * 1999-09-24 2005-08-24 液态空气-乔治克罗德方法研究监督及咨询股份有限公司 新的聚酰亚胺酰胺酸盐以及由此形成的聚酰亚胺膜
WO2001083591A1 (en) * 2000-04-28 2001-11-08 Mitsui Chemicals, Inc. Polyimides and polyamic acids
JP4390028B2 (ja) * 2000-10-04 2009-12-24 日産化学工業株式会社 ポジ型感光性ポリイミド樹脂組成物
EP1229066A1 (en) * 2001-02-05 2002-08-07 Rolic AG Photoactive polymer
US20040166311A1 (en) * 2003-02-25 2004-08-26 Clemson University Electrostatic spinning of aromatic polyamic acid
JP2004308031A (ja) * 2003-04-03 2004-11-04 Teijin Ltd ポリアミド酸不織布、それから得られるポリイミド不織布およびそれらの製造方法
WO2006042161A2 (en) * 2004-10-07 2006-04-20 E.I. Dupont De Nemours And Company Polysaccharide-based polymer tissue adhesive for medical use
JP2008002011A (ja) * 2006-06-22 2008-01-10 Toyobo Co Ltd ポリイミド不織布およびその製造方法
JP2009203314A (ja) * 2008-02-27 2009-09-10 Toyobo Co Ltd ポリイミド繊維補強熱可塑性樹脂板状体およびその製造方法
CA2640517A1 (en) * 2008-05-19 2009-11-19 Industry-University Cooperation Foundation, Hanyang University Polyamic acids dope composition, preparation method of hollow fiber using the same and hollow fiber prepared therefrom
JP2010077565A (ja) * 2008-09-26 2010-04-08 Kaneka Corp ポリイミド繊維及びその利用、並びに当該ポリイミド繊維の製造方法。
JP5429101B2 (ja) * 2009-11-25 2014-02-26 宇部興産株式会社 高耐熱性ポリイミド微細繊維の製造方法、高耐熱性ポリイミド微細繊維及び該ポリイミド微細繊維からなる不織布
US20110139331A1 (en) * 2009-12-15 2011-06-16 E. I. Du Pont De Nemours And Company Method for increasing the strength and solvent resistance of polyimide nanowebs
JP6003261B2 (ja) * 2012-06-12 2016-10-05 宇部興産株式会社 ポリイミド繊維の製造方法

Also Published As

Publication number Publication date
EP2625322A4 (en) 2017-04-19
EP2625322A2 (en) 2013-08-14
JP2013539824A (ja) 2013-10-28
EP2625322B1 (en) 2019-01-09
US20110144297A1 (en) 2011-06-16
KR20130115278A (ko) 2013-10-21
CN103154335B (zh) 2016-08-24
CN103154335A (zh) 2013-06-12
WO2012047960A2 (en) 2012-04-12
WO2012047960A3 (en) 2012-08-02

Similar Documents

Publication Publication Date Title
JP6035632B2 (ja) ポリアミド酸繊維からポリイミド繊維への高速熱転化
CN101473080B (zh) 聚酰亚胺无纺布及其制造方法
JP5720574B2 (ja) 着色ポリイミド成形体及びその製造方法
CN101925398B (zh) 聚酰亚胺气体分离膜和气体分离方法
JP4189569B2 (ja) 炭素フィルムの製造方法
WO2011125988A1 (ja) 多孔質ポリイミド膜及びその製造方法
CN109563300B (zh) 多孔质聚酰亚胺膜的制造方法及由该方法制造的多孔质聚酰亚胺膜
Cheng et al. High‐strength and high‐toughness polyimide nanofibers: Synthesis and characterization
Oktay et al. Superhydrophobic behavior of polyimide–siloxane mats produced by electrospinning
JP2011132651A (ja) 高耐熱性ポリイミド微細繊維の製造方法、高耐熱性ポリイミド微細繊維及び該ポリイミド微細繊維からなる不織布
JP2003013351A (ja) 耐熱性不織布及びバインダ−樹脂
JP6917027B2 (ja) ポリイミド繊維およびその製造方法
JP5041271B2 (ja) 加熱硬化性溶液組成物および未硬化樹脂複合体
JP7634675B2 (ja) グラファイトシート用ポリイミドフィルム、その製造方法およびそれから製造されたグラファイトシート
JP2004255845A (ja) ガスバリアー性ポリイミドフィルムおよびそれを用いた金属積層体
JP6003261B2 (ja) ポリイミド繊維の製造方法
TWI690633B (zh) 熔噴不織布
WO2005082594A1 (ja) 合成樹脂フィルムの製造方法および合成樹脂フィルム
Nesterova et al. Imide Containing Polymers as Promising Filtration Nonwovens
JP4075221B2 (ja) ポリイミド多孔質フィルムの製造方法、ポリイミド多孔質フィルム、フィルター用多孔質フィルムおよびフィルター
Xu et al. Preparation and Properties of PBO Nanofiber Membranes via Electrospinning and Thermal Conversion
JP2017070215A (ja) 細胞培養用フィルム及び細胞培養用フィルムの製造方法
JP2024015908A (ja) ポリイミド前駆体溶液及びポリイミド成形体
JP2004168858A (ja) ポリイミドウィスカー及びその製造方法

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20141003

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20141003

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20151013

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20151102

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20160201

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20160404

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20161003

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20161013

R150 Certificate of patent or registration of utility model

Ref document number: 6035632

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

S111 Request for change of ownership or part of ownership

Free format text: JAPANESE INTERMEDIATE CODE: R313113

R350 Written notification of registration of transfer

Free format text: JAPANESE INTERMEDIATE CODE: R350

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

LAPS Cancellation because of no payment of annual fees