CN103154335B - 聚酰胺酸纤维至聚酰亚胺纤维的快速热转化 - Google Patents

聚酰胺酸纤维至聚酰亚胺纤维的快速热转化 Download PDF

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Publication number
CN103154335B
CN103154335B CN201180047942.XA CN201180047942A CN103154335B CN 103154335 B CN103154335 B CN 103154335B CN 201180047942 A CN201180047942 A CN 201180047942A CN 103154335 B CN103154335 B CN 103154335B
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CN
China
Prior art keywords
polyamic acid
temperature
fibers
fiber
polyimide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201180047942.XA
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English (en)
Chinese (zh)
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CN103154335A (zh
Inventor
T.J.丹尼斯
L.克里什纳墨菲
G.E.西蒙斯
S.弗里斯克
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DuPont Safety and Construction Inc
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EI Du Pont de Nemours and Co
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Publication of CN103154335A publication Critical patent/CN103154335A/zh
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Expired - Fee Related legal-status Critical Current
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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D69/00Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D69/00Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/06Flat membranes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D71/00Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/06Organic material
    • B01D71/58Other polymers having nitrogen in the main chain, with or without oxygen or carbon only
    • B01D71/62Polycondensates having nitrogen-containing heterocyclic rings in the main chain
    • B01D71/64Polyimides; Polyamide-imides; Polyester-imides; Polyamide acids or similar polyimide precursors
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D10/00Physical treatment of artificial filaments or the like during manufacture, i.e. during a continuous production process before the filaments have been collected
    • D01D10/02Heat treatment
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F6/00Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
    • D01F6/58Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products
    • D01F6/74Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products from polycondensates of cyclic compounds, e.g. polyimides, polybenzimidazoles
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01HSPINNING OR TWISTING
    • D01H1/00Spinning or twisting machines in which the product is wound-up continuously
    • D01H1/14Details
    • D01H1/42Guards or protectors for yarns or threads, e.g. separator plates, anti-ballooning devices
    • DTEXTILES; PAPER
    • D02YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02JFINISHING OR DRESSING OF FILAMENTS, YARNS, THREADS, CORDS, ROPES OR THE LIKE
    • D02J13/00Heating or cooling the yarn, thread, cord, rope, or the like, not specific to any one of the processes provided for in this subclass
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/4326Condensation or reaction polymers
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/4326Condensation or reaction polymers
    • D04H1/4334Polyamides
    • D04H1/4342Aromatic polyamides
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/70Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres
    • D04H1/72Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged
    • D04H1/728Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged by electro-spinning
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/0007Electro-spinning

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Textile Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
  • Artificial Filaments (AREA)
  • Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
CN201180047942.XA 2010-10-07 2011-10-05 聚酰胺酸纤维至聚酰亚胺纤维的快速热转化 Expired - Fee Related CN103154335B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US12/899,770 US20110144297A1 (en) 2009-12-15 2010-10-07 Rapid thermal conversion of a polyamic acid fiber to a polyimide fiber
US12/899770 2010-10-07
PCT/US2011/054863 WO2012047960A2 (en) 2010-10-07 2011-10-05 Rapid thermal conversion of a polyamic acid fiber to a polyimide fiber

Publications (2)

Publication Number Publication Date
CN103154335A CN103154335A (zh) 2013-06-12
CN103154335B true CN103154335B (zh) 2016-08-24

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CN201180047942.XA Expired - Fee Related CN103154335B (zh) 2010-10-07 2011-10-05 聚酰胺酸纤维至聚酰亚胺纤维的快速热转化

Country Status (6)

Country Link
US (1) US20110144297A1 (enExample)
EP (1) EP2625322B1 (enExample)
JP (1) JP6035632B2 (enExample)
KR (1) KR20130115278A (enExample)
CN (1) CN103154335B (enExample)
WO (1) WO2012047960A2 (enExample)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102168317B (zh) * 2011-03-11 2012-07-25 北京化工大学 一种聚酰亚胺纤维的制备方法
US8679200B2 (en) 2011-11-18 2014-03-25 E I Du Pont De Nemours And Company Method for reducing self discharge in an electrochemical cell
WO2013181333A1 (en) * 2012-06-01 2013-12-05 E. I. Du Pont De Nemours And Company An electrochemical cell comprising a nanoweb comprising nanofibers of a cross-linked polyimide
US9090996B2 (en) * 2012-08-15 2015-07-28 E I Du Pont De Nemours And Company Multizone electroblowing process
CN103337595B (zh) * 2013-07-04 2016-04-06 上海和辉光电有限公司 柔性封装衬底及其制造方法和使用该衬底的oled封装方法
JP5946565B1 (ja) * 2015-06-23 2016-07-06 紘邦 張本 紡糸口金及び極細繊維製造装置
CN105040276B (zh) * 2015-06-23 2017-08-01 北京化工大学常州先进材料研究院 一种具有交联形貌的聚酰亚胺纤维膜及其制备方法
WO2017007302A2 (en) * 2015-07-06 2017-01-12 Universiti Putra Malaysia Post conditioning machine
CN105040512A (zh) * 2015-09-09 2015-11-11 长春高琦聚酰亚胺材料有限公司 一种聚酰亚胺纸模塑制品及其制备方法
US11077325B2 (en) 2016-04-01 2021-08-03 Dupont Safety & Construction, Inc. Flame and particulate resistant knit article
CN105734710A (zh) * 2016-05-06 2016-07-06 江苏奥神新材料股份有限公司 一种有色聚酰亚胺纤维的制备方法
EP3491178B1 (en) * 2017-01-06 2019-11-20 SABIC Global Technologies B.V. Apparatus for continuous needleless electrospinning a nanoscale or submicron scale polymer fiber web onto a substrate
CN106958047B (zh) * 2017-04-06 2019-10-25 中国科学院长春应用化学研究所 一种热酰亚胺化制备聚酰亚胺纤维的方法
US20190330766A1 (en) * 2018-04-28 2019-10-31 Dennis Joseph Steibel, JR. Apparatus for removing moisture from a section of polymer filament
CN110681266B (zh) * 2018-07-06 2021-11-30 中国石油化工股份有限公司 分离非质子极性溶剂中小分子溶剂的方法
CN109509678A (zh) * 2018-11-22 2019-03-22 漳州雅宝电子有限公司 一种熔点为236±2℃的耐高温热敏材料
CN115989457A (zh) 2020-09-25 2023-04-18 富士胶片株式会社 固化物的制造方法、层叠体的制造方法及半导体器件的制造方法
CN119663548A (zh) * 2024-12-17 2025-03-21 井冈山大学 一种萘基聚酰亚胺复合柔性纳米纤维材料及其制备方法和应用

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5708128A (en) * 1995-06-28 1998-01-13 Mitsui Toatsu Chemicals, Inc. Linear polyamic acid, linear polyimide and thermoset polyimide
US20030164090A1 (en) * 1999-09-24 2003-09-04 Yong Ding Novel polyimide amic acid salts and polyimide membranes formed therefrom
CN1468391A (zh) * 2000-10-04 2004-01-14 �ղ���ѧ��ҵ��ʽ���� 正感光性聚酰亚胺树脂组合物
CN1491251A (zh) * 2001-02-05 2004-04-21 光活性聚合物
CN1148400C (zh) * 2000-04-28 2004-05-05 三井化学株式会社 聚酰亚胺和聚酰胺酸
US20090286904A1 (en) * 2008-05-19 2009-11-19 Industry-University Cooperation Foundation, Hanyang University Polyamic acids dope composition, preparation method of hollow fiber using the same and hollow fiber prepared therefrom

Family Cites Families (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB903272A (en) 1959-04-01 1962-08-15 Du Pont Method of preparing polyimides
US3814719A (en) * 1972-05-01 1974-06-04 Ciba Geigy Corp Zeta-triazine-imide copolymers
US4167620A (en) * 1978-02-01 1979-09-11 Standard Oil Company (Indiana) Method for heat treating shaped articles of amide-imide or amic acid polymers
US4874368A (en) * 1988-07-25 1989-10-17 Micromedics, Inc. Fibrin glue delivery system
JPH02234911A (ja) * 1988-11-07 1990-09-18 Mitsui Toatsu Chem Inc ポリイミド繊維の製造方法
CA2002147A1 (en) * 1988-11-07 1990-05-07 Shuichi Morikawa Production process for polyimide fibers
JPH0314617A (ja) * 1989-06-12 1991-01-23 Asahi Chem Ind Co Ltd 高強度、高弾性率ポリイミド成形物の製造方法
US5374708A (en) * 1989-12-22 1994-12-20 Mitsui Toatsu Chemicals, Incorporated Formed polyimide article
US5089360A (en) * 1990-02-08 1992-02-18 Tonen Chemical Corporation High-strength non-woven fabric, method of producing same and battery separator constituted thereby
JP2626827B2 (ja) * 1990-03-15 1997-07-02 宇部興産株式会社 ポリイミド延伸成形体及びその製造法
US5367046A (en) * 1992-04-10 1994-11-22 The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration Low dielectric polyimide fibers
US5518779A (en) * 1992-12-16 1996-05-21 Industrial Technology Research Institute Forming copper clad laminates
KR0161313B1 (ko) * 1994-10-31 1999-01-15 강박광 폴리이미드 아미 에스테르 화합물 및 그 제조방법
JPH11269268A (ja) * 1998-03-20 1999-10-05 Mitsui Chem Inc 線状ポリアミド酸、線状ポリイミド及び熱硬化性ポリイミド
JP2000071268A (ja) * 1998-08-31 2000-03-07 Du Pont Toray Co Ltd ポリイミドフィルムおよびその製造方法
ATA49899A (de) * 1999-03-19 2002-06-15 Immuno Ag Verfahren und vorrichtung zum mischen von komponenten
US20040166311A1 (en) * 2003-02-25 2004-08-26 Clemson University Electrostatic spinning of aromatic polyamic acid
JP2004308031A (ja) * 2003-04-03 2004-11-04 Teijin Ltd ポリアミド酸不織布、それから得られるポリイミド不織布およびそれらの製造方法
WO2006042161A2 (en) * 2004-10-07 2006-04-20 E.I. Dupont De Nemours And Company Polysaccharide-based polymer tissue adhesive for medical use
JP2008002011A (ja) * 2006-06-22 2008-01-10 Toyobo Co Ltd ポリイミド不織布およびその製造方法
JP2009203314A (ja) * 2008-02-27 2009-09-10 Toyobo Co Ltd ポリイミド繊維補強熱可塑性樹脂板状体およびその製造方法
JP2010077565A (ja) * 2008-09-26 2010-04-08 Kaneka Corp ポリイミド繊維及びその利用、並びに当該ポリイミド繊維の製造方法。
JP5429101B2 (ja) * 2009-11-25 2014-02-26 宇部興産株式会社 高耐熱性ポリイミド微細繊維の製造方法、高耐熱性ポリイミド微細繊維及び該ポリイミド微細繊維からなる不織布
US20110139331A1 (en) * 2009-12-15 2011-06-16 E. I. Du Pont De Nemours And Company Method for increasing the strength and solvent resistance of polyimide nanowebs
JP6003261B2 (ja) * 2012-06-12 2016-10-05 宇部興産株式会社 ポリイミド繊維の製造方法

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5708128A (en) * 1995-06-28 1998-01-13 Mitsui Toatsu Chemicals, Inc. Linear polyamic acid, linear polyimide and thermoset polyimide
US20030164090A1 (en) * 1999-09-24 2003-09-04 Yong Ding Novel polyimide amic acid salts and polyimide membranes formed therefrom
CN1148400C (zh) * 2000-04-28 2004-05-05 三井化学株式会社 聚酰亚胺和聚酰胺酸
CN1468391A (zh) * 2000-10-04 2004-01-14 �ղ���ѧ��ҵ��ʽ���� 正感光性聚酰亚胺树脂组合物
CN1491251A (zh) * 2001-02-05 2004-04-21 光活性聚合物
US20090286904A1 (en) * 2008-05-19 2009-11-19 Industry-University Cooperation Foundation, Hanyang University Polyamic acids dope composition, preparation method of hollow fiber using the same and hollow fiber prepared therefrom

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
共聚与机械共混对PMDA/ODA型聚酰亚胺性能的影响;杨建伟等;《应用化工》;20090328;第38卷(第3期);第363-365页 *
静电纺丝法制备聚酰亚胺纳米纤维;王兆礼等;《绝缘材料》;20061220;第39卷(第6期);第8页第2.3节 *

Also Published As

Publication number Publication date
EP2625322A4 (en) 2017-04-19
JP6035632B2 (ja) 2016-11-30
EP2625322A2 (en) 2013-08-14
JP2013539824A (ja) 2013-10-28
EP2625322B1 (en) 2019-01-09
US20110144297A1 (en) 2011-06-16
KR20130115278A (ko) 2013-10-21
CN103154335A (zh) 2013-06-12
WO2012047960A2 (en) 2012-04-12
WO2012047960A3 (en) 2012-08-02

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