FI86719B - Foerfarande foer framstaellning av 2-oxo-1,3-dioxolaner. - Google Patents

Foerfarande foer framstaellning av 2-oxo-1,3-dioxolaner. Download PDF

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Publication number
FI86719B
FI86719B FI863298A FI863298A FI86719B FI 86719 B FI86719 B FI 86719B FI 863298 A FI863298 A FI 863298A FI 863298 A FI863298 A FI 863298A FI 86719 B FI86719 B FI 86719B
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Finland
Prior art keywords
process according
epoxide
parts
reaction
group
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FI863298A
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English (en)
Finnish (fi)
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FI86719C (sv
FI863298A0 (fi
FI863298A (fi
Inventor
Gerhard Brindoepke
Manfred Marten
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Hoechst Ag
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Publication of FI863298A0 publication Critical patent/FI863298A0/fi
Publication of FI863298A publication Critical patent/FI863298A/fi
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Publication of FI86719B publication Critical patent/FI86719B/fi
Publication of FI86719C publication Critical patent/FI86719C/sv

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
    • C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
    • C07D317/32—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D317/34—Oxygen atoms
    • C07D317/36—Alkylene carbonates; Substituted alkylene carbonates

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Epoxy Compounds (AREA)
  • Epoxy Resins (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Secondary Cells (AREA)

Claims (11)

1. Förfarande för framställning av 2-oxo-l,3-dioxo-laner genom att omsätta epoxider med koldioxid i närvaro 5 av en katalysator och eventuellt i närvaro av en kokataly-sator och ett inert lösningsmedel, känneteck-n a t därav, att reaktionen utförs vid en temperatur av 40 - 180 °C och under normaltryck eller nägot förhöjt tryck i närvaro av minst en katalysator, som är trifenyl-10 fosfan, tritolylfosfan, diazabicyklo[2.2.2]oktan, 4-dime-tylaminopyridin, 4-(1-pyrrolidinyl)pyridin, amidin, imid-azol eller en alkyl-, aryl- eller aralkyl-substitutions-produkt därav.
2. Förfarande enligt patentkravet 1, k ä n n e -15 tecknat därav, att reaktionen utförs under ett tryck av 1 - 5 bar.
3. Förfarande enligt patentkravet 1 eller 2, k ä n-netecknat därav, att man använder 0,02 - 10 vikt-% katalysator beräknat pä epoxidkomponenten. 20
4. Förfarande enligt nägot av patentkraven 1-3, kännetecknat därav, att reaktionen av epoxid-föreningen med koldioxid utförs endast delvis.
5. Förfarande enligt nägot av patentkraven 1-4, kännetecknat därav, att som imidazol används 25 1-metyl-, 2-metyl- och/eller 2-etyl-4-metyl-imidazol.
6. Förfarande enligt nägot av patentkraven 1-5, kännetecknat därav, att ytterligare används 0,1 - 10 vikt-% kokatalysatorer beräknat pä epoxidkomponenten . 30
7. Förfarande enligt nägot av patentkraven 1-6, kännetecknat därav, att som kokatalysator används natrium- och/eller kaliumjodid.
8. Förfarande enligt nägot av de föregäende patentkraven, kännetecknat därav, att epoxidföre-35 ningarna innehäller minst en terminal 1,2-epoxigrupp. 2i 86719
9. Förfarande enligt patentkravet 8, känne- t e c k n a t därav, att som epoxidföreningar används alifatiska epoxider, som innehäller minst 6 kolatomer, glycidol eller en epihalogenhydrin med formeln (2), 5 Z X-CH0-C-CH„ (2) 2 \</ 10 där Z är en väteatom eller en metyl- eller etylgrupp, och X är en halogenatom eller en OH-grupp.
10. Förfarande enligt patentkravet 8, känne-t e c k n a t därav, att som epoxidföreningar används sä-dana epoxider, som innehäller i medeltal minst en substi- 15 tuerad eller icke-substituerad glycidyletergrupp med formeln (3), Z -0-CHo-C-CH„ (3) 2 \ / 2 20 0 eller en substituerad eller icke-substituerad glycidyles-tergrupp med formeln (4),
25 Z l -OC-O-CH^-C-CH0 (4) 2 varvid Z i bäda formlerna betecknar samma som ovan, och 30 ytterligare epoxiderade, mängfaldigt omättade föreningar och epoxider innehällande amid- eller uretangrupper.
11. Förfarande enligt nägot av patentkraven 8 - 10, kännetecknat därav, att som epoxidföreningar används en polyglycidyleter, plasticerade epoxihartser, 35 som innehäller terminals epoxidgrupper, eller glycidylest-rar av mättade eller etyleniskt omättade (poly)karboxylsy-ror.
FI863298A 1985-08-16 1986-08-14 Förfarande för framställning av 2-oxo-1,3-dioxolaner FI86719C (sv)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE3529263 1985-08-16
DE19853529263 DE3529263A1 (de) 1985-08-16 1985-08-16 Verfahren zur herstellung von 2-oxo-1,3-dioxolanen

Publications (4)

Publication Number Publication Date
FI863298A0 FI863298A0 (fi) 1986-08-14
FI863298A FI863298A (fi) 1987-02-17
FI86719B true FI86719B (fi) 1992-06-30
FI86719C FI86719C (sv) 1992-10-12

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Family Applications (1)

Application Number Title Priority Date Filing Date
FI863298A FI86719C (sv) 1985-08-16 1986-08-14 Förfarande för framställning av 2-oxo-1,3-dioxolaner

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US (1) US4892954A (sv)
EP (1) EP0212409B1 (sv)
JP (1) JP2565875B2 (sv)
KR (1) KR940008751B1 (sv)
CN (1) CN1020729C (sv)
AR (1) AR242201A1 (sv)
AT (1) ATE51225T1 (sv)
AU (1) AU585385B2 (sv)
BR (1) BR8603901A (sv)
CA (1) CA1334851C (sv)
DE (2) DE3529263A1 (sv)
DK (1) DK164864C (sv)
ES (1) ES2000286A6 (sv)
FI (1) FI86719C (sv)
MX (1) MX170907B (sv)
NO (1) NO863302L (sv)
PT (1) PT83209B (sv)
ZA (1) ZA866149B (sv)

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AU585385B2 (en) 1989-06-15
EP0212409B1 (de) 1990-03-21
DK387386A (da) 1987-02-17
AR242201A1 (es) 1993-03-31
EP0212409A3 (en) 1987-10-21
BR8603901A (pt) 1987-03-24
CA1334851C (en) 1995-03-21
MX170907B (es) 1993-09-22
KR870002117A (ko) 1987-03-30
AU6150686A (en) 1987-02-19
ATE51225T1 (de) 1990-04-15
NO863302D0 (no) 1986-08-15
PT83209A (en) 1986-09-01
FI86719C (sv) 1992-10-12
FI863298A0 (fi) 1986-08-14
US4892954A (en) 1990-01-09
ZA866149B (en) 1987-04-29
CN86105205A (zh) 1987-02-11
JPS6245584A (ja) 1987-02-27
ES2000286A6 (es) 1988-02-01
DK164864B (da) 1992-08-31
DK387386D0 (da) 1986-08-14
KR940008751B1 (ko) 1994-09-26
EP0212409A2 (de) 1987-03-04
NO863302L (no) 1987-02-17
DE3529263A1 (de) 1987-02-19
JP2565875B2 (ja) 1996-12-18
DK164864C (da) 1993-01-18
DE3669717D1 (de) 1990-04-26
FI863298A (fi) 1987-02-17
CN1020729C (zh) 1993-05-19
PT83209B (pt) 1989-03-30

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