FI113764B - Menetelmä heterosyklisten yhdisteiden sulfinyloimiseksi - Google Patents

Menetelmä heterosyklisten yhdisteiden sulfinyloimiseksi Download PDF

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Publication number
FI113764B
FI113764B FI950800A FI950800A FI113764B FI 113764 B FI113764 B FI 113764B FI 950800 A FI950800 A FI 950800A FI 950800 A FI950800 A FI 950800A FI 113764 B FI113764 B FI 113764B
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FI
Finland
Prior art keywords
eller
group
het
alkyl
med
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FI950800A
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English (en)
Finnish (fi)
Swedish (sv)
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FI950800A (fi
FI950800A0 (fi
Inventor
Roy Pierre Le
Virginie Pevere
Michel Casado
Original Assignee
Rhone Poulenc Agrochimie
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Publication date
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Application filed by Rhone Poulenc Agrochimie filed Critical Rhone Poulenc Agrochimie
Publication of FI950800A0 publication Critical patent/FI950800A0/fi
Publication of FI950800A publication Critical patent/FI950800A/fi
Application granted granted Critical
Publication of FI113764B publication Critical patent/FI113764B/fi

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom
    • C07D231/20—One oxygen atom attached in position 3 or 5
    • C07D231/22—One oxygen atom attached in position 3 or 5 with aryl radicals attached to ring nitrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
    • C07D233/66—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D233/88—Nitrogen atoms, e.g. allantoin
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/38—Nitrogen atoms
    • C07D231/40—Acylated on said nitrogen atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/44—Oxygen and nitrogen or sulfur and nitrogen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pyrrole Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Coloring (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Cephalosporin Compounds (AREA)
FI950800A 1994-02-22 1995-02-21 Menetelmä heterosyklisten yhdisteiden sulfinyloimiseksi FI113764B (fi)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR9402222A FR2716453B1 (fr) 1994-02-22 1994-02-22 Procédé de sulfinylation de composés hétérocycliques.
FR9402222 1994-02-22

Publications (3)

Publication Number Publication Date
FI950800A0 FI950800A0 (fi) 1995-02-21
FI950800A FI950800A (fi) 1995-08-23
FI113764B true FI113764B (fi) 2004-06-15

Family

ID=9460460

Family Applications (1)

Application Number Title Priority Date Filing Date
FI950800A FI113764B (fi) 1994-02-22 1995-02-21 Menetelmä heterosyklisten yhdisteiden sulfinyloimiseksi

Country Status (24)

Country Link
US (1) US5618945A (cs)
EP (1) EP0668269B1 (cs)
JP (3) JP3963965B2 (cs)
KR (1) KR100370990B1 (cs)
CN (1) CN1056833C (cs)
AT (1) ATE218127T1 (cs)
AU (1) AU678876B2 (cs)
BR (1) BR9500858A (cs)
CA (1) CA2143135C (cs)
CZ (1) CZ294640B6 (cs)
DE (1) DE69526815T2 (cs)
DK (1) DK0668269T3 (cs)
ES (1) ES2173932T3 (cs)
FI (1) FI113764B (cs)
FR (1) FR2716453B1 (cs)
HU (1) HU214283B (cs)
IL (1) IL112708A (cs)
PL (1) PL183151B1 (cs)
PT (1) PT668269E (cs)
RO (1) RO113639B1 (cs)
RU (1) RU2136665C1 (cs)
SK (1) SK282510B6 (cs)
UA (1) UA44226C2 (cs)
ZA (1) ZA951468B (cs)

Families Citing this family (31)

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KR100500181B1 (ko) * 1997-04-07 2005-07-12 니혼노야쿠가부시키가이샤 피라졸 유도체, 이의 제조방법, 중간체 및 이를 유효 성분으로서 함유하는 유해 생물 방제제
FR2784101B1 (fr) * 1998-09-14 2000-11-17 Rhodia Chimie Sa Procede de condensation de derive(s) aromatique(s) et d'un derive sulfinique dont la chaine carbonee est attachee a la fonction sulfinique par un atome de carbone perhalogene
GB9907458D0 (en) * 1999-03-31 1999-05-26 Rhone Poulenc Agrochimie Processes for preparing pesticidal intermediates
MXPA01013211A (es) 1999-06-29 2002-08-12 Mitsubishi Chem Corp Derivados de pirazol y procedimiento para producir los mismos, pesticidas que contienen los mismos como el ingrediente activo.
TR200202806T2 (tr) 1999-10-22 2003-03-21 Aventis Cropscience Sa 4-Triflorometilsulfinilpirazol türevi hazırlama süreci
EP1331222A1 (en) * 2002-01-28 2003-07-30 Virbac S.A. Environment friendly reagents and process for halogenoalkylsulfinylation of organic compounds
US20060182808A1 (en) * 2003-04-29 2006-08-17 Akzo Nobel N.V. Antisolvent solidification process
AU2005223483B2 (en) * 2004-03-18 2009-04-23 Zoetis Llc N-(1-arylpyrazol-4l)sulfonamides and their use as parasiticides
WO2007069254A2 (en) 2005-12-14 2007-06-21 Makhteshim Chemical Works Ltd. POLYMORPHS AND AMORPHOUS FORMS OF 5-AMINO-l-[2,6- DICHLORO-4-(TRIFLUOROMETHYL)PHENYL]-4- [(TRIFLUOROMETHYL)SULFINYL]-IH-PYRAZOLE-3-CARBONITRILE
CN101168529B (zh) * 2006-10-24 2011-03-23 温州大学 氟虫腈、乙虫腈及其衍生物的合成方法
AU2007316639B2 (en) 2006-11-10 2012-12-20 Basf Se Crystalline modification of fipronil
UA95991C2 (ru) 2006-11-10 2011-09-26 Басф Се Кристаллическая модификация v фипронила, способ ее получения, применения, пестицидна или паразитицидная композиция, способ контроля вредителей, способ защиты растения от заражения или нападения вредителей, способ защиты семян и способ лечения, контроля, предотвращения или защиты животных от заражения или инфекции паразитами
JP5877624B2 (ja) 2006-11-10 2016-03-08 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ フィプロニルの結晶変態
UA110598C2 (uk) 2006-11-10 2016-01-25 Басф Се Спосіб одержання кристалічної модифікації фіпронілу
NZ576593A (en) * 2006-11-10 2011-12-22 Basf Se Process for the sulfinylation of a pyrazole derivative
CA2667559A1 (en) 2006-11-10 2008-05-15 Basf Se Process for the sulfinylation of a pyrazole derivative
CA2667565A1 (en) * 2006-11-10 2008-05-15 Basf Se Process for the sulfinylation of a pyrazole derivative
US7378547B1 (en) 2006-11-28 2008-05-27 E.I. Du Pont De Nemours And Company Process for the synthesis of hydroxy aromatic acids
FR2925493B1 (fr) * 2007-12-19 2011-09-30 Vetoquinol Procede de preparation du fipronil et d'analogues de celui-ci.
BRPI0919577A2 (pt) * 2008-10-02 2015-12-08 Basf Se processos para purificar e para preparar ácido trifluorometanossulfínico, e, para preparar fipronila.
WO2012095871A2 (en) 2011-01-14 2012-07-19 Keki Hormusji Gharda Polymorphism in 5-amino- 1 -(2,6-dichloro-4- trifluoromethylphenyl)-3-cyano-4-trifluoro methyl sulfinyl pyrazole
CN102093295A (zh) * 2011-03-10 2011-06-15 江苏长青农化股份有限公司 一种农药杀虫剂氟虫腈的合成方法
TWI579274B (zh) 2012-04-20 2017-04-21 龍馬躍公司 製備１－芳基－５－烷基吡唑化合物的改良方法
US9049860B2 (en) 2013-04-17 2015-06-09 The Hartz Mountain Corporation Ectoparasiticidal methods
CN104557713B (zh) * 2013-10-22 2018-08-21 江苏托球农化股份有限公司 高纯度氟虫腈制备方法
EP3412659A1 (en) * 2017-06-09 2018-12-12 Solvay Sa Processes for the manufacture of sulfur-substituted pyrazole derivatives
CN107963993A (zh) * 2018-01-06 2018-04-27 江苏托球农化股份有限公司 一种高纯度氟虫腈的制备方法
US20220185783A1 (en) * 2019-03-19 2022-06-16 Gharda Chemicals Limited Process for synthesis of fipronil
CN113149873A (zh) * 2021-03-10 2021-07-23 浙江埃森化学有限公司 一种三氟甲基亚磺酰氯的制备方法
CN115650919A (zh) * 2022-04-13 2023-01-31 华东理工大学 一种自三氯甲基亚磺酰氯制备氟虫腈的方法
CN115353490A (zh) * 2022-09-26 2022-11-18 安徽美诺华药物化学有限公司 一种氟虫腈的纯化工艺

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5187185A (en) * 1988-12-09 1993-02-16 Rhone-Poulenc Ag Company Pesticidal 1-arylpyrroles
JPS55157570A (en) * 1979-05-26 1980-12-08 Nissan Chem Ind Ltd Sulfamylimidazole derivative, and agricultural and horticultural fungicide
GB8713768D0 (en) * 1987-06-12 1987-07-15 May & Baker Ltd Compositions of matter
US5232940A (en) * 1985-12-20 1993-08-03 Hatton Leslie R Derivatives of N-phenylpyrazoles
DE3820190A1 (de) * 1988-06-14 1989-12-21 Cassella Ag Pyrrolderivate, ihre herstellung und ihre verwendung als pharmazeutische wirkstoffe
CA2004776C (fr) * 1988-12-13 2000-04-25 Claude Wakselman Procede de preparation de perfluoroalkylthioethers
US5223525A (en) * 1989-05-05 1993-06-29 Rhone-Poulenc Ag Company Pesticidal 1-arylimidazoles
GB9120641D0 (en) * 1991-09-27 1991-11-06 Ici Plc Heterocyclic compounds

Also Published As

Publication number Publication date
SK23495A3 (en) 1995-09-13
FI950800A (fi) 1995-08-23
FR2716453B1 (fr) 1996-03-29
CZ46195A3 (en) 1995-10-18
JPH07278106A (ja) 1995-10-24
US5618945A (en) 1997-04-08
AU1238395A (en) 1995-08-31
EP0668269A1 (fr) 1995-08-23
HU214283B (hu) 1998-03-02
CA2143135C (fr) 2010-01-19
ES2173932T3 (es) 2002-11-01
PL183151B1 (pl) 2002-05-31
RO113639B1 (ro) 1998-09-30
ZA951468B (en) 1996-02-16
JP2007153906A (ja) 2007-06-21
JP2005187478A (ja) 2005-07-14
FI950800A0 (fi) 1995-02-21
PL307393A1 (en) 1995-09-04
BR9500858A (pt) 1995-10-24
IL112708A0 (en) 1995-05-26
AU678876B2 (en) 1997-06-12
CN1110682A (zh) 1995-10-25
SK282510B6 (sk) 2002-10-08
DK0668269T3 (da) 2002-06-17
KR950032134A (ko) 1995-12-20
CZ294640B6 (cs) 2005-02-16
JP4731503B2 (ja) 2011-07-27
CN1056833C (zh) 2000-09-27
HUT69333A (en) 1995-09-28
KR100370990B1 (ko) 2003-04-21
HU9500522D0 (en) 1995-04-28
DE69526815T2 (de) 2002-11-14
JP3963965B2 (ja) 2007-08-22
IL112708A (en) 2005-05-17
RU95102481A (ru) 1996-11-20
RU2136665C1 (ru) 1999-09-10
PT668269E (pt) 2002-09-30
CA2143135A1 (fr) 1995-08-23
DE69526815D1 (de) 2002-07-04
EP0668269B1 (fr) 2002-05-29
JP4447478B2 (ja) 2010-04-07
ATE218127T1 (de) 2002-06-15
FR2716453A1 (fr) 1995-08-25
UA44226C2 (uk) 2002-02-15

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Owner name: BASF AGRO B.V., ARNHEM (NL), WAEDENSWIL-BRANCH

Free format text: BASF AGRO B.V., ARNHEM (NL), WAEDENSWIL-BRANCH

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