DE112008002403T5 - Dispersionsflüssigkeit von vernetzten Harzteilchen - Google Patents
Dispersionsflüssigkeit von vernetzten Harzteilchen Download PDFInfo
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- DE112008002403T5 DE112008002403T5 DE112008002403T DE112008002403T DE112008002403T5 DE 112008002403 T5 DE112008002403 T5 DE 112008002403T5 DE 112008002403 T DE112008002403 T DE 112008002403T DE 112008002403 T DE112008002403 T DE 112008002403T DE 112008002403 T5 DE112008002403 T5 DE 112008002403T5
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- Prior art keywords
- dispersion
- resin particles
- particles
- resin
- toner
- Prior art date
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- 229920000515 polycarbonate Polymers 0.000 description 1
- 229920005668 polycarbonate resin Polymers 0.000 description 1
- 239000004431 polycarbonate resin Substances 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 229920001225 polyester resin Polymers 0.000 description 1
- 239000004645 polyester resin Substances 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 239000004926 polymethyl methacrylate Substances 0.000 description 1
- 229920000098 polyolefin Polymers 0.000 description 1
- 229920000259 polyoxyethylene lauryl ether Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 239000005077 polysulfide Substances 0.000 description 1
- 229920001021 polysulfide Polymers 0.000 description 1
- 150000008117 polysulfides Polymers 0.000 description 1
- 229920005749 polyurethane resin Polymers 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 229940051201 quinoline yellow Drugs 0.000 description 1
- 235000012752 quinoline yellow Nutrition 0.000 description 1
- IZMJMCDDWKSTTK-UHFFFAOYSA-N quinoline yellow Chemical compound C1=CC=CC2=NC(C3C(C4=CC=CC=C4C3=O)=O)=CC=C21 IZMJMCDDWKSTTK-UHFFFAOYSA-N 0.000 description 1
- 239000004172 quinoline yellow Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- PYWVYCXTNDRMGF-UHFFFAOYSA-N rhodamine B Chemical compound [Cl-].C=12C=CC(=[N+](CC)CC)C=C2OC2=CC(N(CC)CC)=CC=C2C=1C1=CC=CC=C1C(O)=O PYWVYCXTNDRMGF-UHFFFAOYSA-N 0.000 description 1
- 229940043267 rhodamine b Drugs 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 229960004889 salicylic acid Drugs 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 229920002050 silicone resin Polymers 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 229940083542 sodium Drugs 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 229940083575 sodium dodecyl sulfate Drugs 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- MNCGMVDMOKPCSQ-UHFFFAOYSA-M sodium;2-phenylethenesulfonate Chemical compound [Na+].[O-]S(=O)(=O)C=CC1=CC=CC=C1 MNCGMVDMOKPCSQ-UHFFFAOYSA-M 0.000 description 1
- 239000011877 solvent mixture Substances 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 229940037312 stearamide Drugs 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 229920001909 styrene-acrylic polymer Polymers 0.000 description 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-L succinate(2-) Chemical compound [O-]C(=O)CCC([O-])=O KDYFGRWQOYBRFD-UHFFFAOYSA-L 0.000 description 1
- 239000001384 succinic acid Chemical group 0.000 description 1
- 150000003444 succinic acids Chemical group 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 238000010557 suspension polymerization reaction Methods 0.000 description 1
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- JRMUNVKIHCOMHV-UHFFFAOYSA-M tetrabutylammonium bromide Chemical compound [Br-].CCCC[N+](CCCC)(CCCC)CCCC JRMUNVKIHCOMHV-UHFFFAOYSA-M 0.000 description 1
- HWCKGOZZJDHMNC-UHFFFAOYSA-M tetraethylammonium bromide Chemical compound [Br-].CC[N+](CC)(CC)CC HWCKGOZZJDHMNC-UHFFFAOYSA-M 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 239000001017 thiazole dye Substances 0.000 description 1
- JOUDBUYBGJYFFP-FOCLMDBBSA-N thioindigo Chemical compound S\1C2=CC=CC=C2C(=O)C/1=C1/C(=O)C2=CC=CC=C2S1 JOUDBUYBGJYFFP-FOCLMDBBSA-N 0.000 description 1
- KSBAEPSJVUENNK-UHFFFAOYSA-L tin(ii) 2-ethylhexanoate Chemical compound [Sn+2].CCCCC(CC)C([O-])=O.CCCCC(CC)C([O-])=O KSBAEPSJVUENNK-UHFFFAOYSA-L 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 230000001960 triggered effect Effects 0.000 description 1
- RBKBGHZMNFTKRE-UHFFFAOYSA-K trisodium 2-[(2-oxido-3-sulfo-6-sulfonatonaphthalen-1-yl)diazenyl]benzoate Chemical compound C1=CC=C(C(=C1)C(=O)[O-])N=NC2=C3C=CC(=CC3=CC(=C2[O-])S(=O)(=O)O)S(=O)(=O)[O-].[Na+].[Na+].[Na+] RBKBGHZMNFTKRE-UHFFFAOYSA-K 0.000 description 1
- 229920001567 vinyl ester resin Polymers 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 239000001018 xanthene dye Substances 0.000 description 1
- 239000011592 zinc chloride Substances 0.000 description 1
- 235000005074 zinc chloride Nutrition 0.000 description 1
- 239000004711 α-olefin Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/24—Crosslinking, e.g. vulcanising, of macromolecules
- C08J3/246—Intercrosslinking of at least two polymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
- C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
- C08J3/05—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media from solid polymers
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/0802—Preparation methods
- G03G9/0804—Preparation methods whereby the components are brought together in a liquid dispersing medium
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/0802—Preparation methods
- G03G9/0804—Preparation methods whereby the components are brought together in a liquid dispersing medium
- G03G9/0806—Preparation methods whereby the components are brought together in a liquid dispersing medium whereby chemical synthesis of at least one of the toner components takes place
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/087—Binders for toner particles
- G03G9/08784—Macromolecular material not specially provided for in a single one of groups G03G9/08702 - G03G9/08775
- G03G9/08793—Crosslinked polymers
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/087—Binders for toner particles
- G03G9/08784—Macromolecular material not specially provided for in a single one of groups G03G9/08702 - G03G9/08775
- G03G9/08795—Macromolecular material not specially provided for in a single one of groups G03G9/08702 - G03G9/08775 characterised by their chemical properties, e.g. acidity, molecular weight, sensitivity to reactants
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/087—Binders for toner particles
- G03G9/08784—Macromolecular material not specially provided for in a single one of groups G03G9/08702 - G03G9/08775
- G03G9/08797—Macromolecular material not specially provided for in a single one of groups G03G9/08702 - G03G9/08775 characterised by their physical properties, e.g. viscosity, solubility, melting temperature, softening temperature, glass transition temperature
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/093—Encapsulated toner particles
- G03G9/09307—Encapsulated toner particles specified by the shell material
- G03G9/09314—Macromolecular compounds
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/093—Encapsulated toner particles
- G03G9/0935—Encapsulated toner particles specified by the core material
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/093—Encapsulated toner particles
- G03G9/0935—Encapsulated toner particles specified by the core material
- G03G9/09357—Macromolecular compounds
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/093—Encapsulated toner particles
- G03G9/0935—Encapsulated toner particles specified by the core material
- G03G9/09357—Macromolecular compounds
- G03G9/09371—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/093—Encapsulated toner particles
- G03G9/09392—Preparation thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2367/00—Characterised by the use of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Derivatives of such polymers
- C08J2367/06—Unsaturated polyesters
Landscapes
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Developing Agents For Electrophotography (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2007232476 | 2007-09-07 | ||
| JP2007-232476 | 2007-09-07 | ||
| JP2008-147063 | 2008-06-04 | ||
| JP2008147063A JP5297094B2 (ja) | 2007-09-07 | 2008-06-04 | 架橋樹脂粒子分散液 |
| PCT/JP2008/066090 WO2009031655A1 (ja) | 2007-09-07 | 2008-09-05 | 架橋樹脂粒子分散液 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE112008002403T5 true DE112008002403T5 (de) | 2010-07-15 |
Family
ID=40654204
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE112008002403T Withdrawn DE112008002403T5 (de) | 2007-09-07 | 2008-09-05 | Dispersionsflüssigkeit von vernetzten Harzteilchen |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US8409775B2 (enExample) |
| JP (1) | JP5297094B2 (enExample) |
| CN (1) | CN101796102B (enExample) |
| DE (1) | DE112008002403T5 (enExample) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5015743B2 (ja) * | 2007-11-29 | 2012-08-29 | 花王株式会社 | トナー用離型剤分散液の製造方法 |
| JP5119074B2 (ja) * | 2008-07-24 | 2013-01-16 | シャープ株式会社 | トナーの製造方法およびトナー、現像剤、現像装置ならびに画像形成装置 |
| CN102667630B (zh) * | 2009-12-22 | 2015-02-18 | 花王株式会社 | 电子照相用色调剂的制备方法 |
| JP5431423B2 (ja) * | 2011-07-08 | 2014-03-05 | 東芝テック株式会社 | 消色性トナーおよびその製造方法 |
| JP5480851B2 (ja) * | 2011-07-08 | 2014-04-23 | 東芝テック株式会社 | トナーおよびその製造方法 |
| JP6071826B2 (ja) * | 2012-10-05 | 2017-02-01 | 花王株式会社 | 電子写真用トナーの製造方法 |
| JP6220266B2 (ja) * | 2013-12-27 | 2017-10-25 | 花王株式会社 | 電子写真用トナーの製造方法 |
| JP6279899B2 (ja) * | 2013-12-27 | 2018-02-14 | 花王株式会社 | 電子写真用トナーの製造方法 |
| JP2016040573A (ja) * | 2014-08-12 | 2016-03-24 | 富士ゼロックス株式会社 | 画像形成方法 |
| JP6470942B2 (ja) * | 2014-10-29 | 2019-02-13 | 花王株式会社 | 静電荷像現像用トナーの製造方法 |
| JP2016224432A (ja) * | 2015-05-28 | 2016-12-28 | 三洋化成工業株式会社 | トナーバインダーおよびトナー |
| JP6773543B2 (ja) * | 2015-12-16 | 2020-10-21 | 三洋化成工業株式会社 | トナーバインダーおよびトナー |
| JP6648706B2 (ja) * | 2017-01-26 | 2020-02-14 | 京セラドキュメントソリューションズ株式会社 | 静電潜像現像用トナー及びその製造方法 |
| JP6610574B2 (ja) * | 2017-02-03 | 2019-11-27 | 京セラドキュメントソリューションズ株式会社 | 静電潜像現像用トナー及びその製造方法 |
| JP6702257B2 (ja) * | 2017-04-27 | 2020-05-27 | 京セラドキュメントソリューションズ株式会社 | 静電潜像現像用トナー |
| JP6904191B2 (ja) * | 2017-09-20 | 2021-07-14 | 京セラドキュメントソリューションズ株式会社 | 正帯電性トナー及びその製造方法 |
| JP6915571B2 (ja) * | 2018-03-06 | 2021-08-04 | 京セラドキュメントソリューションズ株式会社 | 正帯電性トナー、及び正帯電性トナーの製造方法 |
| JP6888583B2 (ja) * | 2018-04-23 | 2021-06-16 | 京セラドキュメントソリューションズ株式会社 | トナー |
| JP6838578B2 (ja) * | 2018-04-25 | 2021-03-03 | 京セラドキュメントソリューションズ株式会社 | トナー |
| JP7463218B2 (ja) * | 2019-09-06 | 2024-04-08 | 三洋化成工業株式会社 | トナーバインダー |
| JP7098597B2 (ja) * | 2019-12-27 | 2022-07-11 | キヤノン株式会社 | 二成分現像剤 |
| JP7643117B2 (ja) * | 2021-03-19 | 2025-03-11 | 富士フイルムビジネスイノベーション株式会社 | 静電荷像現像用トナーの製造方法、及び、静電荷像現像用トナー |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0820636A (ja) | 1994-07-07 | 1996-01-23 | Mitsubishi Rayon Co Ltd | トナー用架橋ポリエステル樹脂 |
| JPH1010774A (ja) | 1996-06-19 | 1998-01-16 | Dainippon Ink & Chem Inc | 粉体トナーの製造方法 |
| JPH10239903A (ja) | 1997-02-27 | 1998-09-11 | Sanyo Chem Ind Ltd | 静電荷像現像用トナーバインダー |
| JPH11133668A (ja) | 1997-10-31 | 1999-05-21 | Sanyo Chem Ind Ltd | トナーバインダー |
| JP2000347455A (ja) | 1999-06-09 | 2000-12-15 | Dainippon Ink & Chem Inc | トナー及びその製法 |
| JP2004163854A (ja) | 2002-09-19 | 2004-06-10 | Fuji Xerox Co Ltd | 静電荷像現像用トナー、静電荷像現像用トナーの製造方法、静電荷像現像用現像剤、及び、画像形成方法 |
| JP2006106291A (ja) | 2004-10-04 | 2006-04-20 | Seiko Epson Corp | トナーの製造方法およびトナー |
| JP2006317715A (ja) | 2005-05-12 | 2006-11-24 | Fuji Xerox Co Ltd | 静電荷像現像用トナー及び静電荷像現像用トナー用樹脂粒子分散液 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0253078A (ja) * | 1988-08-17 | 1990-02-22 | Nippon Synthetic Chem Ind Co Ltd:The | トナー用バインダー |
| JP3308812B2 (ja) * | 1995-05-31 | 2002-07-29 | キヤノン株式会社 | 静電荷像現像用トナー及びその製造方法 |
| US6017670A (en) | 1996-02-29 | 2000-01-25 | Dainippon Ink And Chemicals, Inc. | Electrophotographic toner and process for the preparation thereof |
| US6194510B1 (en) | 1997-11-12 | 2001-02-27 | S. C. Johnson Commercial Markets, Inc. | Aqueous dispersions of non-gelled polymeric compositions having designated amounts of reactive groups |
| JP4968993B2 (ja) | 2000-09-28 | 2012-07-04 | ユニチカ株式会社 | ポリエステル樹脂水性分散体およびその製造方法 |
| US20030148073A1 (en) * | 2001-12-20 | 2003-08-07 | Eastman Kodak Company | Porous organic particles for ink recording element use |
| EP1505128B2 (en) * | 2002-05-16 | 2017-05-24 | Seiko Epson Corporation | Pigment dispersion and ink composition for ink-jet |
| JP2006070123A (ja) * | 2004-09-01 | 2006-03-16 | Seiko Epson Corp | インク組成物、インクセット、記録方法、及び記録像 |
| JP2006182950A (ja) * | 2004-12-28 | 2006-07-13 | Unitika Ltd | ポリエステル樹脂水性分散体 |
| JP2007031603A (ja) * | 2005-07-28 | 2007-02-08 | Sanyo Chem Ind Ltd | 樹脂粒子の製造法 |
| JP5134207B2 (ja) * | 2006-02-22 | 2013-01-30 | 花王株式会社 | 着色剤含有樹脂乳化粒子の製造方法 |
-
2008
- 2008-06-04 JP JP2008147063A patent/JP5297094B2/ja not_active Expired - Fee Related
- 2008-09-05 CN CN200880105622.3A patent/CN101796102B/zh not_active Expired - Fee Related
- 2008-09-05 DE DE112008002403T patent/DE112008002403T5/de not_active Withdrawn
- 2008-09-05 US US12/676,531 patent/US8409775B2/en not_active Expired - Fee Related
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0820636A (ja) | 1994-07-07 | 1996-01-23 | Mitsubishi Rayon Co Ltd | トナー用架橋ポリエステル樹脂 |
| JPH1010774A (ja) | 1996-06-19 | 1998-01-16 | Dainippon Ink & Chem Inc | 粉体トナーの製造方法 |
| JPH10239903A (ja) | 1997-02-27 | 1998-09-11 | Sanyo Chem Ind Ltd | 静電荷像現像用トナーバインダー |
| JPH11133668A (ja) | 1997-10-31 | 1999-05-21 | Sanyo Chem Ind Ltd | トナーバインダー |
| JP2000347455A (ja) | 1999-06-09 | 2000-12-15 | Dainippon Ink & Chem Inc | トナー及びその製法 |
| JP2004163854A (ja) | 2002-09-19 | 2004-06-10 | Fuji Xerox Co Ltd | 静電荷像現像用トナー、静電荷像現像用トナーの製造方法、静電荷像現像用現像剤、及び、画像形成方法 |
| JP2006106291A (ja) | 2004-10-04 | 2006-04-20 | Seiko Epson Corp | トナーの製造方法およびトナー |
| JP2006317715A (ja) | 2005-05-12 | 2006-11-24 | Fuji Xerox Co Ltd | 静電荷像現像用トナー及び静電荷像現像用トナー用樹脂粒子分散液 |
Non-Patent Citations (2)
| Title |
|---|
| ASTM D36-86 |
| JIS K0070 |
Also Published As
| Publication number | Publication date |
|---|---|
| JP2009079207A (ja) | 2009-04-16 |
| JP5297094B2 (ja) | 2013-09-25 |
| CN101796102A (zh) | 2010-08-04 |
| US8409775B2 (en) | 2013-04-02 |
| US20100183969A1 (en) | 2010-07-22 |
| CN101796102B (zh) | 2013-01-16 |
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