CN105652349A - 核壳纳米粒子 - Google Patents
核壳纳米粒子 Download PDFInfo
- Publication number
- CN105652349A CN105652349A CN201610154455.8A CN201610154455A CN105652349A CN 105652349 A CN105652349 A CN 105652349A CN 201610154455 A CN201610154455 A CN 201610154455A CN 105652349 A CN105652349 A CN 105652349A
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- polymer
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- coating
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- 239000002105 nanoparticle Substances 0.000 title claims abstract description 39
- 239000011258 core-shell material Substances 0.000 title claims abstract description 35
- 229920000642 polymer Polymers 0.000 claims abstract description 58
- 239000011257 shell material Substances 0.000 claims abstract description 35
- 229910044991 metal oxide Inorganic materials 0.000 claims abstract description 26
- 150000004706 metal oxides Chemical class 0.000 claims abstract description 24
- 239000000203 mixture Substances 0.000 claims description 49
- 239000000463 material Substances 0.000 claims description 37
- 239000008199 coating composition Substances 0.000 claims description 33
- 229920001577 copolymer Polymers 0.000 claims description 33
- 239000011230 binding agent Substances 0.000 claims description 32
- 239000011824 nuclear material Substances 0.000 claims description 28
- 230000003287 optical effect Effects 0.000 claims description 27
- 229920000359 diblock copolymer Polymers 0.000 claims description 14
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 13
- 239000010703 silicon Substances 0.000 claims description 13
- 229910052710 silicon Inorganic materials 0.000 claims description 13
- 239000004575 stone Substances 0.000 claims description 13
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 9
- 239000004816 latex Substances 0.000 claims description 9
- 229920000126 latex Polymers 0.000 claims description 9
- 229920000428 triblock copolymer Polymers 0.000 claims description 8
- 125000002091 cationic group Chemical group 0.000 claims description 7
- 239000011800 void material Substances 0.000 claims description 6
- 229920000728 polyester Polymers 0.000 claims description 5
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- 229920002635 polyurethane Polymers 0.000 claims description 4
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- 229910052809 inorganic oxide Inorganic materials 0.000 claims description 3
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- 238000000576 coating method Methods 0.000 description 53
- 239000011248 coating agent Substances 0.000 description 52
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- 239000000243 solution Substances 0.000 description 15
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- 238000000151 deposition Methods 0.000 description 10
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 8
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- 238000001723 curing Methods 0.000 description 8
- 239000002243 precursor Substances 0.000 description 8
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 7
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- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 6
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- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 6
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
- 125000000217 alkyl group Chemical group 0.000 description 6
- 239000003795 chemical substances by application Substances 0.000 description 6
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- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 4
- 125000003545 alkoxy group Chemical group 0.000 description 4
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- 238000002360 preparation method Methods 0.000 description 4
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- 238000003756 stirring Methods 0.000 description 4
- 239000004094 surface-active agent Substances 0.000 description 4
- LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 description 4
- 238000012546 transfer Methods 0.000 description 4
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 3
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 3
- 125000003277 amino group Chemical group 0.000 description 3
- FUSUHKVFWTUUBE-UHFFFAOYSA-N buten-2-one Chemical compound CC(=O)C=C FUSUHKVFWTUUBE-UHFFFAOYSA-N 0.000 description 3
- 239000003093 cationic surfactant Substances 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 238000003618 dip coating Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000011147 inorganic material Substances 0.000 description 3
- 239000010410 layer Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 230000005499 meniscus Effects 0.000 description 3
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 3
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- 229920003229 poly(methyl methacrylate) Polymers 0.000 description 3
- 239000004926 polymethyl methacrylate Substances 0.000 description 3
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- 238000003786 synthesis reaction Methods 0.000 description 3
- 150000003512 tertiary amines Chemical class 0.000 description 3
- 125000001302 tertiary amino group Chemical group 0.000 description 3
- CXBDYQVECUFKRK-UHFFFAOYSA-N 1-methoxybutane Chemical compound CCCCOC CXBDYQVECUFKRK-UHFFFAOYSA-N 0.000 description 2
- 238000005160 1H NMR spectroscopy Methods 0.000 description 2
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 2
- CEYHHQSTMVVZQP-UHFFFAOYSA-N 2-ethenoxyethanamine Chemical class NCCOC=C CEYHHQSTMVVZQP-UHFFFAOYSA-N 0.000 description 2
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
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- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- RRHGJUQNOFWUDK-UHFFFAOYSA-N Isoprene Chemical compound CC(=C)C=C RRHGJUQNOFWUDK-UHFFFAOYSA-N 0.000 description 2
- XOBKSJJDNFUZPF-UHFFFAOYSA-N Methoxyethane Chemical compound CCOC XOBKSJJDNFUZPF-UHFFFAOYSA-N 0.000 description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
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- 239000004115 Sodium Silicate Substances 0.000 description 2
- OKJPEAGHQZHRQV-UHFFFAOYSA-N Triiodomethane Natural products IC(I)I OKJPEAGHQZHRQV-UHFFFAOYSA-N 0.000 description 2
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical class C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 description 2
- NJSSICCENMLTKO-HRCBOCMUSA-N [(1r,2s,4r,5r)-3-hydroxy-4-(4-methylphenyl)sulfonyloxy-6,8-dioxabicyclo[3.2.1]octan-2-yl] 4-methylbenzenesulfonate Chemical compound C1=CC(C)=CC=C1S(=O)(=O)O[C@H]1C(O)[C@@H](OS(=O)(=O)C=2C=CC(C)=CC=2)[C@@H]2OC[C@H]1O2 NJSSICCENMLTKO-HRCBOCMUSA-N 0.000 description 2
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- VSDMVRFSCLVCOF-UHFFFAOYSA-N 1-ethenoxybutan-2-amine Chemical class CCC(N)COC=C VSDMVRFSCLVCOF-UHFFFAOYSA-N 0.000 description 1
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Abstract
Description
Claims (10)
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GB0617480.9 | 2006-09-06 | ||
GBGB0617480.9A GB0617480D0 (en) | 2006-09-06 | 2006-09-06 | Novel nanoparticles |
CN2007800331182A CN101512387B (zh) | 2006-09-06 | 2007-09-05 | 核壳纳米粒子 |
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CN2007800331182A Division CN101512387B (zh) | 2006-09-06 | 2007-09-05 | 核壳纳米粒子 |
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CN105652349A true CN105652349A (zh) | 2016-06-08 |
CN105652349B CN105652349B (zh) | 2018-05-11 |
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CN201610301487.6A Active CN105969022B (zh) | 2006-09-06 | 2007-09-05 | 核壳纳米粒子 |
CN2007800331182A Expired - Fee Related CN101512387B (zh) | 2006-09-06 | 2007-09-05 | 核壳纳米粒子 |
CN2007800331286A Active CN101611084B (zh) | 2006-09-06 | 2007-09-05 | 新型的纳米粒子 |
CN201310308983.0A Pending CN103487849A (zh) | 2006-09-06 | 2007-09-05 | 核壳纳米粒子 |
CN201610154455.8A Active CN105652349B (zh) | 2006-09-06 | 2007-09-05 | 核壳纳米粒子 |
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CN2007800331182A Expired - Fee Related CN101512387B (zh) | 2006-09-06 | 2007-09-05 | 核壳纳米粒子 |
CN2007800331286A Active CN101611084B (zh) | 2006-09-06 | 2007-09-05 | 新型的纳米粒子 |
CN201310308983.0A Pending CN103487849A (zh) | 2006-09-06 | 2007-09-05 | 核壳纳米粒子 |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN106430222A (zh) * | 2016-09-29 | 2017-02-22 | 上海特栎材料科技有限公司 | 一种纳米二氧化硅微球及其制备方法 |
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