CN105362309A - Herba Portulacae freshly-squeezed freeze-dried powder decoction pieces and preparation process thereof - Google Patents
Herba Portulacae freshly-squeezed freeze-dried powder decoction pieces and preparation process thereof Download PDFInfo
- Publication number
- CN105362309A CN105362309A CN201510774363.5A CN201510774363A CN105362309A CN 105362309 A CN105362309 A CN 105362309A CN 201510774363 A CN201510774363 A CN 201510774363A CN 105362309 A CN105362309 A CN 105362309A
- Authority
- CN
- China
- Prior art keywords
- herba portulacae
- decoction pieces
- squeezed
- freeze
- medicine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
Abstract
The invention discloses Herba Portulacae freshly-squeezed freeze-dried powder decoction pieces and a preparation process thereof. In the process, Herba Portulacae is purified, selected and washed after being harvested and is squeezed and filtered when it is fresh to obtain medicine juice; medicine residue is stirred with water and is filtered and squeezed; medicine juices obtained are combined and concentrated under reduced pressure and are freeze-dried to obtain a freeze-dried product that is crushed and vacuum packaged. The Herba Portulacae powder decoction pieces prepared by the method allow polar and non-polar effective ingredients in herbs to be retained to maximum extent; the decoction pieces are easy to storage and transport and convenient to dispense, have controllable quality and reliable therapeutic effect and are significant to ensuring traditional Chinese medicine clinical therapeutic effect. The popularization and implementation of the method has significant social implication and economic benefits.
Description
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Portulaca oleracea L decoction pieces.
Background technology
Portulaca oleracea L is portulacaceous plant
portulacaoleraceal. dry aerial parts.This product has heat-clearing and toxic substances removing, the function of loose blood detumescence.Clinical main in order to treat hematodiarrhoea pus and blood, pyretic stranguria, stranguria with blood, leukorrhagia, carbuncle malignant boil, erysipelas etc.
The processing mode of conventional Herba Portulacae decoction pieces is: after gathering, and removing impurity, dries, then accumulating of packing.This type of prepared herbal medicine in small pieces ready for decoction, bulky, Hygienic Index is poor, easily pollutes and goes mouldy, and quality is difficult to ensure, is unfavorable for that formula is adjusted and guarantees its clinical efficacy, even brings recessive harm to patient.
At present, granule pieces market also having purslane medicinal material to make after extracting is sold.The preparation process of granule pieces, extracts not only time consumption and energy consumption, and does solvent because commonly using a large amount of water, and the nonpolar effective ingredient in medical material is difficult to be extracted.In addition, because the purslane medicinal material extracted also is dry also through long-time storage, therefore, the loss of effective ingredient is also very large.In order to ensure clinical effective, the steady quality of purslane medicinal material, a kind of novel Herba Portulacae decoction pieces and preparation technology thereof urgently develop.
Summary of the invention
The present invention discloses " a kind of Herba Portulacae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof ".This technique can retain polarity in purslane medicinal material and nonpolar effective ingredient to greatest extent, the loss of effective ingredient avoiding medical material to cause in existing decoction pieces processing and storage and transport process and the decline of medical material quanlity, reduce the pollution of medical material by mycete etc., the steady quality and clinical safety guaranteeing Herba Portulacae decoction pieces is effectively had great importance.
To achieve these goals, technical scheme of the present invention is:
Gather its aerial parts collection period Herba Portulacae, clean, after washing, take advantage of fresh squeezing, medicinal residues add the water of 1 ~ 5 times amount, and stir 5 ~ 30min, filter press filter pressing extracting juice, remaining medicinal residues squeeze extracting juice again, merge three medicine juice, 40 ~ 120 mesh screen, obtain Herba Portulacae medicine juice.The Herba Portulacae medicine juice obtained is evaporated to the extractum that relative density is 1.05 ~ 1.25 under 40 ~ 75 DEG C of conditions, and this extractum is freezed 6 ~ 24 hours in-20 ~-80 DEG C of refrigerators, lyophilization again, pressure is 0.06 ~ 0.09MPa, and temperature is-15 ~-40 DEG C, and cooling time is 12 ~ 48 hours, after collecting lyophilized products, through pulverizing, sieving, packing.
On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, decoction pieces manufacturer, date of manufacture, Contents of Main Components, meridian distribution of property and flavor, function cure mainly, the information such as usage and dosage, toxic and side effects and contraindication.The TLC distinguish collection of illustrative plates of the included upper Herba Portulacae of bag and/or high-efficient liquid phase character collection of illustrative plates, as " identity card " of product.In addition, in the packaging bag of product, be printed on Quick Response Code, the information such as former plant photo, medical material photo, decoction pieces photo, character and the microscopical identification feature obtaining product can be linked by scanning.
Usefulness of the present invention is:
The purslane medicinal material of fresh collection, direct squeezing, filtration, concentrating under reduced pressure, lyophilization after cleaning washing, the powder decoction pieces obtained, can retain the effective ingredient in medical material to greatest extent.This decoction pieces volume compares to traditional decoction pieces volume and reduces widely, and vacuum packaging, makes prepared slice quality more stable, is beneficial to accumulating and clinical adjustment, has very significant social meaning and economic implications.
Detailed description of the invention
Embodiment 1
By the purslane medicinal material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add the tap water of 3 times amount, stir 20min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.Above-mentioned 3 medicine juice are merged, filters with 100 eye mesh screens.Filtrate reduced in volume, temperature is set as 65 DEG C.When concentrated gained extractum relative density is 1.15, extractum is freezed 6 hours in-80 DEG C of refrigerators.Take out east knot thing, lyophilization, pressure is 0.09Mpa, and temperature is-20 DEG C, dry 24 hours.Take out lyophilized products, pulverize at low temperature, cross 80 mesh sieves, moisture is not higher than 12%, and pack, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, labeling.
Embodiment 2
By the purslane medicinal material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add the tap water of 5 times amount, stir 30min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.Above-mentioned 3 medicine juice are merged, filters with 80 eye mesh screens.Filtrate reduced in volume, temperature is set as 70 DEG C.When concentrated gained extractum relative density is 1.10, extractum is freezed 8 hours in-80 DEG C of refrigerators.Take out east knot thing, lyophilization, pressure is 0.08Mpa, and temperature is-40 DEG C, dry 48 hours.Take out lyophilized products, pulverize at low temperature, cross 60 mesh sieves, moisture is not higher than 12%, and pack, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, labeling.
Above embodiment, is only the technological thought that this invention is described, can not limit the every technological thought proposed according to the present invention of protection scope of the present invention whereby, any change that technical scheme basis is done, all falls within the scope of protection of the invention.
Claims (2)
1. a Herba Portulacae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof, it is characterized in that: gather its aerial parts collection period Herba Portulacae, clean, after washing, take advantage of fresh squeezing, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, filter press filter pressing extracting juice, remaining medicinal residues squeeze extracting juice again, merge three medicine juice, 40 ~ 120 mesh screen, obtain Herba Portulacae medicine juice.
2. a kind of Herba Portulacae according to claim 1 fresh squeezing lyophilization powder decoction pieces and preparation technology thereof, it is characterized in that: the Herba Portulacae medicine juice obtained in claim 1 is evaporated to the extractum that relative density is 1.05 ~ 1.25 under 40 ~ 75 DEG C of conditions, and this extractum is freezed 6 ~ 24 hours in-20 ~-80 DEG C of refrigerators, then lyophilization, pressure is 0.06 ~ 0.09MPa, temperature is-15 ~-40 DEG C, cooling time is 12 ~ 48 hours, after collecting lyophilized products, through pulverizing, sieve, pack.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510774363.5A CN105362309A (en) | 2015-11-14 | 2015-11-14 | Herba Portulacae freshly-squeezed freeze-dried powder decoction pieces and preparation process thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510774363.5A CN105362309A (en) | 2015-11-14 | 2015-11-14 | Herba Portulacae freshly-squeezed freeze-dried powder decoction pieces and preparation process thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105362309A true CN105362309A (en) | 2016-03-02 |
Family
ID=55365263
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510774363.5A Pending CN105362309A (en) | 2015-11-14 | 2015-11-14 | Herba Portulacae freshly-squeezed freeze-dried powder decoction pieces and preparation process thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105362309A (en) |
Cited By (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105998132A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Chinese lobelia freshly-squeezed freeze drying powder decoction tablets and preparation process thereof |
| CN105998130A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Folium Isatidis freshly-pressed lyophilized powdery decoction pieces and preparation process thereof |
| CN106109545A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Euphorbiae Humifusae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
| CN106214741A (en) * | 2016-07-24 | 2016-12-14 | 徐漫 | A kind of Herba Scutellariae Barbatae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
| CN107028998A (en) * | 2017-06-19 | 2017-08-11 | 徐漫 | A kind of field thistle is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107213187A (en) * | 2017-06-20 | 2017-09-29 | 徐漫 | A kind of acalypha copperleaf is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107233385A (en) * | 2017-06-22 | 2017-10-10 | 徐漫 | A kind of motherwort is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107320566A (en) * | 2017-08-25 | 2017-11-07 | 徐漫 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of black nightshade |
| CN107320515A (en) * | 2017-08-25 | 2017-11-07 | 徐漫 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of Artemisia anomala |
| CN107375425A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of schizonepeta is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107375512A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of cordate houttuynia |
| CN107375419A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of elscholtiza |
| CN107375352A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of phoenix-tail fern |
| CN107375394A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of fringed pink |
| CN107397768A (en) * | 2017-08-25 | 2017-11-28 | 徐漫 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of ardisia japonica |
| CN107412307A (en) * | 2017-08-25 | 2017-12-01 | 徐自升 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of oriental wormwood |
| CN107432878A (en) * | 2017-08-25 | 2017-12-05 | 徐漫 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of scouring rush |
| CN107441154A (en) * | 2017-08-25 | 2017-12-08 | 徐自升 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of Pogostemon cablin |
| CN107441155A (en) * | 2017-08-25 | 2017-12-08 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of Longtube Ground Ivy Herb |
| CN107485629A (en) * | 2017-08-25 | 2017-12-19 | 徐自升 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of desmodium |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1364468A (en) * | 2001-01-19 | 2002-08-21 | 赵国林 | Wall breaking and extracting method for Chinese herbal medicine and formulation |
| CN102119992A (en) * | 2011-03-07 | 2011-07-13 | 贵州百灵企业集团制药股份有限公司 | Pharmaceutical preparation prepared from fresh motherwort and fresh aloe and preparation method thereof |
| CN102406175A (en) * | 2011-12-06 | 2012-04-11 | 张天久 | Preparation method of fresh sow thistle juice |
-
2015
- 2015-11-14 CN CN201510774363.5A patent/CN105362309A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1364468A (en) * | 2001-01-19 | 2002-08-21 | 赵国林 | Wall breaking and extracting method for Chinese herbal medicine and formulation |
| CN102119992A (en) * | 2011-03-07 | 2011-07-13 | 贵州百灵企业集团制药股份有限公司 | Pharmaceutical preparation prepared from fresh motherwort and fresh aloe and preparation method thereof |
| CN102406175A (en) * | 2011-12-06 | 2012-04-11 | 张天久 | Preparation method of fresh sow thistle juice |
Non-Patent Citations (3)
| Title |
|---|
| 刘永新: "《国家药典中药实用手册》", 30 April 2011, 中医古籍出版社 * |
| 南京药学院药剂学教研组: "《药剂学》", 31 May 1962, 人民卫生出版社 * |
| 郝近大: "《鲜品中药及其临床应用》", 31 December 1996, 上海科学技术出版社 * |
Cited By (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105998132A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Chinese lobelia freshly-squeezed freeze drying powder decoction tablets and preparation process thereof |
| CN105998130A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Folium Isatidis freshly-pressed lyophilized powdery decoction pieces and preparation process thereof |
| CN106109545A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Euphorbiae Humifusae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
| CN106214741A (en) * | 2016-07-24 | 2016-12-14 | 徐漫 | A kind of Herba Scutellariae Barbatae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
| CN107028998A (en) * | 2017-06-19 | 2017-08-11 | 徐漫 | A kind of field thistle is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107213187A (en) * | 2017-06-20 | 2017-09-29 | 徐漫 | A kind of acalypha copperleaf is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107233385A (en) * | 2017-06-22 | 2017-10-10 | 徐漫 | A kind of motherwort is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107320566A (en) * | 2017-08-25 | 2017-11-07 | 徐漫 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of black nightshade |
| CN107320515A (en) * | 2017-08-25 | 2017-11-07 | 徐漫 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of Artemisia anomala |
| CN107375425A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of schizonepeta is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107375512A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of cordate houttuynia |
| CN107375419A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of elscholtiza |
| CN107375352A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of phoenix-tail fern |
| CN107375394A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of fringed pink |
| CN107397768A (en) * | 2017-08-25 | 2017-11-28 | 徐漫 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of ardisia japonica |
| CN107412307A (en) * | 2017-08-25 | 2017-12-01 | 徐自升 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of oriental wormwood |
| CN107432878A (en) * | 2017-08-25 | 2017-12-05 | 徐漫 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of scouring rush |
| CN107441154A (en) * | 2017-08-25 | 2017-12-08 | 徐自升 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of Pogostemon cablin |
| CN107441155A (en) * | 2017-08-25 | 2017-12-08 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of Longtube Ground Ivy Herb |
| CN107485629A (en) * | 2017-08-25 | 2017-12-19 | 徐自升 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of desmodium |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105362309A (en) | Herba Portulacae freshly-squeezed freeze-dried powder decoction pieces and preparation process thereof | |
| CN105213444A (en) | A kind of Herba Portulacae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof | |
| CN105287859A (en) | Freshly-squeezed paulownia flower freeze-dried powdery decoction piece and preparation technology thereof | |
| CN105998133A (en) | Chinese lobelia freshly-squeezed vacuum drying powder decoction tablets and preparation process thereof | |
| CN105998132A (en) | Chinese lobelia freshly-squeezed freeze drying powder decoction tablets and preparation process thereof | |
| CN105213453A (en) | A kind of Herba Taraxaci fresh squeezing lyophilization powder decoction pieces and preparation technology thereof | |
| CN105193883A (en) | Freshly squeezed spray drying parslane herb granular decoction pieces and preparation process thereof | |
| CN105213551A (en) | A kind of Herba Hedyotidis Diffusae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof | |
| CN105287860A (en) | Freshly-squeezed paulownia flower spray-dried powdery decoction piece and preparation technology thereof | |
| CN105213553A (en) | A kind of Herba Hedyotidis Diffusae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof | |
| CN105213552A (en) | A kind of Herba Hedyotidis Diffusae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof | |
| CN106236868A (en) | A kind of Herba Potentillae Discoloris fresh squeezing lyophilization powder decoction pieces and preparation technology thereof | |
| CN105213661A (en) | A kind of Aloe fresh squeezing lyophilization powder decoction pieces and preparation technology thereof | |
| CN105213445A (en) | A kind of Herba Portulacae fresh squeezing vacuum drying powder decoction pieces and preparation technology thereof | |
| CN105362528A (en) | Folium Aloes fresh-squeezed spray-dried powder decoction pieces and preparation method thereof | |
| CN106214741A (en) | A kind of Herba Scutellariae Barbatae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof | |
| CN105287861A (en) | Freshly-squeezed paulownia flower vacuum-dried powdery decoction piece and preparation technology thereof | |
| CN106109560A (en) | A kind of Flos Sophorae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof | |
| CN105998167A (en) | Vacuum-dried powdery medicinal slices prepared from freshly squeezed flos sophorae and preparation process thereof | |
| CN105213459A (en) | A kind of Radix et Caulis Opuntiae Dillenii fresh squeezing lyophilization powder decoction pieces and preparation technology thereof | |
| CN105194009A (en) | Freshly squeezed vacuum drying spreading hedyotis herb powdery decoction pieces and preparation process thereof | |
| CN107050082A (en) | A kind of field thistle is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology | |
| CN106109543A (en) | A kind of Herba Euphorbiae Humifusae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof | |
| CN106109624A (en) | A kind of Herba Potentillae Discoloris fresh squeezing spray-dried powders decoction pieces and preparation technology thereof | |
| CN105193894A (en) | Freshly squeezed vacuum drying cholla stem powdery decoction pieces and preparation process thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20160302 |