CN106109543A - A kind of Herba Euphorbiae Humifusae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof - Google Patents
A kind of Herba Euphorbiae Humifusae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof Download PDFInfo
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- CN106109543A CN106109543A CN201610583305.9A CN201610583305A CN106109543A CN 106109543 A CN106109543 A CN 106109543A CN 201610583305 A CN201610583305 A CN 201610583305A CN 106109543 A CN106109543 A CN 106109543A
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- Prior art keywords
- herba euphorbiae
- euphorbiae humifusae
- decoction pieces
- spray
- dried
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/47—Euphorbiaceae (Spurge family), e.g. Ricinus (castorbean)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/13—Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Alternative & Traditional Medicine (AREA)
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- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of Herba Euphorbiae Humifusae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof.This technique, after Herba Euphorbiae Humifusae medical material is gathered, cleans, drip washing, and takes advantage of fresh squeezing, leaching medicine juice.Medicinal residues add water stirring, filter squeezing.Concentrating under reduced pressure after the merging of gained medicine juice, is spray-dried, and collects spray drying product, is vacuum-packed after crushed.Herba Euphorbiae Humifusae powder decoction pieces prepared by this method, remains the polarity in medical material and nonpolar effective ingredient to greatest extent.Decoction pieces is beneficial to accumulating, convenient adjustment, and quality controllable, curative effect is reliable, to ensureing that tcm clinical curative effect has great importance.The promotion and implementation of this law, will have significant social meaning and economic benefit.
Description
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Chinese medicine Herba Euphorbiae Humifusae decoction pieces.
Background technology
Chinese medicine Herba Euphorbiae Humifusae is euphorbia plant Radix seu Caulis Parthenocissi tricuspidataeEuphorbia humifusa Or Herba Euphorbiae supinae Willd.Euphorbia maculataL. dry herb.Its nature and flavor are pungent flat, have heat-clearing and toxic substances removing, cooling blood for hemostasis, effect of dampness removing jaundice eliminating.For dysentery
Disease, has loose bowels, spitting of blood, and hematuria is had blood in stool, metrorrhagia, furuncle carbuncle, jaundice due to damp-heat.
The processing mode of conventional Herba Euphorbiae Humifusae decoction pieces is: summer, season in autumn two gather, and removes impurity, dries, then accumulating of packing.
This type of prepared herbal medicine in small pieces ready for decoction, bulky, Hygienic Index is poor, easily pollutes and goes mouldy, quality it is difficult to ensure that, be unfavorable for that formula is adjusted
With guarantee its clinical efficacy, even to patient bring recessiveness harm.
At present, granule pieces market also having Herba Euphorbiae Humifusae medical material to make after extracting is sold.The preparation of granule pieces
Process, extracts not only time consumption and energy consumption, and because conventional substantial amounts of water does solvent, the nonpolar effective ingredient in medical material is difficult to be carried
Take out.Additionally, due to the Herba Euphorbiae Humifusae medical material extracted also is to be dried and through long-time storage, therefore, effective ingredient
Loss is also the biggest.In order to ensure Herba Euphorbiae Humifusae medical material clinical effectively, steady quality, a kind of novel Herba Euphorbiae Humifusae decoction pieces and
Preparation technology urgently develops.
Summary of the invention
The invention discloses " a kind of Herba Euphorbiae Humifusae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof ".This technique is permissible
Polarity in reservation brocade medical herbs material and nonpolar effective ingredient while to greatest extent, it is to avoid medical material is processed at existing decoction pieces
With loss and the decline of medical material quanlity of the effective ingredient caused in storage and transport process, reduce the medical material pollution by mycete etc., to really
Steady quality and the clinical safety of protecting Herba Euphorbiae Humifusae decoction pieces effectively have great importance.
To achieve these goals, the technical scheme is that
Gather its herb collection period Herba Euphorbiae Humifusae, clean, after washing, take advantage of fresh squeezing.Gained medicinal residues add the water of 1 ~ 5 times amount,
Stirring 5 ~ 30min, filter press filter pressing extracting juice.Remaining medicinal residues are squeezed extracting juice again.Merge three medicine juice, with 40 ~ 120 mesh sieves
Filter, obtain Herba Euphorbiae Humifusae medicine juice.The Herba Euphorbiae Humifusae medicine juice obtained is evaporated under the conditions of 40 ~ 75 DEG C relative density be 1.02 ~
The concentrated solution of 1.15, and this concentrated solution is spray-dried, intake air temperature is set as 90 ~ 140 DEG C, and air outlet temperature is 80 ~ 110
DEG C, collect desciccate, cross 60 ~ 100 mesh sieves after pulverizing, be vacuum-packed.
On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, decoction pieces manufacturer, the date of manufacture,
The information such as Contents of Main Components, meridian distribution of property and flavor, function cure mainly, usage and dosage, toxic and side effects and contraindication.The included upper Herba Euphorbiae Humifusae of bag
Thin layer differentiate collection of illustrative plates and/or high-efficient liquid phase character collection of illustrative plates, as " identity card " of product.Additionally, in the packaging bag of product,
It is printed on Quick Response Code, the acquisition former plant photo of product, medical material photo, decoction pieces photo, character and micro-can be linked by scanning
The information such as diagnostic characteristics.
The invention have benefit that:
The Herba Euphorbiae Humifusae medical material of fresh collection, directly squeezes after cleaning washing, filters, concentrating under reduced pressure, spray drying, obtained powder
End decoction pieces, can retain the effective ingredient in medical material to greatest extent.This decoction pieces volume compares to tradition decoction pieces volume significantly
Ground reduces, vacuum packaging so that prepared slice quality is more stable, and beneficially accumulating and clinic is adjusted, and has very significantly society's meaning
Justice and economic implications.
Detailed description of the invention
Embodiment 1
By the Herba Euphorbiae Humifusae medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add 3
The tap water of times amount, stirs 20min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.By above-mentioned
3 times medicine juice merges, and filters with 100 eye mesh screens.Filtrate reduced in volume, temperature is set as 65 DEG C.Concentrating, gained extractum is the closeest
When degree is 1.05, being spray-dried, intake air temperature is 140 DEG C, and air outlet temperature is 100 DEG C, collection spray drying thing, low-temperature grinding,
Crossing 80 mesh sieves, moisture is not higher than 12%, packs, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, and labeling is i.e.
Can.
Embodiment 2
By the Herba Euphorbiae Humifusae medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add 5
The tap water of times amount, stirs 30min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.By above-mentioned
3 times medicine juice merges, and filters with 80 eye mesh screens.Filtrate reduced in volume, temperature is set as 70 DEG C.Concentrating gained extractum relative density
When being 1.10, being spray-dried, intake air temperature is 120 DEG C, and air outlet temperature is 90 DEG C, collects spray drying thing, low-temperature grinding, crosses 60
Mesh sieve, moisture is not higher than 12%, packs, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, labeling.
Above example, is only the technological thought that this invention is described, it is impossible to limit protection scope of the present invention whereby all
It is the technological thought proposed according to the present invention, any change done on the basis of technical scheme, each fall within present invention protection
Within the scope of.
Claims (2)
1. a Herba Euphorbiae Humifusae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof, it is characterised in that: adopt collection period Herba Euphorbiae Humifusae
Collecting its herb, clean, after washing, take advantage of fresh squeezing, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, filter press filter pressing
Extracting juice, remaining medicinal residues squeeze extracting juice again, merge three medicine juice, 40 ~ 120 mesh screen, obtain Herba Euphorbiae Humifusae medicine juice.
A kind of Herba Euphorbiae Humifusae fresh squeezing spray-dried powders decoction pieces the most according to claim 1 and preparation technology thereof, its feature exists
In: the Herba Euphorbiae Humifusae medicine juice obtained is evaporated under the conditions of 40 ~ 75 DEG C the concentrated solution that relative density is 1.02 ~ 1.15, and
Being spray-dried by this concentrated solution, intake air temperature is set as 90 ~ 140 DEG C, and air outlet temperature is 80 ~ 110 DEG C, collects to be dried and produces
Thing, crosses 60 ~ 100 mesh sieves, is vacuum-packed after pulverizing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610583305.9A CN106109543A (en) | 2016-07-24 | 2016-07-24 | A kind of Herba Euphorbiae Humifusae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610583305.9A CN106109543A (en) | 2016-07-24 | 2016-07-24 | A kind of Herba Euphorbiae Humifusae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
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| Publication Number | Publication Date |
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| CN106109543A true CN106109543A (en) | 2016-11-16 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610583305.9A Pending CN106109543A (en) | 2016-07-24 | 2016-07-24 | A kind of Herba Euphorbiae Humifusae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107157934A (en) * | 2017-06-19 | 2017-09-15 | 徐漫 | A kind of Ilex Latifolia Thunb is fresh to squeeze spray-dried powders medicine materical crude slice and its preparation technology |
| CN107334814A (en) * | 2017-08-25 | 2017-11-10 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Longtube Ground Ivy Herb |
| CN107362180A (en) * | 2017-08-25 | 2017-11-21 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of lycopodium calvatum |
| CN107375565A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of pipewort |
| CN107375378A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of gerbera |
| CN107375541A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of field pennycress |
| CN107441132A (en) * | 2017-08-25 | 2017-12-08 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of geranium wilfordii |
| CN107485645A (en) * | 2017-08-25 | 2017-12-19 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of mulberry leaf |
| CN107485638A (en) * | 2017-08-25 | 2017-12-19 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of lopseed |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105213553A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Hedyotidis Diffusae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
| CN105213444A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Portulacae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
| CN105213450A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Taraxaci fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
| CN105213460A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Radix et Caulis Opuntiae Dillenii fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
| CN105287860A (en) * | 2015-11-22 | 2016-02-03 | 徐漫 | Freshly-squeezed paulownia flower spray-dried powdery decoction piece and preparation technology thereof |
| CN105362528A (en) * | 2015-11-14 | 2016-03-02 | 芜湖天成普阳中药科技有限公司 | Folium Aloes fresh-squeezed spray-dried powder decoction pieces and preparation method thereof |
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2016
- 2016-07-24 CN CN201610583305.9A patent/CN106109543A/en active Pending
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| CN105213553A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Hedyotidis Diffusae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
| CN105213444A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Portulacae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
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| CN105213460A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Radix et Caulis Opuntiae Dillenii fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107157934A (en) * | 2017-06-19 | 2017-09-15 | 徐漫 | A kind of Ilex Latifolia Thunb is fresh to squeeze spray-dried powders medicine materical crude slice and its preparation technology |
| CN107334814A (en) * | 2017-08-25 | 2017-11-10 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Longtube Ground Ivy Herb |
| CN107362180A (en) * | 2017-08-25 | 2017-11-21 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of lycopodium calvatum |
| CN107375565A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of pipewort |
| CN107375378A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of gerbera |
| CN107375541A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of field pennycress |
| CN107441132A (en) * | 2017-08-25 | 2017-12-08 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of geranium wilfordii |
| CN107485645A (en) * | 2017-08-25 | 2017-12-19 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of mulberry leaf |
| CN107485638A (en) * | 2017-08-25 | 2017-12-19 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of lopseed |
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Application publication date: 20161116 |
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