CN106214723A - A kind of Herba Lobeliae Chinensis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof - Google Patents
A kind of Herba Lobeliae Chinensis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof Download PDFInfo
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- CN106214723A CN106214723A CN201610582772.XA CN201610582772A CN106214723A CN 106214723 A CN106214723 A CN 106214723A CN 201610582772 A CN201610582772 A CN 201610582772A CN 106214723 A CN106214723 A CN 106214723A
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- herba lobeliae
- lobeliae chinensis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/34—Campanulaceae (Bellflower family)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization
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- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
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- Biotechnology (AREA)
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- General Health & Medical Sciences (AREA)
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- Medicinal Preparation (AREA)
Abstract
The invention discloses a kind of Herba Lobeliae Chinensis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof.This technique, after Herba Lobeliae Chinensis medical material is gathered, cleans, drip washing, and takes advantage of fresh squeezing, leaching medicine juice.Medicinal residues add water stirring, filter squeezing.Concentrating under reduced pressure after the merging of gained medicine juice, is spray-dried, and collects spray drying product, size-reduced and first squeezing medicine juice mixing granulation, and granulate final vacuum is packed.Herba Lobeliae Chinensis granule pieces prepared by this method, remains the polarity in medical material and nonpolar effective ingredient to greatest extent.Granule pieces good fluidity, beneficially accumulating, convenient adjustment, quality controllable, curative effect is reliable, to ensureing that tcm clinical curative effect has great importance.The promotion and implementation of this law, will have significant social meaning and economic benefit.
Description
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Chinese medicine Herba Lobeliae Chinensis decoction pieces.
Background technology
Chinese medicine Herba Lobeliae Chinensis is campanulaceae lobelia herbaceos perennial Herba Lobeliae Chinensis Lobelia chinensis Lour.
Dry herb.This product nature and flavor are sweet flat, containing multiple alkaloid, have the effect of heat-clearing and toxic substances removing, inducing diuresis to remove edema, control venom, liver hard
Change ascites, advanced schistosomiasis ascites, appendicitis effect etc..
The processing mode of conventional Herba Lobeliae Chinensis decoction pieces is: summer, season in autumn two gather, and removes impurity, dries, then accumulating of packing.
This type of prepared herbal medicine in small pieces ready for decoction, bulky, Hygienic Index is poor, easily pollutes and goes mouldy, quality it is difficult to ensure that, be unfavorable for that formula is adjusted
With guarantee its clinical efficacy, even to patient bring recessiveness harm.
At present, granule pieces market also having Herba Lobeliae Chinensis medical material to make after extracting is sold.The preparation of granule pieces
Process, extracts not only time consumption and energy consumption, and because conventional substantial amounts of water does solvent, the nonpolar effective ingredient in medical material is difficult to be carried
Take out.Additionally, due to the Herba Lobeliae Chinensis medical material extracted also is to be dried and through long-time storage, therefore, effective ingredient
Loss is also the biggest.In order to ensure Herba Lobeliae Chinensis medical material clinical effectively, steady quality, a kind of novel Herba Lobeliae Chinensis decoction pieces and
Preparation technology urgently develops.
Summary of the invention
The invention discloses " a kind of Herba Lobeliae Chinensis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof ".This technique is permissible
Retain the polarity in Herba Lobeliae Chinensis medical material and nonpolar effective ingredient to greatest extent, it is to avoid medical material is in the processing of existing decoction pieces and storage
The loss of the effective ingredient caused during fortune and the decline of medical material quanlity, reduce the medical material pollution by mycete etc., to guaranteeing half
Steady quality and the clinical safety of limit lotus decoction pieces effectively have great importance.
To achieve these goals, the technical scheme is that
Gather its herb collection period Herba Lobeliae Chinensis, clean, after washing, take advantage of fresh squeezing, collect and just squeeze medicine juice, retain 0.5% ~ 5%
Just squeezing medicine juice standby, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, and filter press filter pressing extracting juice, remaining medicinal residues are pressed again
Extracting juice, merges remaining just squeezing medicine juice and rear twice squeezing medicine juice, 60 ~ 120 mesh screen, obtains Herba Lobeliae Chinensis medicine juice.To obtain
Herba Lobeliae Chinensis medicine juice under the conditions of 40 ~ 75 DEG C, be evaporated to the concentrated solution that relative density is 1.02 ~ 1.15, and by this concentrated solution
Being spray-dried, intake air temperature is set as 90 ~ 140 DEG C, and air outlet temperature is 80 ~ 110 DEG C, collects desciccate, mistake after pulverizing
60 ~ 100 mesh sieves.By above-mentioned Herba Lobeliae Chinensis spray drying powder, mix with the first squeezing medicine juice retained, prepare soft material, pelletize, 50 ~ 80 DEG C
It is dried 4 ~ 8 hours, granulate, vacuum packaging.On the label of product packaging bags, the name of an article, medicinal part, planting site, drink in printing
Sheet manufacturer, date of manufacture, Contents of Main Components, meridian distribution of property and flavor, function cure mainly, usage and dosage, toxic and side effects and contraindication etc.
Information.The thin layer of the included upper lotus of bag differentiates collection of illustrative plates and/or high-efficient liquid phase character collection of illustrative plates, as " identity card " of product.This
Outward, in the packaging bag of product, be printed on Quick Response Code, by scanning can link acquisition the former plant photo of product, medical material photo,
The information such as decoction pieces photo, character and microscopical identification feature.
The invention have benefit that:
The Herba Lobeliae Chinensis medical material of fresh collection, directly squeezes after cleaning washing, filters, concentrating under reduced pressure, is spray-dried, pelletizes, gained
The granule pieces arrived, can retain the effective ingredient in medical material to greatest extent.This decoction pieces volume compares to tradition decoction pieces body
Amass and be greatly reduced, good fluidity, vacuum packaging so that prepared slice quality is more stable, beneficially accumulating and clinical adjustment, have ten
Divide significant social meaning and economic implications.
Detailed description of the invention
Embodiment 1
By the Herba Lobeliae Chinensis medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice, retain 1% weight
First squeezing medicine juice separately use.Gained medicinal residues add the tap water of 3 times amount, stir 20min, filter press squeezing extracting juice.Remaining medicine
Slag squeezes extracting juice with squeezer again.The above-mentioned remaining medicine juice that just squeezes is merged, by 100 eye mesh screen mistakes with follow-up twice squeezing medicine juice
Filter.Filtrate reduced in volume, temperature is set as 65 DEG C.When concentrating gained extractum relative density and being 1.05, it is spray-dried, air inlet
Temperature is 140 DEG C, and air outlet temperature is 100 DEG C, collects spray drying thing, low-temperature grinding, crosses 80 mesh sieves.By this spray drying powder with upper
The first squeezing medicine juice stating retention mixes soft material processed, pelletizes, and 75 DEG C are dried 6 hours, granulate, pack, and 1kg/ bag adds packed antioxidant
And desiccant, Vacuum Package, labeling.
Embodiment 2
By the Herba Lobeliae Chinensis medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice, retain 5% weight
First squeezing medicine juice separately use.Gained medicinal residues add the tap water of 5 times amount, stir 30min, filter press squeezing extracting juice.Remaining medicine
Slag squeezes extracting juice with squeezer again.The above-mentioned remaining medicine juice that just squeezes is merged, by 100 eye mesh screen mistakes with follow-up twice squeezing medicine juice
Filter.Filtrate reduced in volume, temperature is set as 70 DEG C.When concentrating gained extractum relative density and being 1.10, it is spray-dried, air inlet
Temperature is 120 DEG C, and air outlet temperature is 90 DEG C, collects spray drying thing, low-temperature grinding, crosses 80 mesh sieves.By this spray drying powder with upper
The first squeezing medicine juice stating retention mixes soft material processed, pelletizes, and 70 DEG C are dried 8 hours, granulate, pack, and 1kg/ bag adds packed antioxidant
And desiccant, Vacuum Package, labeling.
Above example, is only the technological thought that this invention is described, it is impossible to limit protection scope of the present invention whereby
Every technological thought proposed according to the present invention, any change done on the basis of technical scheme, each fall within present invention protection
Within the scope of.
Claims (3)
1. a Herba Lobeliae Chinensis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof, it is characterised in that: adopt collection period Herba Lobeliae Chinensis
Collecting its herb, clean, after washing, take advantage of fresh squeezing, collect and just squeeze medicine juice, the first squeezing medicine juice of retention 0.5% ~ 5% is standby, and medicinal residues add
The water of 1 ~ 5 times amount, stirs 5 ~ 30min, filter press filter pressing extracting juice, and remaining medicinal residues squeeze extracting juice again, merges remaining just squeezing
Medicine juice and rear twice squeezing medicine juice, 60 ~ 120 mesh screen, obtain Herba Lobeliae Chinensis medicine juice.
A kind of Herba Lobeliae Chinensis fresh squeezing spray-dried granules decoction pieces the most according to claim 1 and preparation technology thereof, its feature exists
In: the Herba Lobeliae Chinensis medicine juice obtained is evaporated under the conditions of 40 ~ 75 DEG C the concentrated solution that relative density is 1.02 ~ 1.15, and
Being spray-dried by this concentrated solution, intake air temperature is set as 90 ~ 140 DEG C, and air outlet temperature is 80 ~ 110 DEG C, collects to be dried and produces
Thing, crosses 60 ~ 100 mesh sieves after pulverizing.
A kind of Herba Lobeliae Chinensis fresh squeezing spray-dried granules decoction pieces the most according to claim 1 and preparation technology thereof, its feature exists
In: by the Herba Lobeliae Chinensis spray drying powder in claim 2, mix with the first squeezing medicine juice retained in claim 1, prepare soft material,
Pelletizing, 50 ~ 80 DEG C are dried 4 ~ 8 hours, and granulate is vacuum-packed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610582772.XA CN106214723A (en) | 2016-07-23 | 2016-07-23 | A kind of Herba Lobeliae Chinensis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610582772.XA CN106214723A (en) | 2016-07-23 | 2016-07-23 | A kind of Herba Lobeliae Chinensis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
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| CN106214723A true CN106214723A (en) | 2016-12-14 |
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| CN201610582772.XA Pending CN106214723A (en) | 2016-07-23 | 2016-07-23 | A kind of Herba Lobeliae Chinensis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107233377A (en) * | 2017-06-19 | 2017-10-10 | 徐漫 | A kind of field thistle is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
| CN107281236A (en) * | 2017-06-19 | 2017-10-24 | 徐漫 | A kind of Ilex Latifolia Thunb is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
| CN107334796A (en) * | 2017-08-25 | 2017-11-10 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of ardisia japonica |
| CN107375543A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of field pennycress |
| CN107375417A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of Herba Lycopi |
| CN107375379A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of gerbera |
| CN107375349A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of scouring rush |
| CN107375370A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of coriander |
| CN107375403A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of gynostemma pentaphylla |
| CN107375364A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of desmodium |
| CN107375529A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of bittersweet |
| CN107412327A (en) * | 2017-08-25 | 2017-12-01 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of elscholtiza |
| CN107412434A (en) * | 2017-08-25 | 2017-12-01 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of black nightshade |
| CN107441380A (en) * | 2017-08-25 | 2017-12-08 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of lophatherum gracile |
| CN107485639A (en) * | 2017-08-25 | 2017-12-19 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of lopseed |
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| CN105287858A (en) * | 2015-11-22 | 2016-02-03 | 徐漫 | Freshly-squeezed paulownia flower spray-dried granular decoction piece and preparation technology thereof |
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107233377A (en) * | 2017-06-19 | 2017-10-10 | 徐漫 | A kind of field thistle is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
| CN107281236A (en) * | 2017-06-19 | 2017-10-24 | 徐漫 | A kind of Ilex Latifolia Thunb is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
| CN107334796A (en) * | 2017-08-25 | 2017-11-10 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of ardisia japonica |
| CN107375543A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of field pennycress |
| CN107375417A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of Herba Lycopi |
| CN107375379A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of gerbera |
| CN107375349A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of scouring rush |
| CN107375370A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of coriander |
| CN107375403A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of gynostemma pentaphylla |
| CN107375364A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of desmodium |
| CN107375529A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of bittersweet |
| CN107412327A (en) * | 2017-08-25 | 2017-12-01 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of elscholtiza |
| CN107412434A (en) * | 2017-08-25 | 2017-12-01 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of black nightshade |
| CN107441380A (en) * | 2017-08-25 | 2017-12-08 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of lophatherum gracile |
| CN107485639A (en) * | 2017-08-25 | 2017-12-19 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of lopseed |
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Application publication date: 20161214 |