CN105213551A - A kind of Herba Hedyotidis Diffusae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof - Google Patents
A kind of Herba Hedyotidis Diffusae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof Download PDFInfo
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- CN105213551A CN105213551A CN201510774858.8A CN201510774858A CN105213551A CN 105213551 A CN105213551 A CN 105213551A CN 201510774858 A CN201510774858 A CN 201510774858A CN 105213551 A CN105213551 A CN 105213551A
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Abstract
The present invention discloses a kind of Herba Hedyotidis Diffusae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof.This technique, after Herba Hedyotidis Diffusae medical material is gathered, to clean, drip washing, and takes advantage of fresh squeezing, leaching medicine juice.Medicinal residues add water stirring again, filter squeezing.Concentrating under reduced pressure after gained medicine juice merges, spraying dry, soft material processed after pulverizing, granulates, dry, and granulate final vacuum is packed.The Herba Hedyotidis Diffusae granule pieces that this legal system is standby, good fluidity, remains the polarity in medical material and nonpolar effective ingredient to greatest extent.Decoction pieces is beneficial to accumulating, convenient adjustment, and quality controllable, curative effect is reliable, has great importance to guarantee tcm clinical curative effect.The promotion and implementation of this law, will have significant social meaning and economic benefit.
Description
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Chinese medicine Herba Hedyotidis Diffusae decoction pieces.
Background technology
Chinese medicine Herba Hedyotidis Diffusae is Maguireothamnus speciosus Herba Hedyotidis Diffusae
oldenlandiadiffusa(Willd.) the dry herb of Roxb. is bitter in the mouth, light, cold in nature.This product has effect of heat-clearing and toxic substances removing, medicinal powder for relieving pain knot, promoting urination to remove dampness.Can be used for the diseases such as treatment dyspnea and cough due to lung-heat, laryngopharynx swelling and pain, acute appendicitis, furuncle and phyma skin infection, venom, the puckery pain of pyretic stranguria, dysentery, enteritis.
The processing mode of conventional Herba Hedyotidis Diffusae decoction pieces is: after herb of gathering, and removing impurity, cleans silt, dry, then accumulating of packing.This type of prepared herbal medicine in small pieces ready for decoction, bulky, easily pollute and go mouldy, quality is difficult to ensure, is unfavorable for that formula is adjusted and guarantees its clinical efficacy, even brings recessive harm to patient.
At present, granule pieces market also having Herba Hedyotidis Diffusae medical material to make after extracting is sold.The preparation process of granule pieces, extracts not only time consumption and energy consumption, and does solvent because commonly using a large amount of water, and the nonpolar effective ingredient in medical material is difficult to be extracted.In addition, because the Herba Hedyotidis Diffusae medical material extracted also is dry also through long-time storage, therefore, the loss of effective ingredient is also very large.In order to ensure clinical effective, the steady quality of Herba Hedyotidis Diffusae medical material, a kind of novel Herba Hedyotidis Diffusae decoction pieces and preparation technology thereof urgently develop.
Summary of the invention
The present invention discloses " a kind of Herba Hedyotidis Diffusae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof ".This technique can retain polarity in Herba Hedyotidis Diffusae medical material and nonpolar effective ingredient to greatest extent, the loss of effective ingredient avoiding medical material to cause in existing decoction pieces processing and storage and transport process and the decline of medical material quanlity, reduce the pollution of medical material by mycete etc., the steady quality and clinical safety guaranteeing Herba Hedyotidis Diffusae decoction pieces is effectively had great importance.
To achieve these goals, technical scheme of the present invention is:
Gather its herb collection period Herba Hedyotidis Diffusae, clean, after washing, take advantage of the section that fresh-cut becomes 1 ~ 10cm, squeezing extracting juice, retain 0.5% ~ 5% medicine juice separately use, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, filter press filter pressing extracting juice, remaining medicinal residues squeeze extracting juice again, merge three squeezings except the medicine juice retaining another use, 80 ~ 120 mesh screen, obtain Herba Hedyotidis Diffusae medicine juice.The Herba Hedyotidis Diffusae medicine juice obtained is evaporated to the concentrated solution that relative density is 1.05 ~ 1.15 under 40 ~ 75 DEG C of conditions, and by this concentrated solution spraying dry, intake air temperature is 90 ~ 140 DEG C, air outlet temperature is 70 ~ 120 DEG C, collect spray dry product, pulverized 40 ~ 100 mesh sieves, and obtained spray powder.By this spray powder, with the medicine juice of above-mentioned retention, mix soft material processed, granulate, dry, granulate, vacuum packaging, obtains product.
On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, decoction pieces manufacturer, date of manufacture, Contents of Main Components, meridian distribution of property and flavor, function cure mainly, the information such as usage and dosage, toxic and side effects and contraindication.TLC distinguish collection of illustrative plates and/or the high-efficient liquid phase character collection of illustrative plates of Herba Hedyotidis Diffusae is enclosed, as " identity card " of product in bag.In addition, in the packaging bag of product, be printed on Quick Response Code, the information such as former plant photo, medical material photo, decoction pieces photo, character and the microscopical identification feature obtaining product can be linked by scanning.
Usefulness of the present invention is:
The Herba Hedyotidis Diffusae medical material of fresh collection, direct squeezing, filtration, concentrating under reduced pressure, spraying dry after cleaning washing, the powder decoction pieces obtained, can retain the effective ingredient in medical material to greatest extent.This decoction pieces volume compares to traditional decoction pieces volume and reduces widely, and vacuum packaging, makes prepared slice quality more stable, is beneficial to accumulating and clinical adjustment, has very significant social meaning and economic implications.
Detailed description of the invention
Embodiment 1
By the Herba Hedyotidis Diffusae medical material of fresh collection, clean, wash silt with water, take advantage of the section that fresh-cut becomes 5cm, squeeze extracting juice with squeezer, the medicine juice retaining 1% weight is separately used.Gained medicinal residues add the tap water of 3 times amount, stir 20min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.The medicine juice of above-mentioned 3 squeezings is merged, filters with 100 eye mesh screens.Filtrate reduced in volume, temperature is set as 65 DEG C.When concentrated gained extractum relative density is 1.05, transfer to spray drying tower, intake air temperature is 120 DEG C, and air outlet temperature is 100 DEG C, collects spray dry product, pulverizes, cross 80 mesh sieves.By this spray drying powder, mix homogeneously with the medicine juice of above-mentioned retention, soft material processed, granulates, and dries, granulate, and collection can all by 24 mesh sieves, and not by the granule of 60 mesh sieves, pack, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package.
Embodiment 2
By the Herba Hedyotidis Diffusae medical material of fresh collection, clean, wash silt with water, take advantage of the section that fresh-cut becomes 10cm, squeeze extracting juice with squeezer, the medicine juice retaining 3% weight is separately used.Gained medicinal residues add the tap water of 5 times amount, stir 30min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.The medicine juice of above-mentioned 3 squeezings is merged, filters with 100 eye mesh screens.Filtrate reduced in volume, temperature is set as 70 DEG C.When concentrated gained extractum relative density is 1.02, transfer to spray drying tower, intake air temperature is 140 DEG C, and air outlet temperature is 110 DEG C, collects spray dry product, pulverizes, cross 80 mesh sieves.By this spray drying powder, mix homogeneously with the medicine juice of above-mentioned retention, soft material processed, granulates, and dries, granulate, and collection can all by 24 mesh sieves, and not by the granule of 60 mesh sieves, pack, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package.
Above embodiment, is only the technological thought that this invention is described, can not limit the every technological thought proposed according to the present invention of protection scope of the present invention whereby, any change that technical scheme basis is done, all falls within the scope of protection of the invention.
Claims (3)
1. Herba Hedyotidis Diffusae fresh squeezing spray-dried powders decoction pieces and a preparation technology thereof, is characterized in that: gather its herb collection period Herba Hedyotidis Diffusae, clean, after washing, take advantage of the section that fresh-cut becomes 1 ~ 10cm, squeezing extracting juice, retain 0.5% ~ 5% medicine juice separately to use, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, filter press filter pressing extracting juice, remaining medicinal residues squeeze extracting juice again, merge three squeezings except the medicine juice retaining another use, 80 ~ 120 mesh screen, obtain Herba Hedyotidis Diffusae medicine juice.
2. a kind of Herba Hedyotidis Diffusae fresh squeezing spray-dried powders decoction pieces according to claim 1 and preparation technology thereof, it is characterized in that: the Herba Hedyotidis Diffusae medicine juice obtained in claim 1 is evaporated to the concentrated solution that relative density is 1.05 ~ 1.15 under 40 ~ 75 DEG C of conditions, and by this concentrated solution spraying dry, intake air temperature is 90 ~ 140 DEG C, air outlet temperature is 70 ~ 120 DEG C, collect spray dry product, pulverized 40 ~ 100 mesh sieves, and obtained spray powder.
3. a kind of Herba Hedyotidis Diffusae fresh squeezing spray-dried powders decoction pieces according to claim 1 and preparation technology thereof, is characterized in that: by the spray powder in claim 2, with the retention medicine juice in claim 1, mix soft material processed, granulate, dry, granulate, vacuum packaging, obtains product.
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| CN106038491A (en) * | 2016-07-23 | 2016-10-26 | 徐漫 | Freshly squeezed and spray-dried granular decoction pieces with verbena officinalis and process for preparing freshly squeezed and spray-dried granular decoction pieces |
| CN106109622A (en) * | 2016-07-23 | 2016-11-16 | 徐漫 | A kind of Herba Agrimoniae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN106109530A (en) * | 2016-07-23 | 2016-11-16 | 徐漫 | A kind of Folium Isatidis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN106109575A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Scutellariae Barbatae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN106214723A (en) * | 2016-07-23 | 2016-12-14 | 徐漫 | A kind of Herba Lobeliae Chinensis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN107050328A (en) * | 2017-03-07 | 2017-08-18 | 重庆医药高等专科学校 | A kind of reed rhizome is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107050327A (en) * | 2017-03-07 | 2017-08-18 | 重庆医药高等专科学校 | A kind of rhizoma imperatae is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107080760A (en) * | 2017-03-07 | 2017-08-22 | 重庆医药高等专科学校 | A kind of desmodium is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107213186A (en) * | 2017-06-20 | 2017-09-29 | 徐漫 | A kind of acalypha copperleaf is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
| CN107233384A (en) * | 2017-06-22 | 2017-10-10 | 徐漫 | A kind of motherwort is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
| CN107320508A (en) * | 2017-08-25 | 2017-11-07 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of Chinese trumpet creeper |
| CN107320527A (en) * | 2017-08-25 | 2017-11-07 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of mulberry leaf |
| CN107334796A (en) * | 2017-08-25 | 2017-11-10 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of ardisia japonica |
| CN107334790A (en) * | 2017-08-25 | 2017-11-10 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of phoenix-tail fern |
| CN107334797A (en) * | 2017-08-25 | 2017-11-10 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of Chinese trumpet creeper |
| CN107334814A (en) * | 2017-08-25 | 2017-11-10 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Longtube Ground Ivy Herb |
| CN107375385A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of Artemisia anomala |
| CN107375556A (en) * | 2017-08-25 | 2017-11-24 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Chinese violet |
| CN107375379A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of gerbera |
| CN107375410A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of Canton love-pea vine |
| CN107375403A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of gynostemma pentaphylla |
| CN107375370A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of coriander |
| CN107375389A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of oriental wormwood |
| CN107375417A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of Herba Lycopi |
| CN107375395A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of fringed pink |
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| CN107375566A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of pipewort |
| CN107375349A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of scouring rush |
| CN107375433A (en) * | 2017-08-25 | 2017-11-24 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of mulberry leaf |
| CN107397788A (en) * | 2017-08-25 | 2017-11-28 | 徐自升 | A kind of schizonepeta is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
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| CN107412285A (en) * | 2017-08-25 | 2017-12-01 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of lycopodium calvatum |
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| CN107412327A (en) * | 2017-08-25 | 2017-12-01 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of elscholtiza |
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| CN107468831A (en) * | 2017-08-25 | 2017-12-15 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of Chinese violet |
| CN107468751A (en) * | 2017-08-25 | 2017-12-15 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of Longtube Ground Ivy Herb |
| CN107485639A (en) * | 2017-08-25 | 2017-12-19 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of lopseed |
| CN108619412A (en) * | 2018-07-06 | 2018-10-09 | 徐自升 | Rhizoma imperatae is fresh to carry spray-dried granules medicine materical crude slice |
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