CN107375379A - A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of gerbera - Google Patents
A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of gerbera Download PDFInfo
- Publication number
- CN107375379A CN107375379A CN201710738581.2A CN201710738581A CN107375379A CN 107375379 A CN107375379 A CN 107375379A CN 201710738581 A CN201710738581 A CN 201710738581A CN 107375379 A CN107375379 A CN 107375379A
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- China
- Prior art keywords
- gerbera
- squeezing
- concoction
- spray
- crude slice
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 241000735332 Gerbera Species 0.000 title claims abstract description 28
- 239000003814 drug Substances 0.000 title claims abstract description 20
- 238000005516 engineering process Methods 0.000 title claims abstract description 10
- 239000008187 granular material Substances 0.000 title claims abstract description 10
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- 239000000463 material Substances 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 238000003756 stirring Methods 0.000 claims abstract description 8
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 239000012141 concentrate Substances 0.000 claims description 5
- 230000014759 maintenance of location Effects 0.000 claims description 5
- 238000004806 packaging method and process Methods 0.000 claims description 4
- 239000011122 softwood Substances 0.000 claims description 4
- 239000007921 spray Substances 0.000 claims description 4
- 235000020985 whole grains Nutrition 0.000 claims description 4
- 230000000717 retained effect Effects 0.000 claims 1
- 239000004480 active ingredient Substances 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 4
- 238000002386 leaching Methods 0.000 abstract description 3
- 238000000034 method Methods 0.000 abstract description 3
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 238000003306 harvesting Methods 0.000 abstract description 2
- 230000000192 social effect Effects 0.000 abstract description 2
- 229940079593 drug Drugs 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 description 4
- 238000000605 extraction Methods 0.000 description 3
- 239000003963 antioxidant agent Substances 0.000 description 2
- 230000003078 antioxidant effect Effects 0.000 description 2
- 230000006837 decompression Effects 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 238000002372 labelling Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000012567 medical material Substances 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 244000025254 Cannabis sativa Species 0.000 description 1
- 206010007247 Carbuncle Diseases 0.000 description 1
- 235000008495 Chrysanthemum leucanthemum Nutrition 0.000 description 1
- 244000192528 Chrysanthemum parthenium Species 0.000 description 1
- 235000000604 Chrysanthemum parthenium Nutrition 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- 229920001353 Dextrin Polymers 0.000 description 1
- 239000004375 Dextrin Substances 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010017553 Furuncle Diseases 0.000 description 1
- 206010018612 Gonorrhoea Diseases 0.000 description 1
- 208000004880 Polyuria Diseases 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 235000019425 dextrin Nutrition 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000035619 diuresis Effects 0.000 description 1
- 208000001848 dysentery Diseases 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 235000008384 feverfew Nutrition 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 208000001786 gonorrhea Diseases 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 201000003068 rheumatic fever Diseases 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/16—Agglomerates; Granulates; Microbeadlets ; Microspheres; Pellets; Solid products obtained by spray drying, spray freeze drying, spray congealing,(multiple) emulsion solvent evaporation or extraction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/13—Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation or decoction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
Landscapes
- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Epidemiology (AREA)
- Medicinal Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Alternative & Traditional Medicine (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Medical Informatics (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of gerbera.The technique is cleaned, eluted after the harvesting of gerbera medicinal material, and takes advantage of fresh squeezing, leaching concoction.The dregs of a decoction add water stirring, filtering squeezing.Gained concoction is concentrated under reduced pressure after merging, and is spray-dried, then particle is made.Gerbera granule pieces prepared by this method, not only good fluidity, and to greatest extent while remain polarity and nonpolar active ingredient in medicinal material.Medicine materical crude slice is beneficial to accumulating, and convenient to adjust, quality controllable, curative effect is reliable, to ensureing that tcm clinical curative effect has great importance.The promotion and implementation of this law, will there are significant social effect and economic benefit.
Description
Technical field
The invention belongs to Chinese medicine manufacture field, more particularly to the processing technology of Chinese medicine gerbera medicine materical crude slice.
Background technology
Chinese medicine gerbera is the herb of feverfew gerbera.The effect of with clearing heat and promoting diuresis, removing toxicity for detumescence.Clinic cures mainly
Cough with lung heat, damp-heat dysentery, heat gonorrhea, rheumatic arthritis, carbuncle furuncle poison etc..
The processing mode of conventional gerbera medicine materical crude slice is：After harvesting, impurity is removed, is dried, directly packing storage and transport.
These dry gerbera Hygienic Indexes can not be up to standard, easily occur medicinal material go mouldy, so as to cause the decline of medical material quanlity and
The reduction of clinical efficacy.Such prepared herbal medicine in small pieces ready for decoction, it is bulky, easily occur it is rotten and contaminated, quality it is difficult to ensure that, be unfavorable for adjusting
Agent prescription and ensure its clinical efficacy.
At present, in the market also has the manufactured granule pieces sale after extraction of gerbera medicinal material.Due to granule pieces system
During standby, extraction not only time consumption and energy consumption, and also because conventional water does solvent, the nonpolar active ingredient in medicinal material is difficult to be extracted
Out.Further, since the gerbera medicinal material of extraction is also to dry and stored by long-time, therefore, its raw material easily pollutes
It is difficult to avoid to be also with situation about going mouldy.In order to ensure gerbera medicinal material clinic effectively, steady quality, it is a kind of new big
Fourth grass medicine materical crude slice and its preparation technology urgently develop.
The content of the invention
The invention discloses " a kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of gerbera ".This technique can be most
The polarity and the nonpolar active ingredient that retain in gerbera medicinal material of limits, avoid medicinal material from being processed and accumulating in existing medicine materical crude slice
During the loss of caused active ingredient and the decline of medical material quanlity, reduce medicinal material by mould etc. pollution, to ensuring big fourth
The steady quality and clinical safety of careless medicine materical crude slice effectively have great importance.
To achieve these goals, the technical scheme is that：
Its herb is gathered in gerbera picking time, is cleaned, is cut into 1 ~ 2cm section, the water of 0.5 ~ 1 times of amount of medicinal material weight is added, stirs
Mix 15 ~ 30 minutes, take advantage of fresh squeezing, collect and just squeeze concoction, the first squeezing concoction of 0.1% ~ 0.5% weight of retention is standby, and the dregs of a decoction add 1 ~ 5
The water of amount again, 5 ~ 30min is stirred, press extracting juice, the remaining dregs of a decoction add the water of 1 ~ 5 times of amount, pressure extracting juice, merge and just squeeze concoction
Concoction is squeezed after and twice, 100 ~ 200 mesh screens, obtains gerbera concoction.By the concoction of gained, it is concentrated under reduced pressure in 40 ~ 80 DEG C,
Obtain the concentrate that relative density is 1.02 ~ 1.10.This concentrate is spray-dried, intake air temperature is set as 100 ~
140 DEG C, air outlet temperature is set as 90 ~ 120 DEG C, collects dried object and is crushed, crosses 60 ~ 100 mesh sieves.By above-mentioned retention
Just squeeze concoction to mix with obtained spray powder, add appropriate starch and dextrin as one sees fit, prepare softwood, pelletize, dry, whole grain,
Packaging.
It is the name of an article in printing, medicinal part, planting site, manufacturer, the date of manufacture, main on the label of product packaging bags
The information such as component content, meridian distribution of property and flavor, major function, usage and dosage, toxic side effect and contraindication.The thin of gerbera is enclosed in bag
Layer differentiates collection of illustrative plates and/or efficient liquid phase characteristic spectrum, " identity card " as product.In addition, in the packaging bag of product, it is printed on
Quick Response Code, former plant photo, medicinal material photo, medicine materical crude slice photo, character and the microscopical characters for obtaining product can be linked by scanning
The information such as feature.
The present invention is advantageous in that：
Fresh gerbera medicinal material directly squeezes after cleaning washing, filter, be concentrated under reduced pressure, being spray-dried, pelletize after, resulting
Grain medicine materical crude slice, not only good fluidity, moreover it is possible to retain the active ingredient in medicinal material to greatest extent.This medicine materical crude slice volume is compared to biography
System medicine materical crude slice volume greatly reduces, and quality is more stable, beneficial to accumulating and it is clinical adjust, have very significant social effect and
Economic implications.
Embodiment
Embodiment 1
By the gerbera medicinal material of fresh collection, clean, clean, be cut into 1cm section, add the water of 0.5 times of amount of medicinal material weight, stirring
15 minutes, fresh squeezing is taken advantage of, retain this first squeezing concoction 0.1% is standby.The gained dregs of a decoction add the running water of 2 times of amounts, stir 20min, plate
Frame filter press presses extracting juice.The gained dregs of a decoction are squeezed with squeezer again, leaching concoction.Above-mentioned 3 gerbera concoctions are merged, with 60
Mesh screen, filtrate decompression concentration, temperature are set as 60 DEG C.When gained concentrate relative density is 1.03, spraying is transferred to
Drying tower is spray-dried, and intake air temperature is set as 140 DEG C, and air outlet temperature is set as 110 DEG C, collects dried object, powder
It is broken, cross 60 mesh sieves.By this spray powder, softwood processed is mixed with the first squeezing concoction of above-mentioned retention, is pelletized, is dried, whole grain, pack,
1kg/ bags, add packed antioxidant and drier, Vacuum Package, labeling.
Embodiment 2
By the gerbera medicinal material of fresh collection, clean, clean, be cut into 2cm section, add the water of 1 times of amount of medicinal material weight, stirring 30
Minute, fresh squeezing is taken advantage of, retain this first squeezing concoction 0.3% is standby.The gained dregs of a decoction add the running water of 5 times of amounts, stir 30min, sheet frame
Filter press presses extracting juice.The gained dregs of a decoction are squeezed with squeezer again, leaching concoction.Above-mentioned 3 gerbera concoctions are merged, with 100
Mesh screen, filtrate decompression concentration, temperature are set as 70 DEG C.When gained concentrate relative density is 1.05, spraying is transferred to
Drying tower is spray-dried, and intake air temperature is set as 120 DEG C, and air outlet temperature is set as 90 DEG C, collects dried object, powder
It is broken, cross 60 mesh sieves.By this spray powder, softwood processed is mixed with the first squeezing concoction of above-mentioned retention, is pelletized, is dried, whole grain, pack,
1kg/ bags, add packed antioxidant and drier, Vacuum Package, labeling.
Above example, only illustrate the technological thought of this invention, it is impossible to it is all whereby to limit protection scope of the present invention
It is any change for being done on the basis of technical scheme according to technological thought proposed by the present invention, each falls within what the present invention protected
Within the scope of.
Claims (3)
- A kind of 1. fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of gerbera, it is characterised in that：Gathered in gerbera picking time Its herb, clean, be cut into 1 ~ 2cm section, add the water of 0.5 ~ 1 times of amount of medicinal material weight, stir 15 ~ 30 minutes, take advantage of fresh squeezing, receive Collection just squeezes concoction, and the first squeezing concoction of 0.1% ~ 0.5% weight of retention is standby, and the dregs of a decoction add the water of 1 ~ 5 times of amount, stirs 5 ~ 30min, pressure Extracting juice, the remaining dregs of a decoction add the water of 1 ~ 5 times of amount, press extracting juice, merge just squeeze concoction and after squeeze concoction twice, 100 ~ 200 mesh screens, obtain gerbera concoction.
- A kind of 2. fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of gerbera according to claim 1, it is characterised in that： By the concoction of gained in claim 1, it is concentrated under reduced pressure in 40 ~ 80 DEG C, obtains the concentrate that relative density is 1.02 ~ 1.10, it is right It is spray-dried, and intake air temperature is set as 100 ~ 140 DEG C, and air outlet temperature is set as 90 ~ 120 DEG C, collects dried object Crushed, cross 60 ~ 100 mesh sieves.
- A kind of 3. fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of gerbera according to claim 1, it is characterised in that： The first squeezing concoction retained in claim 1 is mixed with the spray powder obtained in claim 2, prepares softwood, is pelletized, is dried, Whole grain, packaging.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710738581.2A CN107375379A (en) | 2017-08-25 | 2017-08-25 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of gerbera |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710738581.2A CN107375379A (en) | 2017-08-25 | 2017-08-25 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of gerbera |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107375379A true CN107375379A (en) | 2017-11-24 |
Family
ID=60346021
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710738581.2A Pending CN107375379A (en) | 2017-08-25 | 2017-08-25 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of gerbera |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107375379A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105213551A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Hedyotidis Diffusae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN105213660A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Aloe fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN106109530A (en) * | 2016-07-23 | 2016-11-16 | 徐漫 | A kind of Folium Isatidis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN106214723A (en) * | 2016-07-23 | 2016-12-14 | 徐漫 | A kind of Herba Lobeliae Chinensis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
-
2017
- 2017-08-25 CN CN201710738581.2A patent/CN107375379A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105213551A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Hedyotidis Diffusae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN105213660A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Aloe fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN106109530A (en) * | 2016-07-23 | 2016-11-16 | 徐漫 | A kind of Folium Isatidis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN106214723A (en) * | 2016-07-23 | 2016-12-14 | 徐漫 | A kind of Herba Lobeliae Chinensis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
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