CN106038491A - Freshly squeezed and spray-dried granular decoction pieces with verbena officinalis and process for preparing freshly squeezed and spray-dried granular decoction pieces - Google Patents
Freshly squeezed and spray-dried granular decoction pieces with verbena officinalis and process for preparing freshly squeezed and spray-dried granular decoction pieces Download PDFInfo
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- CN106038491A CN106038491A CN201610582773.4A CN201610582773A CN106038491A CN 106038491 A CN106038491 A CN 106038491A CN 201610582773 A CN201610582773 A CN 201610582773A CN 106038491 A CN106038491 A CN 106038491A
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- decoction pieces
- medicine juice
- dried
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- 238000004519 manufacturing process Methods 0.000 title abstract description 4
- 235000018718 Verbena officinalis Nutrition 0.000 title abstract 5
- 240000001519 Verbena officinalis Species 0.000 title abstract 5
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 39
- 239000003814 drug Substances 0.000 claims abstract description 38
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 230000008901 benefit Effects 0.000 claims abstract description 7
- 238000001694 spray drying Methods 0.000 claims abstract description 7
- 238000003756 stirring Methods 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims abstract description 4
- 238000005520 cutting process Methods 0.000 claims abstract 2
- 239000008187 granular material Substances 0.000 claims description 12
- 238000005516 engineering process Methods 0.000 claims description 7
- 238000002360 preparation method Methods 0.000 claims description 7
- 239000000843 powder Substances 0.000 claims description 4
- 239000007779 soft material Substances 0.000 claims description 4
- 230000014759 maintenance of location Effects 0.000 claims description 3
- 239000002893 slag Substances 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- 238000003825 pressing Methods 0.000 claims description 2
- 238000010298 pulverizing process Methods 0.000 claims description 2
- 230000000717 retained effect Effects 0.000 claims description 2
- 238000005453 pelletization Methods 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 4
- 238000003860 storage Methods 0.000 abstract description 4
- 238000004806 packaging method and process Methods 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract 3
- 238000001914 filtration Methods 0.000 abstract 2
- 230000002349 favourable effect Effects 0.000 abstract 1
- 238000003306 harvesting Methods 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 238000007493 shaping process Methods 0.000 abstract 1
- 229940126680 traditional chinese medicines Drugs 0.000 abstract 1
- 239000012567 medical material Substances 0.000 description 13
- 239000004615 ingredient Substances 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 239000003963 antioxidant agent Substances 0.000 description 2
- 230000003078 antioxidant effect Effects 0.000 description 2
- 239000002274 desiccant Substances 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 238000002372 labelling Methods 0.000 description 2
- 201000004792 malaria Diseases 0.000 description 2
- 239000008399 tap water Substances 0.000 description 2
- 235000020679 tap water Nutrition 0.000 description 2
- 238000009461 vacuum packaging Methods 0.000 description 2
- 206010000077 Abdominal mass Diseases 0.000 description 1
- 201000000736 Amenorrhea Diseases 0.000 description 1
- 206010001928 Amenorrhoea Diseases 0.000 description 1
- 208000005171 Dysmenorrhea Diseases 0.000 description 1
- 206010013935 Dysmenorrhoea Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010023126 Jaundice Diseases 0.000 description 1
- 206010030113 Oedema Diseases 0.000 description 1
- 206010068319 Oropharyngeal pain Diseases 0.000 description 1
- 201000007100 Pharyngitis Diseases 0.000 description 1
- 241001143928 Psilurus incurvus Species 0.000 description 1
- 241001073567 Verbenaceae Species 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 231100000540 amenorrhea Toxicity 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000002934 diuretic Substances 0.000 description 1
- 230000001882 diuretic effect Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/16—Agglomerates; Granulates; Microbeadlets ; Microspheres; Pellets; Solid products obtained by spray drying, spray freeze drying, spray congealing,(multiple) emulsion solvent evaporation or extraction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/85—Verbenaceae (Verbena family)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation or decoction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Epidemiology (AREA)
- Medicinal Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Alternative & Traditional Medicine (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Medical Informatics (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses freshly squeezed and spray-dried granular decoction pieces with verbena officinalis and a process for preparing the freshly squeezed and spray-dried granular decoction pieces. The process includes harvesting verbena officinalis medicinal materials, then selecting, rinsing and cutting the verbena officinalis medicinal materials to obtain sections, squeezing the sections while the sections are fresh and filtering primarily squeezed medicine juice; adding medicine residues into water, stirring the medicine residues in the water and filtering and squeezing the medicine residues and the water to obtain medicine juice; combining the medicine juice to obtain mixed medicine juice, then concentrating the mixed medicine juice under reduced pressure, carrying out spray-drying on the mixed medicine juice, collecting spray-dried products, smashing the spray-dried products, mixing the spray-dried products with the primarily squeezed medicine juice to obtain mixtures, granulating the mixtures to obtain grains, shaping the grains and then packaging the grains under vacuum conditions. The freshly squeezed and spray-dried granular decoction pieces with the verbena officinalis and the process have the advantages that polar and non-polar effective components in the medicinal materials can be reserved to the greatest extent; the granular decoction pieces are good in flowability, favorable for storage and transportation and convenient to regulate, the quality of the freshly squeezed and spray-dried granular decoction pieces can be controlled, reliable curative effects can be realized, and the freshly squeezed and spray-dried granular decoction pieces and the process have important significance on guaranteeing clinical curative effects of traditional Chinese medicines; the process can have obvious social significance and economic benefits if the process is popularized and implemented.
Description
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Chinese medicine Herba Verbenae decoction pieces.
Background technology
Chinese medicine Herba Verbenae is Verbenaceae Herba VerbenaeVerbena officinalis L. dry aerial parts.This
Product have effect of promoting blood circulation to remove blood stasis, removing toxic substances, diuretic, jaundice eliminating, preventing the attack (or recurrence) of malaria, for abdominal mass accumulation, dysmenorrhea amenorrhea, sore throat, edema, malaria
Deng treatment.
The processing mode of conventional Herba Verbenae decoction pieces is: tap when 6 ~ August, the flowers are in blossom, removes impurity, dries, then storage of packing
Fortune.This type of prepared herbal medicine in small pieces ready for decoction, bulky, Hygienic Index is poor, easily pollutes and goes mouldy, quality it is difficult to ensure that, be unfavorable for formula
Adjust and guarantee its clinical efficacy, even bringing the harm of recessiveness to patient.
At present, granule pieces market also having Herba Verbenae medical material to make after extracting is sold.The preparation of granule pieces
Process, extracts not only time consumption and energy consumption, and because conventional substantial amounts of water does solvent, the nonpolar effective ingredient in medical material is difficult to be carried
Take out.Additionally, due to the Herba Verbenae medical material extracted also is to be dried and through long-time storage, therefore, effective ingredient
Loss is also the biggest.In order to ensure Herba Verbenae medical material clinical effectively, steady quality, a kind of novel Herba Verbenae decoction pieces and
Preparation technology urgently develops.
Summary of the invention
The invention discloses " a kind of Herba Verbenae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof ".This technique is permissible
Retain the polarity in Herba Verbenae medical material and nonpolar effective ingredient to greatest extent, it is to avoid medical material is in the processing of existing decoction pieces and storage
The loss of the effective ingredient caused during fortune and the decline of medical material quanlity, reduce the medical material pollution by mycete etc., to guaranteeing horse
Steady quality and the clinical safety of whip grass decoction pieces effectively have great importance.
To achieve these goals, the technical scheme is that
Gather its herb collection period Herba Verbenae, clean, after washing, take advantage of fresh squeezing, collect and just squeeze medicine juice, retain 0.5% ~ 5%
Just squeezing medicine juice standby, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, and filter press filter pressing extracting juice, remaining medicinal residues are pressed again
Extracting juice, merges remaining just squeezing medicine juice and rear twice squeezing medicine juice, 60 ~ 120 mesh screen, obtains Herba Verbenae medicine juice.To obtain
Herba Verbenae medicine juice under the conditions of 40 ~ 75 DEG C, be evaporated to the concentrated solution that relative density is 1.02 ~ 1.15, and by this concentrated solution
Being spray-dried, intake air temperature is set as 90 ~ 140 DEG C, and air outlet temperature is 80 ~ 110 DEG C, collects desciccate, mistake after pulverizing
60 ~ 100 mesh sieves.By above-mentioned Herba Verbenae spray drying powder, mix with the first squeezing medicine juice retained, prepare soft material, pelletize, 50 ~ 80 DEG C
It is dried 4 ~ 8 hours, granulate, vacuum packaging.On the label of product packaging bags, the name of an article, medicinal part, planting site, drink in printing
Sheet manufacturer, date of manufacture, Contents of Main Components, meridian distribution of property and flavor, function cure mainly, usage and dosage, toxic and side effects and contraindication etc.
Information.The thin layer of the included upper Herba Verbenae of bag differentiates collection of illustrative plates and/or high-efficient liquid phase character collection of illustrative plates, as " identity card " of product.This
Outward, in the packaging bag of product, be printed on Quick Response Code, by scanning can link acquisition the former plant photo of product, medical material photo,
The information such as decoction pieces photo, character and microscopical identification feature.
The invention have benefit that:
The Herba Verbenae medical material of fresh collection, directly squeezes after cleaning washing, filters, concentrating under reduced pressure, is spray-dried, pelletizes, gained
The granule pieces arrived, can retain the effective ingredient in medical material to greatest extent.This decoction pieces volume compares to tradition decoction pieces body
Amass and be greatly reduced, good fluidity, vacuum packaging so that prepared slice quality is more stable, beneficially accumulating and clinical adjustment, have ten
Divide significant social meaning and economic implications.
Detailed description of the invention
Embodiment 1
By the Herba Verbenae medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice, retain 1% weight
First squeezing medicine juice separately use.Gained medicinal residues add the tap water of 3 times amount, stir 20min, filter press squeezing extracting juice.Remaining medicine
Slag squeezes extracting juice with squeezer again.The above-mentioned remaining medicine juice that just squeezes is merged, by 100 eye mesh screen mistakes with follow-up twice squeezing medicine juice
Filter.Filtrate reduced in volume, temperature is set as 65 DEG C.When concentrating gained extractum relative density and being 1.05, it is spray-dried, air inlet
Temperature is 140 DEG C, and air outlet temperature is 100 DEG C, collects spray drying thing, low-temperature grinding, crosses 80 mesh sieves.By this spray drying powder with upper
The first squeezing medicine juice stating retention mixes soft material processed, pelletizes, and 75 DEG C are dried 6 hours, granulate, pack, and 1kg/ bag adds packed antioxidant
And desiccant, Vacuum Package, labeling.
Embodiment 2
By the Herba Verbenae medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice, retain 5% weight
First squeezing medicine juice separately use.Gained medicinal residues add the tap water of 5 times amount, stir 30min, filter press squeezing extracting juice.Remaining medicine
Slag squeezes extracting juice with squeezer again.The above-mentioned remaining medicine juice that just squeezes is merged, by 100 eye mesh screen mistakes with follow-up twice squeezing medicine juice
Filter.Filtrate reduced in volume, temperature is set as 70 DEG C.When concentrating gained extractum relative density and being 1.10, it is spray-dried, air inlet
Temperature is 120 DEG C, and air outlet temperature is 90 DEG C, collects spray drying thing, low-temperature grinding, crosses 80 mesh sieves.By this spray drying powder with upper
The first squeezing medicine juice stating retention mixes soft material processed, pelletizes, and 70 DEG C are dried 8 hours, granulate, pack, and 1kg/ bag adds packed antioxidant
And desiccant, Vacuum Package, labeling.
Above example, is only the technological thought that this invention is described, it is impossible to limit protection scope of the present invention whereby all
It is the technological thought proposed according to the present invention, any change done on the basis of technical scheme, each fall within present invention protection
Within the scope of.
Claims (3)
1. a Herba Verbenae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof, it is characterised in that: adopt collection period Herba Verbenae
Collect its herb, clean, washing, after cutting, to take advantage of fresh squeezing, collect and just squeeze medicine juice, the first squeezing medicine juice of retention 0.5% ~ 5% is standby, medicine
Slag adds the water of 1 ~ 5 times amount, stirs 5 ~ 30min, filter press filter pressing extracting juice, and remaining medicinal residues squeeze extracting juice again, merges remaining
First squeezing medicine juice and rear twice squeezing medicine juice, 60 ~ 120 mesh screen, obtain Herba Verbenae medicine juice.
A kind of Herba Verbenae fresh squeezing spray-dried granules decoction pieces the most according to claim 1 and preparation technology thereof, its feature exists
In: the Herba Verbenae medicine juice obtained is evaporated under the conditions of 40 ~ 75 DEG C the concentrated solution that relative density is 1.02 ~ 1.15, and
Being spray-dried by this concentrated solution, intake air temperature is set as 90 ~ 140 DEG C, and air outlet temperature is 80 ~ 110 DEG C, collects to be dried and produces
Thing, crosses 60 ~ 100 mesh sieves after pulverizing.
A kind of Herba Verbenae fresh squeezing spray-dried granules decoction pieces the most according to claim 1 and preparation technology thereof, its feature exists
In: by the Herba Verbenae spray drying powder in claim 2, mix with the first squeezing medicine juice retained in claim 1, prepare soft material,
Pelletizing, 50 ~ 80 DEG C are dried 4 ~ 8 hours, and granulate is vacuum-packed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610582773.4A CN106038491A (en) | 2016-07-23 | 2016-07-23 | Freshly squeezed and spray-dried granular decoction pieces with verbena officinalis and process for preparing freshly squeezed and spray-dried granular decoction pieces |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610582773.4A CN106038491A (en) | 2016-07-23 | 2016-07-23 | Freshly squeezed and spray-dried granular decoction pieces with verbena officinalis and process for preparing freshly squeezed and spray-dried granular decoction pieces |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106038491A true CN106038491A (en) | 2016-10-26 |
Family
ID=57417286
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610582773.4A Pending CN106038491A (en) | 2016-07-23 | 2016-07-23 | Freshly squeezed and spray-dried granular decoction pieces with verbena officinalis and process for preparing freshly squeezed and spray-dried granular decoction pieces |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106038491A (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107213186A (en) * | 2017-06-20 | 2017-09-29 | 徐漫 | A kind of acalypha copperleaf is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
| CN107233384A (en) * | 2017-06-22 | 2017-10-10 | 徐漫 | A kind of motherwort is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
| CN107320508A (en) * | 2017-08-25 | 2017-11-07 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of Chinese trumpet creeper |
| CN107334833A (en) * | 2017-08-25 | 2017-11-10 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of loguat leaf |
| CN107375364A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of desmodium |
| CN107375381A (en) * | 2017-08-25 | 2017-11-24 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of tussilago |
| CN107397788A (en) * | 2017-08-25 | 2017-11-28 | 徐自升 | A kind of schizonepeta is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
| CN107441223A (en) * | 2017-08-25 | 2017-12-08 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of cordate houttuynia |
| CN107468751A (en) * | 2017-08-25 | 2017-12-15 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of Longtube Ground Ivy Herb |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107213186A (en) * | 2017-06-20 | 2017-09-29 | 徐漫 | A kind of acalypha copperleaf is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
| CN107233384A (en) * | 2017-06-22 | 2017-10-10 | 徐漫 | A kind of motherwort is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
| CN107320508A (en) * | 2017-08-25 | 2017-11-07 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of Chinese trumpet creeper |
| CN107334833A (en) * | 2017-08-25 | 2017-11-10 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of loguat leaf |
| CN107375364A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of desmodium |
| CN107375381A (en) * | 2017-08-25 | 2017-11-24 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of tussilago |
| CN107397788A (en) * | 2017-08-25 | 2017-11-28 | 徐自升 | A kind of schizonepeta is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
| CN107441223A (en) * | 2017-08-25 | 2017-12-08 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of cordate houttuynia |
| CN107468751A (en) * | 2017-08-25 | 2017-12-15 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of Longtube Ground Ivy Herb |
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Application publication date: 20161026 |
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