CN105998167A - Vacuum-dried powdery medicinal slices prepared from freshly squeezed flos sophorae and preparation process thereof - Google Patents
Vacuum-dried powdery medicinal slices prepared from freshly squeezed flos sophorae and preparation process thereof Download PDFInfo
- Publication number
- CN105998167A CN105998167A CN201610582890.0A CN201610582890A CN105998167A CN 105998167 A CN105998167 A CN 105998167A CN 201610582890 A CN201610582890 A CN 201610582890A CN 105998167 A CN105998167 A CN 105998167A
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- flos sophorae
- medicinal
- vacuum
- preparation process
- decoction pieces
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- 241000628997 Flos Species 0.000 title claims abstract description 29
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 239000003814 drug Substances 0.000 claims abstract description 12
- 230000008901 benefit Effects 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims abstract description 5
- 238000005406 washing Methods 0.000 claims abstract description 4
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 18
- 238000001291 vacuum drying Methods 0.000 claims description 8
- 239000000843 powder Substances 0.000 claims description 7
- 238000005516 engineering process Methods 0.000 claims description 6
- 238000009461 vacuum packaging Methods 0.000 claims description 3
- 238000002386 leaching Methods 0.000 claims description 2
- 238000003825 pressing Methods 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 4
- 238000003860 storage Methods 0.000 abstract description 4
- 238000000034 method Methods 0.000 abstract description 3
- 238000004140 cleaning Methods 0.000 abstract description 2
- 239000000463 material Substances 0.000 abstract 3
- 238000001914 filtration Methods 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 2
- 238000001694 spray drying Methods 0.000 abstract 1
- 239000012567 medical material Substances 0.000 description 13
- 239000004615 ingredient Substances 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 241000196324 Embryophyta Species 0.000 description 2
- 239000003963 antioxidant agent Substances 0.000 description 2
- 230000003078 antioxidant effect Effects 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 239000002274 desiccant Substances 0.000 description 2
- 239000003651 drinking water Substances 0.000 description 2
- 235000020188 drinking water Nutrition 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000004806 packaging method and process Methods 0.000 description 2
- 238000010298 pulverizing process Methods 0.000 description 2
- 206010051625 Conjunctival hyperaemia Diseases 0.000 description 1
- 206010054787 Haemorrhoidal haemorrhage Diseases 0.000 description 1
- 208000027109 Headache disease Diseases 0.000 description 1
- 206010027514 Metrorrhagia Diseases 0.000 description 1
- 244000046101 Sophora japonica Species 0.000 description 1
- 235000010586 Sophora japonica Nutrition 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 208000002173 dizziness Diseases 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 208000001848 dysentery Diseases 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 208000001780 epistaxis Diseases 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 208000035861 hematochezia Diseases 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/489—Sophora, e.g. necklacepod or mamani
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation or decoction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization
Landscapes
- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Veterinary Medicine (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Alternative & Traditional Medicine (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Medical Informatics (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses vacuum-dried powdery medicinal slices prepared from freshly squeezed flos sophorae and a preparation process thereof. The process comprises the steps that after a flos sophorae medicinal material is harvested, cleaning, selection and drip washing are performed, the flos sophorae medicinal material is squeezed in a fresh state, and medicinal liquid is obtained through filtration; water is added to medicinal residues, and stirring, filtration and squeezing are performed; the obtained medicinal liquid is mixed and subjected to reduced-pressure concentration and spray drying, and vacuum package is performed after smashing. The flos sophorae powdery medicinal slices prepared by means of the preparation process retains the polar and nonpolar effective components in the medicinal material to the most degree. The medicinal slices is convenient for storage, transportation and dispensing, is controllable in quality and reliable in curative effect and has the important significance on guarantee of the clinical curative effect of traditional Chinese medicine. The preparation process has remarkable social significance and economic benefits in implementation and popularization.
Description
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Chinese medicine Flos Sophorae decoction pieces.
Background technology
Chinese medicine Flos Sophorae is leguminous plant Chinese scholartreeSophora japonicaL. dry flower and alabastrum.This product only has removing heat from blood
Blood, effect of purging liver-fire, it is used for having blood in stool, hemorrhoidal bleeding, dysentery, metrorrhagia, spit blood, epistaxis, liver-heat conjunctival congestion, controlling of the headache disease such as dizziness
Treat.
The processing mode of conventional Flos Sophorae decoction pieces is: summer, the flowers are in blossom to put or gathers time alabastrum is formed, and is dried, then storage of packing
Fortune.This type of decoction pieces, bulky, Hygienic Index is poor, easily pollutes and goes mouldy, quality it is difficult to ensure that, be unfavorable for that formula is adjusted
With guarantee its clinical efficacy, even to patient bring recessiveness harm.
At present, granule pieces market also having Flos Sophorae medical material to make after extracting is sold.The preparation of granule pieces
Journey, extracts not only time consumption and energy consumption, and because conventional substantial amounts of water does solvent, the nonpolar effective ingredient in medical material is difficult to be extracted
Out.Additionally, due to the Flos Sophorae medical material extracted also is to be dried and through long-time storage, therefore, the loss of effective ingredient
Also it is the biggest.In order to ensure clinical effective, the steady quality of Flos Sophorae medical material, a kind of novel Flos Sophorae decoction pieces and preparation technology thereof
Urgently develop.
Summary of the invention
The invention discloses " a kind of Flos Sophorae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof ".This technique can be
The polarity in Flos Sophorae medical material and nonpolar effective ingredient is retained, it is to avoid medical material is in the processing of existing decoction pieces and storage while limits
The loss of the effective ingredient caused during fortune and the decline of medical material quanlity, reduce the medical material pollution by mycete etc., to guaranteeing Chinese scholartree
Steady quality and the clinical safety of flower decoction pieces effectively have great importance.
To achieve these goals, the technical scheme is that
After Flos Sophorae is gathered, clean, washing, take advantage of fresh squeezing.In medicinal residues after squeezing, add 1 ~ 5 times amount water, stirring 5 ~
30min, with filter press filter pressing extracting juice.Remaining medicinal residues squeeze extracting juice again.Merge three medicine juice, with 40 ~ 120 mesh screen,
Obtain Flos Sophorae medicine juice.The Flos Sophorae medicine juice obtained is evaporated to the leaching that relative density is 1.05 ~ 1.30 under the conditions of 40 ~ 75 DEG C
Cream, and by its in 40 ~ 70 DEG C vacuum drying 4 ~ 8 hours after pulverized 60 ~ 120 mesh sieves, vacuum packaging, obtain Flos Sophorae fresh squeezing vacuum
Dried powder decoction pieces.
On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, decoction pieces manufacturer, the date of manufacture,
The information such as Contents of Main Components, meridian distribution of property and flavor, function cure mainly, usage and dosage, toxic and side effects and contraindication.Flos Sophorae is enclosed in Dai
Thin layer differentiates collection of illustrative plates and/or high-efficient liquid phase character collection of illustrative plates, as " identity card " of product.Additionally, in the packaging bag of product, print
There is Quick Response Code, former plant photo, medical material photo, decoction pieces photo, character and the micro-mirror obtaining product can be linked by scanning
The information such as other feature.
The invention have benefit that:
The Flos Sophorae medical material of fresh collection, directly squeeze after cleaning washing, filter, concentrating under reduced pressure, vacuum drying, obtained powder
Decoction pieces, can retain the effective ingredient in medical material to greatest extent.This decoction pieces volume compares to tradition decoction pieces volume greatly
Reducing, vacuum packaging so that prepared slice quality is more stable, beneficially accumulating and clinical adjustment, have the most significant social meaning
And economic implications.
Detailed description of the invention
Embodiment 1
By the Flos Sophorae medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add 3 times
The drinking water of amount, stirs 20min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.By above-mentioned 3
Secondary medicine juice merges, and filters with 100 eye mesh screens.Filtrate reduced in volume, temperature is set as 65 DEG C.Concentrating gained extractum relative density
When being 1.15, transfer in vacuum drying oven, be dried 8 hours in 60 DEG C, cross 60 mesh sieves, pack, 1kg/ bag after pulverizing, add bag
Dress antioxidant and desiccant, Vacuum Package.
Embodiment 2
By the Flos Sophorae medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add 5 times
The drinking water of amount, stirs 30min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.By above-mentioned 3
Secondary medicine juice merges, and filters with 80 eye mesh screens.Filtrate reduced in volume, temperature is set as 70 DEG C.Concentrating gained extractum relative density
When being 1.10, transfer in vacuum drying oven, be dried 6 hours in 65 DEG C, cross 60 mesh sieves, pack, 1kg/ bag after pulverizing, add bag
Dress antioxidant and desiccant, Vacuum Package.
Above example, is only the technological thought that this invention is described, it is impossible to limit protection scope of the present invention whereby all
It is the technological thought proposed according to the present invention, any change done on the basis of technical scheme, each fall within present invention protection
Within the scope of.
Claims (2)
1. fresh squeezing of Flos Sophorae is vacuum dried powder decoction pieces and preparation technology thereof, it is characterised in that: after Flos Sophorae is gathered, clean,
Washing, takes advantage of fresh squeezing, and medicinal residues add the water of 1 ~ 5 times amount, stirs 5 ~ 30min, and filter press filter pressing extracting juice, remaining medicinal residues are pressed again
Extracting juice, merges three medicine juice, 40 ~ 120 mesh screen, obtains Flos Sophorae medicine juice.
A kind of Flos Sophorae the most according to claim 1 is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof, it is characterised in that:
The Flos Sophorae medicine juice obtained in claim 1 is evaporated to the leaching that relative density is 1.05 ~ 1.30 under the conditions of 40 ~ 75 DEG C
Cream, and by its in 40 ~ 70 DEG C vacuum drying 4 ~ 8 hours after pulverized 60 ~ 120 mesh sieves, vacuum packaging, obtain Flos Sophorae fresh squeezing vacuum
Dried powder decoction pieces.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610582890.0A CN105998167A (en) | 2016-07-23 | 2016-07-23 | Vacuum-dried powdery medicinal slices prepared from freshly squeezed flos sophorae and preparation process thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610582890.0A CN105998167A (en) | 2016-07-23 | 2016-07-23 | Vacuum-dried powdery medicinal slices prepared from freshly squeezed flos sophorae and preparation process thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105998167A true CN105998167A (en) | 2016-10-12 |
Family
ID=57117340
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610582890.0A Pending CN105998167A (en) | 2016-07-23 | 2016-07-23 | Vacuum-dried powdery medicinal slices prepared from freshly squeezed flos sophorae and preparation process thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105998167A (en) |
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107095902A (en) * | 2017-06-22 | 2017-08-29 | 徐漫 | A kind of motherwort is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107233367A (en) * | 2017-06-19 | 2017-10-10 | 徐漫 | A kind of Ilex Latifolia Thunb is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107362187A (en) * | 2017-08-25 | 2017-11-21 | 徐漫 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Artemisia anomala |
| CN107362182A (en) * | 2017-08-25 | 2017-11-21 | 徐漫 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of phoenix-tail fern |
| CN107362197A (en) * | 2017-08-25 | 2017-11-21 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Herba Lycopi |
| CN107362188A (en) * | 2017-08-25 | 2017-11-21 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of folium isatidis |
| CN107375424A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of schizonepeta is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107375348A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of scouring rush |
| CN107375542A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of field pennycress |
| CN107412433A (en) * | 2017-08-25 | 2017-12-01 | 徐漫 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of black nightshade |
| CN107485641A (en) * | 2017-08-25 | 2017-12-19 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of elscholtiza |
| CN107582624A (en) * | 2017-08-25 | 2018-01-16 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Pogostemon cablin |
| CN107714753A (en) * | 2017-08-25 | 2018-02-23 | 徐漫 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of gynostemma pentaphylla |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105287861A (en) * | 2015-11-22 | 2016-02-03 | 徐漫 | Freshly-squeezed paulownia flower vacuum-dried powdery decoction piece and preparation technology thereof |
-
2016
- 2016-07-23 CN CN201610582890.0A patent/CN105998167A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105287861A (en) * | 2015-11-22 | 2016-02-03 | 徐漫 | Freshly-squeezed paulownia flower vacuum-dried powdery decoction piece and preparation technology thereof |
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107233367A (en) * | 2017-06-19 | 2017-10-10 | 徐漫 | A kind of Ilex Latifolia Thunb is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107095902A (en) * | 2017-06-22 | 2017-08-29 | 徐漫 | A kind of motherwort is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107375424A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of schizonepeta is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107362182A (en) * | 2017-08-25 | 2017-11-21 | 徐漫 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of phoenix-tail fern |
| CN107362197A (en) * | 2017-08-25 | 2017-11-21 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Herba Lycopi |
| CN107362188A (en) * | 2017-08-25 | 2017-11-21 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of folium isatidis |
| CN107362187A (en) * | 2017-08-25 | 2017-11-21 | 徐漫 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Artemisia anomala |
| CN107375348A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of scouring rush |
| CN107375542A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of field pennycress |
| CN107412433A (en) * | 2017-08-25 | 2017-12-01 | 徐漫 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of black nightshade |
| CN107485641A (en) * | 2017-08-25 | 2017-12-19 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of elscholtiza |
| CN107582624A (en) * | 2017-08-25 | 2018-01-16 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Pogostemon cablin |
| CN107714753A (en) * | 2017-08-25 | 2018-02-23 | 徐漫 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of gynostemma pentaphylla |
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Application publication date: 20161012 |