CN105232607A - Cactus freshly-squeezed spray dried granule decoction piece and preparation process thereof - Google Patents
Cactus freshly-squeezed spray dried granule decoction piece and preparation process thereof Download PDFInfo
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- CN105232607A CN105232607A CN201510774371.XA CN201510774371A CN105232607A CN 105232607 A CN105232607 A CN 105232607A CN 201510774371 A CN201510774371 A CN 201510774371A CN 105232607 A CN105232607 A CN 105232607A
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- squeezing
- radix
- medicine juice
- caulis opuntiae
- opuntiae dillenii
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Abstract
The invention discloses a cactus freshly-squeezed spray dried granule decoction piece and a preparation process thereof. The process includes the steps of firstly, harvesting, selecting and drip washing cactus medicine materials, squeezing the materials freshly, and filtering medicine juice; secondly, adding water to decoction dregs to be stirred, and conducting filtering and squeezing; thirdly, combining obtained medicine juice, conducting decompression concentration and spray drying, collecting spray-dried products, conducting smashing, medicine juice primary squeezing and mixing to prepare granules, and conducting vacuum packaging after granulation. The cactus granule decoction piece prepared through the method keeps the polar and non-polar effective ingredients in the medicine materials to the maximum extent. The granule decoction piece is high in mobility, beneficial to storage and transportation, convenient to adjust, controllable in quality and reliable in curative effect and has important significance in ensuring the traditional Chinese medicine clinical curative effect; the method is implemented and popularized and has remarkable social significance and economic benefits.
Description
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Chinese medicine Radix et Caulis Opuntiae Dillenii decoction pieces.
Background technology
Chinese medicine Radix et Caulis Opuntiae Dillenii is Cactaeous plants Radix et Caulis Opuntiae Dillenii
opuntiastricta(Haw.) Haw.var.
dillenii(Ker-Gawl.) the dry meat stem of Benson.This product has promoting flow of QI and blood, effect of heat-clearing and toxic substances removing.Be mainly used in dysentery, cough, acute mastitis, the treatment of scald etc.
The processing mode of common Radix et Caulis Opuntiae Dillenii decoction pieces is: after medical material is gathered, and removing impurity, is cut into block, dries, then accumulating of packing.This type of prepared herbal medicine in small pieces ready for decoction, bulky, Hygienic Index is poor, is easy to pollute and go mouldy, and quality is difficult to ensure, is unfavorable for that formula is adjusted and guarantees its clinical efficacy, even brings recessive harm to patient.In addition, because Radix et Caulis Opuntiae Dillenii is fleshy stem, be difficult to dry; And the Radix et Caulis Opuntiae Dillenii dried has much small thorn, can fly upward with the wind in atmosphere, be easy to be inhaled into, or prick skin and difficulty is found, bring to production and processing personnel and bother.Therefore, in order to ensure the safety of operator, also in order to clinical effective, the steady quality of Radix et Caulis Opuntiae Dillenii medical material, a kind of novel Radix et Caulis Opuntiae Dillenii decoction pieces and preparation technology thereof urgently develop.
Summary of the invention
The present invention discloses " a kind of Radix et Caulis Opuntiae Dillenii fresh squeezing spray-dried granules decoction pieces and preparation technology thereof ".This technique can retain polarity in Radix et Caulis Opuntiae Dillenii medical material and nonpolar effective ingredient to greatest extent, the loss of effective ingredient avoiding medical material to cause in existing decoction pieces processing and storage and transport process and the decline of medical material quanlity, reduce the pollution of medical material by mycete etc., the steady quality and clinical safety guaranteeing Radix et Caulis Opuntiae Dillenii decoction pieces is effectively had great importance.
To achieve these goals, technical scheme of the present invention is:
Gather its herb collection period at Radix et Caulis Opuntiae Dillenii, clean, after washing, take advantage of fresh squeezing, collect and just squeeze medicine juice, the first squeezing medicine juice of retention 0.5% ~ 5% is for subsequent use, and medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, filter press filter pressing extracting juice, remaining medicinal residues squeeze extracting juice again, merge remaining first squeezing medicine juice and rear twice squeezing medicine juice, 60 ~ 120 mesh screen, obtain Radix et Caulis Opuntiae Dillenii medicine juice.The Radix et Caulis Opuntiae Dillenii medicine juice obtained is evaporated to the concentrated solution that relative density is 1.02 ~ 1.15 under 40 ~ 75 DEG C of conditions, and by this concentrated solution spraying dry, intake air temperature is set as 90 ~ 140 DEG C, air outlet temperature is 80 ~ 110 DEG C, collect desciccate, after pulverizing, cross 60 ~ 100 mesh sieves.By above-mentioned Radix et Caulis Opuntiae Dillenii spray drying powder, mix with the first squeezing medicine juice retained, prepare soft material, granulation, 50 ~ 80 DEG C of dryings 4 ~ 8 hours, granulate, vacuum packaging.On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, decoction pieces manufacturer, date of manufacture, Contents of Main Components, meridian distribution of property and flavor, function cure mainly, the information such as usage and dosage, toxic and side effects and contraindication.TLC distinguish collection of illustrative plates and/or the high-efficient liquid phase character collection of illustrative plates of Radix et Caulis Opuntiae Dillenii is enclosed, as " identity card " of product in bag.In addition, in the packaging bag of product, be printed on Quick Response Code, the information such as former plant photo, medical material photo, decoction pieces photo, character and the microscopical identification feature obtaining product can be linked by scanning.
Usefulness of the present invention is:
The Radix et Caulis Opuntiae Dillenii medical material of fresh collection, direct squeezing, filtration, concentrating under reduced pressure, spraying dry, granulation after cleaning washing, the granule pieces obtained, can retain the effective ingredient in medical material to greatest extent.This decoction pieces volume compares to traditional decoction pieces volume and reduces widely, good fluidity, and vacuum packaging, makes prepared slice quality more stable, is beneficial to accumulating and clinical adjustment, has very significant social meaning and economic implications.
Detailed description of the invention
Embodiment 1
By the Radix et Caulis Opuntiae Dillenii medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice, the first squeezing medicine juice retaining 1% weight is separately used.Gained medicinal residues add the tap water of 3 times amount, stir 20min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.Above-mentioned remaining just squeezing medicine juice and the follow-up medicine juice that squeezes for twice are merged, filters with 100 eye mesh screens.Filtrate reduced in volume, temperature is set as 65 DEG C.When concentrated gained extractum relative density is 1.05, spraying dry, intake air temperature is 140 DEG C, and air outlet temperature is 100 DEG C, collects spray dry, pulverize at low temperature, crosses 80 mesh sieves.This spray drying powder is mixed soft material processed with the first squeezing medicine juice of above-mentioned retention, granulates, 75 DEG C of dryings 6 hours, granulate, pack, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, labeling.
Embodiment 2
By the Radix et Caulis Opuntiae Dillenii medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice, the first squeezing medicine juice retaining 5% weight is separately used.Gained medicinal residues add the tap water of 5 times amount, stir 30min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.Above-mentioned remaining just squeezing medicine juice and the follow-up medicine juice that squeezes for twice are merged, filters with 100 eye mesh screens.Filtrate reduced in volume, temperature is set as 70 DEG C.When concentrated gained extractum relative density is 1.10, spraying dry, intake air temperature is 120 DEG C, and air outlet temperature is 90 DEG C, collects spray dry, pulverize at low temperature, crosses 80 mesh sieves.This spray drying powder is mixed soft material processed with the first squeezing medicine juice of above-mentioned retention, granulates, 70 DEG C of dryings 8 hours, granulate, pack, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, labeling.
Above embodiment, is only the technological thought that this invention is described, can not limit the every technological thought proposed according to the present invention of protection scope of the present invention whereby, any change that technical scheme basis is done, all falls within the scope of protection of the invention.
Claims (3)
1. Radix et Caulis Opuntiae Dillenii fresh squeezing spray-dried granules decoction pieces and a preparation technology thereof, is characterized in that: gather its herb collection period at Radix et Caulis Opuntiae Dillenii, clean, after washing, take advantage of fresh squeezing, collect and just squeeze medicine juice, the first squeezing medicine juice of retention 0.5% ~ 5% is for subsequent use, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, filter press filter pressing extracting juice, remaining medicinal residues squeeze extracting juice again, merge remaining first squeezing medicine juice and rear twice squeezing medicine juice, 60 ~ 120 mesh screen, obtain Radix et Caulis Opuntiae Dillenii medicine juice.
2. a kind of Radix et Caulis Opuntiae Dillenii fresh squeezing spray-dried granules decoction pieces according to claim 1 and preparation technology thereof, it is characterized in that: the Radix et Caulis Opuntiae Dillenii medicine juice obtained in claim 1 is evaporated to the concentrated solution that relative density is 1.02 ~ 1.15 under 40 ~ 75 DEG C of conditions, and by this concentrated solution spraying dry, intake air temperature is set as 90 ~ 140 DEG C, air outlet temperature is 80 ~ 110 DEG C, collect desciccate, after pulverizing, cross 60 ~ 100 mesh sieves.
3. a kind of Radix et Caulis Opuntiae Dillenii fresh squeezing spray-dried granules decoction pieces according to claim 1 and preparation technology thereof, it is characterized in that: by the Radix et Caulis Opuntiae Dillenii spray drying powder in claim 2, mix with the first squeezing medicine juice retained in claim 1, prepare soft material, granulate, 50 ~ 80 DEG C of dryings 4 ~ 8 hours, granulate, vacuum packaging.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201510774371.XA CN105232607A (en) | 2015-11-14 | 2015-11-14 | Cactus freshly-squeezed spray dried granule decoction piece and preparation process thereof |
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| CN201510774371.XA CN105232607A (en) | 2015-11-14 | 2015-11-14 | Cactus freshly-squeezed spray dried granule decoction piece and preparation process thereof |
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| CN105232607A true CN105232607A (en) | 2016-01-13 |
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| CN201510774371.XA Pending CN105232607A (en) | 2015-11-14 | 2015-11-14 | Cactus freshly-squeezed spray dried granule decoction piece and preparation process thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106109622A (en) * | 2016-07-23 | 2016-11-16 | 徐漫 | A kind of Herba Agrimoniae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN106109575A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Scutellariae Barbatae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN106109530A (en) * | 2016-07-23 | 2016-11-16 | 徐漫 | A kind of Folium Isatidis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN106214723A (en) * | 2016-07-23 | 2016-12-14 | 徐漫 | A kind of Herba Lobeliae Chinensis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN107213186A (en) * | 2017-06-20 | 2017-09-29 | 徐漫 | A kind of acalypha copperleaf is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
| CN107233384A (en) * | 2017-06-22 | 2017-10-10 | 徐漫 | A kind of motherwort is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
Citations (4)
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| CN1364468A (en) * | 2001-01-19 | 2002-08-21 | 赵国林 | Wall breaking and extracting method for Chinese herbal medicine and formulation |
| CN1507805A (en) * | 2002-12-18 | 2004-06-30 | 烟台市泰丰种植养殖科技有限公司 | Cactus juice and preparing method thereof |
| CN102119992A (en) * | 2011-03-07 | 2011-07-13 | 贵州百灵企业集团制药股份有限公司 | Pharmaceutical preparation prepared from fresh motherwort and fresh aloe and preparation method thereof |
| CN102406175A (en) * | 2011-12-06 | 2012-04-11 | 张天久 | Preparation method of fresh sow thistle juice |
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2015
- 2015-11-14 CN CN201510774371.XA patent/CN105232607A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1364468A (en) * | 2001-01-19 | 2002-08-21 | 赵国林 | Wall breaking and extracting method for Chinese herbal medicine and formulation |
| CN1507805A (en) * | 2002-12-18 | 2004-06-30 | 烟台市泰丰种植养殖科技有限公司 | Cactus juice and preparing method thereof |
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| CN102406175A (en) * | 2011-12-06 | 2012-04-11 | 张天久 | Preparation method of fresh sow thistle juice |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106109622A (en) * | 2016-07-23 | 2016-11-16 | 徐漫 | A kind of Herba Agrimoniae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN106109530A (en) * | 2016-07-23 | 2016-11-16 | 徐漫 | A kind of Folium Isatidis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN106214723A (en) * | 2016-07-23 | 2016-12-14 | 徐漫 | A kind of Herba Lobeliae Chinensis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN106109575A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Scutellariae Barbatae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof |
| CN107213186A (en) * | 2017-06-20 | 2017-09-29 | 徐漫 | A kind of acalypha copperleaf is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
| CN107233384A (en) * | 2017-06-22 | 2017-10-10 | 徐漫 | A kind of motherwort is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology |
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Application publication date: 20160113 |