CN105213661A - A kind of Aloe fresh squeezing lyophilization powder decoction pieces and preparation technology thereof - Google Patents
A kind of Aloe fresh squeezing lyophilization powder decoction pieces and preparation technology thereof Download PDFInfo
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- CN105213661A CN105213661A CN201510774369.2A CN201510774369A CN105213661A CN 105213661 A CN105213661 A CN 105213661A CN 201510774369 A CN201510774369 A CN 201510774369A CN 105213661 A CN105213661 A CN 105213661A
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- aloe
- decoction pieces
- fresh squeezing
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Abstract
The present invention discloses a kind of Aloe fresh squeezing lyophilization powder decoction pieces and preparation technology thereof.This technique after Aloe medical material is gathered, clean, drip washing, cutting, and take advantage of fresh squeezing, leaching medicine juice.Medicinal residues add water stirring again, filter squeezing.Concentrating under reduced pressure after gained medicine juice merges, lyophilization, collects lyophilized products, after crushed vacuum packaging.The Alose decoction pieces that this legal system is standby, remains the polarity in medical material and nonpolar effective ingredient to greatest extent simultaneously.Decoction pieces is beneficial to accumulating, convenient adjustment, and quality controllable, curative effect is reliable, has great importance to guarantee tcm clinical curative effect.The promotion and implementation of this law, will have significant social meaning and economic benefit.
Description
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Chinese medicine Aloe decoction pieces.
Background technology
Chinese medicine Aloe is liliaceous plant Aloe vulgaris
aloebarbadensisthe dry product of concentrated juice of Miller leaf.This product has relieving constipation by purgation, purging liver-fire, and parasite killing treats effect of infantile malnutrition, and for pyrolysis constipation, infantile convulsion is twitched, young waiter in a wineshop or an inn's infantile malnutrition, external treatment tinea skin ulcer etc.
The processing mode of conventional Aloe decoction pieces is: after being gathered by its leaf, remove crust, get its juice, decocting and concentrating forms.This method is long for heat time heating time, and comparatively large to the destruction of effective ingredient, finished product presents brownish black bulk.In addition, also containing a large amount of effective ingredient in the leaf skin abandoned.In order to ensure clinical effective, the steady quality of Aloe medical material, a kind of novel Aloe decoction pieces and preparation technology thereof urgently develop.
Summary of the invention
The present invention discloses " a kind of Aloe fresh squeezing lyophilization powder decoction pieces and preparation technology thereof ".This technique can retain polarity in Aloe medical material and nonpolar effective ingredient to greatest extent, the loss of effective ingredient avoiding medical material to cause in existing decoction pieces processing and storage and transport process and the decline of medical material quanlity, reduce the pollution of medical material by mycete etc., the steady quality and clinical safety guaranteeing Aloe decoction pieces is effectively had great importance.
To achieve these goals, technical scheme of the present invention is:
Gather its meat blade collection period Aloe, clean, washing, after cutting, take advantage of fresh squeezing, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, filter press filter pressing extracting juice, remaining medicinal residues squeeze extracting juice again, and merge three medicine juice, 40 ~ 120 mesh screen, obtain Aloe medicine juice.The Aloe medicine juice obtained is evaporated to the extractum that relative density is 1.05 ~ 1.25 under 40 ~ 75 DEG C of conditions, and this extractum is freezed 6 ~ 24 hours in-20 ~-80 DEG C of refrigerators, lyophilization again, pressure is 0.06 ~ 0.09MPa, and temperature is-15 ~-40 DEG C, and cooling time is 12 ~ 48 hours, after collecting lyophilized products, through pulverizing, sieving, packing.
On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, decoction pieces manufacturer, date of manufacture, Contents of Main Components, meridian distribution of property and flavor, function cure mainly, the information such as usage and dosage, toxic and side effects and contraindication.TLC distinguish collection of illustrative plates and/or the high-efficient liquid phase character collection of illustrative plates of Aloe is enclosed, as " identity card " of product in bag.In addition, in the packaging bag of product, be printed on Quick Response Code, the information such as former plant photo, medical material photo, decoction pieces photo, character and the microscopical identification feature obtaining product can be linked by scanning.
Usefulness of the present invention is:
The Aloe medical material of fresh collection, direct squeezing, filtration, concentrating under reduced pressure, lyophilization after cleaning washing, the powder decoction pieces obtained, can retain the effective ingredient in medical material to greatest extent.This decoction pieces volume compares to traditional decoction pieces volume and reduces widely, and vacuum packaging, makes prepared slice quality more stable, is beneficial to accumulating and clinical adjustment, has very significant social meaning and economic implications.
Detailed description of the invention
Embodiment 1
By the Aloe medical material of fresh collection, clean, with water wash, be cut into the section of 3cm, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add the tap water of 3 times amount, stir 20min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.Above-mentioned 3 medicine juice are merged, filters with 100 eye mesh screens.Filtrate reduced in volume, temperature is set as 65 DEG C.When concentrated gained extractum relative density is 1.15, extractum is freezed 6 hours in-80 DEG C of refrigerators.Take out east knot thing, lyophilization, pressure is 0.09Mpa, and temperature is-20 DEG C, dry 24 hours.Take out lyophilized products, pulverize at low temperature, cross 80 mesh sieves, moisture is not higher than 12%, and pack, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, labeling.
Embodiment 2
By the Aloe medical material of fresh collection, clean, with water wash, be cut into the section of 5cm, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add the tap water of 5 times amount, stir 30min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.Above-mentioned 3 medicine juice are merged, filters with 80 eye mesh screens.Filtrate reduced in volume, temperature is set as 70 DEG C.When concentrated gained extractum relative density is 1.10, extractum is freezed 8 hours in-80 DEG C of refrigerators.Take out east knot thing, lyophilization, pressure is 0.08Mpa, and temperature is-40 DEG C, dry 48 hours.Take out lyophilized products, pulverize at low temperature, cross 60 mesh sieves, moisture is not higher than 12%, and pack, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, labeling.
Above embodiment, is only the technological thought that this invention is described, can not limit the every technological thought proposed according to the present invention of protection scope of the present invention whereby, any change that technical scheme basis is done, all falls within the scope of protection of the invention.
Claims (2)
1. Aloe fresh squeezing lyophilization powder decoction pieces and a preparation technology thereof, is characterized in that: gather its blade collection period Aloe, clean, washing, after cutting, take advantage of fresh squeezing, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, filter press filter pressing extracting juice, remaining medicinal residues squeeze extracting juice again, merge three medicine juice, 40 ~ 120 mesh screen, obtain Aloe medicine juice.
2. a kind of Aloe according to claim 1 fresh squeezing lyophilization powder decoction pieces and preparation technology thereof, it is characterized in that: the Aloe medicine juice obtained in claim 1 is evaporated to the extractum that relative density is 1.05 ~ 1.25 under 40 ~ 75 DEG C of conditions, and this extractum is freezed 6 ~ 24 hours in-20 ~-80 DEG C of refrigerators, then lyophilization, pressure is 0.06 ~ 0.09MPa, temperature is-15 ~-40 DEG C, cooling time is 12 ~ 48 hours, after collecting lyophilized products, through pulverizing, sieve, pack.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510774369.2A CN105213661A (en) | 2015-11-14 | 2015-11-14 | A kind of Aloe fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510774369.2A CN105213661A (en) | 2015-11-14 | 2015-11-14 | A kind of Aloe fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
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| CN105213661A true CN105213661A (en) | 2016-01-06 |
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| CN201510774369.2A Pending CN105213661A (en) | 2015-11-14 | 2015-11-14 | A kind of Aloe fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105998132A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Chinese lobelia freshly-squeezed freeze drying powder decoction tablets and preparation process thereof |
| CN105998130A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Folium Isatidis freshly-pressed lyophilized powdery decoction pieces and preparation process thereof |
| CN105998395A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Herba Verbenae freshly squeezed freeze drying powder decoction piece and preparation technology thereof |
| CN106109545A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Euphorbiae Humifusae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
| CN106214741A (en) * | 2016-07-24 | 2016-12-14 | 徐漫 | A kind of Herba Scutellariae Barbatae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
| CN107213187A (en) * | 2017-06-20 | 2017-09-29 | 徐漫 | A kind of acalypha copperleaf is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107233385A (en) * | 2017-06-22 | 2017-10-10 | 徐漫 | A kind of motherwort is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107320582A (en) * | 2017-08-25 | 2017-11-07 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of Chinese violet |
| CN107441202A (en) * | 2017-08-25 | 2017-12-08 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of loguat leaf |
| CN107441201A (en) * | 2017-08-25 | 2017-12-08 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of loguat leaf |
| CN107485628A (en) * | 2017-08-25 | 2017-12-19 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of geranium wilfordii |
| CN107485660A (en) * | 2017-08-25 | 2017-12-19 | 芜湖天成普阳中药科技有限公司 | A kind of tangerine leaf is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107485646A (en) * | 2017-08-25 | 2017-12-19 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of mulberry leaf |
-
2015
- 2015-11-14 CN CN201510774369.2A patent/CN105213661A/en active Pending
Non-Patent Citations (2)
| Title |
|---|
| 孟胜男等: "《药剂学》", 30 September 2011 * |
| 黄达芳等: "《实用中药鉴定学》", 31 August 2004 * |
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105998132A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Chinese lobelia freshly-squeezed freeze drying powder decoction tablets and preparation process thereof |
| CN105998130A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Folium Isatidis freshly-pressed lyophilized powdery decoction pieces and preparation process thereof |
| CN105998395A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Herba Verbenae freshly squeezed freeze drying powder decoction piece and preparation technology thereof |
| CN106109545A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Euphorbiae Humifusae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
| CN106214741A (en) * | 2016-07-24 | 2016-12-14 | 徐漫 | A kind of Herba Scutellariae Barbatae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
| CN107213187A (en) * | 2017-06-20 | 2017-09-29 | 徐漫 | A kind of acalypha copperleaf is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107233385A (en) * | 2017-06-22 | 2017-10-10 | 徐漫 | A kind of motherwort is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107320582A (en) * | 2017-08-25 | 2017-11-07 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of Chinese violet |
| CN107441202A (en) * | 2017-08-25 | 2017-12-08 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of loguat leaf |
| CN107441201A (en) * | 2017-08-25 | 2017-12-08 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of loguat leaf |
| CN107485628A (en) * | 2017-08-25 | 2017-12-19 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of geranium wilfordii |
| CN107485660A (en) * | 2017-08-25 | 2017-12-19 | 芜湖天成普阳中药科技有限公司 | A kind of tangerine leaf is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107485646A (en) * | 2017-08-25 | 2017-12-19 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of mulberry leaf |
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