CN107050082A - A kind of field thistle is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology - Google Patents

A kind of field thistle is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology Download PDF

Info

Publication number
CN107050082A
CN107050082A CN201710466209.0A CN201710466209A CN107050082A CN 107050082 A CN107050082 A CN 107050082A CN 201710466209 A CN201710466209 A CN 201710466209A CN 107050082 A CN107050082 A CN 107050082A
Authority
CN
China
Prior art keywords
field thistle
fresh
vacuum drying
preparation technology
squeeze
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710466209.0A
Other languages
Chinese (zh)
Inventor
徐漫
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201710466209.0A priority Critical patent/CN107050082A/en
Publication of CN107050082A publication Critical patent/CN107050082A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00Medicinal preparations characterised by special physical form
    • A61K9/14Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/31Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/50Methods involving additional extraction steps
    • A61K2236/51Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying

Landscapes

  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
  • Medicinal Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Epidemiology (AREA)
  • Chemical & Material Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Veterinary Medicine (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Medical Informatics (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

Powder decoction pieces and its preparation technology are dried in vacuo the invention discloses a kind of fresh squeeze of field thistle.The technique is cleaned, eluted, and take advantage of fresh squeezing, leaching concoction after the harvesting of field thistle medicinal material.The dregs of a decoction add water stirring, filtering squeezing.Gained concoction is concentrated under reduced pressure after merging, and is dried in vacuo, and dried object is vacuum-packed after crushing.Field Thistle Herb medicine materical crude slice prepared by this method, remains the polarity and nonpolar active ingredient in medicinal material to greatest extent.Medicine materical crude slice is beneficial to accumulating, convenient to adjust, quality controllable, and curative effect is reliable, to ensureing that tcm clinical curative effect has great importance.The promotion and implementation of this law, will there is significant social effect and economic benefit.

Description

A kind of field thistle is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology
Technical field
The invention belongs to the processing technology of Chinese medicine manufacture field, more particularly to Chinese medicine field thistle medicine materical crude slice.
Background technology
Chinese medicine field thistle is feverfew field thistleCephalanoplos segetum(Bunge) Kitam. dry ground Upper part.This product sweet, bitter, cold, the thoughts of returning home, Liver Channel.This product has cooling blood and hemostasis, the effect of eliminating stasis to resolve swelling, is mainly used in bleeding from five sense organs or subcutaneous tissue, urine Blood, have blood in stool, the treatment of metrostaxis etc..
The processing mode of conventional field thistle medicine materical crude slice is:After harvesting, impurity is removed, is dried, then accumulating of packing.Such herbal medicine drink Piece, bulky, Hygienic Index is poor, easily pollutes and goes mouldy, quality it is difficult to ensure that, be unfavorable for formula adjust and ensure that it faces Bed curative effect, or even to patient bring recessiveness harm.
At present, in the market also has the granule pieces sale that field thistle medicinal material is made after extraction.The preparation of granule pieces Journey, extracts not only time consumption and energy consumption, and is difficult to be extracted because commonly using substantial amounts of water to do the nonpolar active ingredient in solvent, medicinal material Out.Further, since the field thistle medicinal material of extraction is also to dry and by storage for a long time, therefore, the loss of active ingredient It is also very big.In order to ensure the clinic of field thistle medicinal material is effective, steady quality, a kind of new field thistle medicine materical crude slice and its preparation technology Urgently develop.
The content of the invention
The invention discloses " a kind of field thistle is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology ".This technique can be most Retain to limits the polarity and nonpolar active ingredient in field thistle medicinal material simultaneously, it is to avoid medicinal material is processed and stored up in existing medicine materical crude slice The loss of active ingredient and the decline of medical material quanlity caused by during fortune, reduce pollution of the medicinal material by mould etc., small to ensuring The steady quality and clinical safety of Ji medicine materical crude slice effectively have great importance.
To achieve these goals, the technical scheme is that:
Its aerial part is gathered in field thistle picking time, is cleaned, after washing, fresh squeezing is taken advantage of.In the dregs of a decoction after squeezing, 1 ~ 5 times is added The water of amount, stirs 5 ~ 30min, juice is taken with plate and frame filter press press filtration.The remaining dregs of a decoction press extracting juice again.Merge three concoctions, with 40 ~ 120 mesh screens, obtain field thistle concoction.Obtained field thistle concoction is concentrated under reduced pressure into relative density under the conditions of 40 ~ 75 DEG C is 1.05 ~ 1.30 medicinal extract, and by its in 40 ~ 70 DEG C vacuum drying 12 ~ 48 hours after crushed 60 ~ 120 mesh sieves, be vacuum-packed, Produce fresh squeeze of field thistle and be dried in vacuo powder decoction pieces.
On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, medicine materical crude slice manufacturer, the date of manufacture, The information such as Contents of Main Components, meridian distribution of property and flavor, major function, usage and dosage, toxic side effect and contraindication.Field thistle is enclosed in bag Thin layer differentiates collection of illustrative plates and/or efficient liquid phase characteristic spectrum, is used as " identity card " of product.In addition, in the packaging bag of product, print There is Quick Response Code, former plant photo, medicinal material photo, medicine materical crude slice photo, character and the micro- mirror for obtaining product can be linked by scanning The information such as other feature.
The present invention is advantageous in that:
The field thistle medicinal material of fresh collection, cleans and is directly squeezed after washing, filter, be concentrated under reduced pressure, being dried in vacuo, resulting powder Medicine materical crude slice, the active ingredient in medicinal material can be retained to greatest extent.This medicine materical crude slice volume compared to traditional medicine materical crude slice volume greatly Reduce, vacuum packaging so that prepared slice quality is more stablized, adjusted beneficial to accumulating and clinic, with very significant social effect And economic implications.
Embodiment
Embodiment 1
By the field thistle medicinal material of fresh collection, clean, silt is washed with water, take advantage of using fresh herb squeezer pressure extracting juice.The gained dregs of a decoction add 3 times The running water of amount, stirs 20min, plate and frame filter press pressure extracting juice.The remaining dregs of a decoction press extracting juice with squeezer again.By above-mentioned 3 Secondary concoction merges, with 100 mesh sieve net filtrations.Filtrate decompression is concentrated, and temperature is set as 65 DEG C.In medicinal extract relative density obtained by concentration For 1.15 when, be transferred in vacuum drying chamber, in 60 DEG C dry 48 hours, after crushing cross 60 mesh sieves, pack, 1kg/ bag, addition Packed antioxidant and drier, Vacuum Package.
Embodiment 2
By the field thistle medicinal material of fresh collection, clean, silt is washed with water, take advantage of using fresh herb squeezer pressure extracting juice.The gained dregs of a decoction add 5 times The running water of amount, stirs 30min, plate and frame filter press pressure extracting juice.The remaining dregs of a decoction press extracting juice with squeezer again.By above-mentioned 3 Secondary concoction merges, with 80 mesh sieve net filtrations.Filtrate decompression is concentrated, and temperature is set as 70 DEG C.In medicinal extract relative density obtained by concentration For 1.10 when, be transferred in vacuum drying chamber, in 65 DEG C dry 12 hours, after crushing cross 60 mesh sieves, pack, 1kg/ bag, addition Packed antioxidant and drier, Vacuum Package.
Above example, only illustrates the technological thought of this invention, it is impossible to whereby limit protection scope of the present invention all It is any change done on the basis of technical scheme according to technological thought proposed by the present invention, each falls within what the present invention was protected Within the scope of.

Claims (2)

1. a kind of field thistle is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology, it is characterised in that:It is gathered in field thistle picking time Aerial part, is cleaned, after washing, takes advantage of fresh squeezing, and the dregs of a decoction add the water of 1 ~ 5 times of amount, stir 5 ~ 30min, plate and frame filter press press filtration Juice is taken, the remaining dregs of a decoction press extracting juice again, merge three concoctions, and 40 ~ 120 mesh screens obtain field thistle concoction.
2. a kind of field thistle according to claim 1 is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology, it is characterised in that: Field thistle concoction obtained by claim 1 is concentrated under reduced pressure into the leaching that relative density is 1.05 ~ 1.30 under the conditions of 40 ~ 75 DEG C Cream, and it was crushed into 60 ~ 120 mesh sieves after 12 ~ 48 hours in 40 ~ 70 DEG C of vacuum drying, is vacuum-packed, and produces that field thistle is fresh to squeeze true Empty dried powder medicine materical crude slice.
CN201710466209.0A 2017-06-19 2017-06-19 A kind of field thistle is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology Pending CN107050082A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710466209.0A CN107050082A (en) 2017-06-19 2017-06-19 A kind of field thistle is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710466209.0A CN107050082A (en) 2017-06-19 2017-06-19 A kind of field thistle is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology

Publications (1)

Publication Number Publication Date
CN107050082A true CN107050082A (en) 2017-08-18

Family

ID=59595305

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710466209.0A Pending CN107050082A (en) 2017-06-19 2017-06-19 A kind of field thistle is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology

Country Status (1)

Country Link
CN (1) CN107050082A (en)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107362197A (en) * 2017-08-25 2017-11-21 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Herba Lycopi
CN107362187A (en) * 2017-08-25 2017-11-21 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Artemisia anomala
CN107362182A (en) * 2017-08-25 2017-11-21 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of phoenix-tail fern
CN107375424A (en) * 2017-08-25 2017-11-24 徐自升 A kind of schizonepeta is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology
CN107375348A (en) * 2017-08-25 2017-11-24 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of scouring rush
CN107412433A (en) * 2017-08-25 2017-12-01 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of black nightshade
CN107485641A (en) * 2017-08-25 2017-12-19 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of elscholtiza
CN107582624A (en) * 2017-08-25 2018-01-16 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Pogostemon cablin
CN107714753A (en) * 2017-08-25 2018-02-23 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of gynostemma pentaphylla

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105213445A (en) * 2015-11-14 2016-01-06 芜湖天成普阳中药科技有限公司 A kind of Herba Portulacae fresh squeezing vacuum drying powder decoction pieces and preparation technology thereof

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105213445A (en) * 2015-11-14 2016-01-06 芜湖天成普阳中药科技有限公司 A kind of Herba Portulacae fresh squeezing vacuum drying powder decoction pieces and preparation technology thereof

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107362197A (en) * 2017-08-25 2017-11-21 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Herba Lycopi
CN107362187A (en) * 2017-08-25 2017-11-21 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Artemisia anomala
CN107362182A (en) * 2017-08-25 2017-11-21 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of phoenix-tail fern
CN107375424A (en) * 2017-08-25 2017-11-24 徐自升 A kind of schizonepeta is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology
CN107375348A (en) * 2017-08-25 2017-11-24 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of scouring rush
CN107412433A (en) * 2017-08-25 2017-12-01 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of black nightshade
CN107485641A (en) * 2017-08-25 2017-12-19 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of elscholtiza
CN107582624A (en) * 2017-08-25 2018-01-16 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Pogostemon cablin
CN107714753A (en) * 2017-08-25 2018-02-23 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of gynostemma pentaphylla

Similar Documents

Publication Publication Date Title
CN107050082A (en) A kind of field thistle is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology
CN105998132A (en) Chinese lobelia freshly-squeezed freeze drying powder decoction tablets and preparation process thereof
CN105362309A (en) Herba Portulacae freshly-squeezed freeze-dried powder decoction pieces and preparation process thereof
CN107432883A (en) A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of lopseed
CN107362182A (en) A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of phoenix-tail fern
CN107320508A (en) A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of Chinese trumpet creeper
CN107281236A (en) A kind of Ilex Latifolia Thunb is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology
CN106109544A (en) A kind of Herba Euphorbiae Humifusae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof
CN106109723A (en) A kind of Herba Verbenae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof
CN105998130A (en) Folium Isatidis freshly-pressed lyophilized powdery decoction pieces and preparation process thereof
CN106109545A (en) A kind of Herba Euphorbiae Humifusae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof
CN107028997A (en) A kind of field thistle is fresh to squeeze spray-dried powders medicine materical crude slice and its preparation technology
CN107028998A (en) A kind of field thistle is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology
CN107441223A (en) A kind of fresh preparation technology for squeezing spray-dried granules medicine materical crude slice of cordate houttuynia
CN107281237A (en) A kind of Ilex Latifolia Thunb is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology
CN106109724A (en) A kind of Herba Verbenae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof
CN107375348A (en) A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of scouring rush
CN107233377A (en) A kind of field thistle is fresh to squeeze spray-dried granules medicine materical crude slice and its preparation technology
CN107233367A (en) A kind of Ilex Latifolia Thunb is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology
CN107456473A (en) A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of gerbera
CN107362197A (en) A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Herba Lycopi
CN107412452A (en) A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of field pennycress
CN107375542A (en) A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of field pennycress
CN107432878A (en) A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of scouring rush
CN107375396A (en) A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of fringed pink

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20170818

WD01 Invention patent application deemed withdrawn after publication