CN107233367A - A kind of Ilex Latifolia Thunb is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology - Google Patents
A kind of Ilex Latifolia Thunb is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology Download PDFInfo
- Publication number
- CN107233367A CN107233367A CN201710464536.2A CN201710464536A CN107233367A CN 107233367 A CN107233367 A CN 107233367A CN 201710464536 A CN201710464536 A CN 201710464536A CN 107233367 A CN107233367 A CN 107233367A
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- CN
- China
- Prior art keywords
- ilex latifolia
- latifolia thunb
- fresh
- decoction pieces
- preparation technology
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization
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- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Alternative & Traditional Medicine (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Medical Informatics (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
Powder decoction pieces and its preparation technology are dried in vacuo the invention discloses a kind of fresh squeeze of Ilex Latifolia Thunb.The technique takes advantage of fresh squeezing, leaching concoction after the harvesting of Ilex Latifolia Thunb tender leaf.The dregs of a decoction add water stirring, filtering squeezing.Gained concoction is concentrated under reduced pressure after merging, and is dried in vacuo, and is vacuum-packed after crushing.Broadleaf Holly Leaf medicine materical crude slice prepared by this method, remains the polarity and nonpolar active ingredient in medicinal material to greatest extent.Medicine materical crude slice is beneficial to accumulating, convenient to adjust, quality controllable, and curative effect is reliable, to ensureing that tcm clinical curative effect has great importance.The promotion and implementation of this law, will there is significant social effect and economic benefit.
Description
Technical field
The invention belongs to the processing technology of Chinese medicine manufacture field, more particularly to Chinese medicine Ilex Latifolia Thunb medicine materical crude slice.
Background technology
Chinese medicine Ilex Latifolia Thunb for Holly bitter leaves tree tender leaf it is processed, dry form.This product is bitter, cold, with heat-clearing
Relieve summer heat, eyesight-improving intelligence-developing, promote the production of body fluid to quench thirst, be depressured fat-reducing, suppression cancer anti-cancer etc. multiple efficacies.
The processing mode of conventional Ilex Latifolia Thunb medicine materical crude slice is：Harvest after its tender leaf, dry, rubbing, packaging.Such medicine materical crude slice, body
Product is huge, and Hygienic Index is poor, easily pollutes and goes mouldy, quality it is difficult to ensure that, be unfavorable for the stable of its curative effect and reappear, or even give
Patient brings the harm of recessiveness.
In order to ensure Ilex Latifolia Thunb is clinical effectively, steady quality, a kind of new Ilex Latifolia Thunb medicine materical crude slice and its preparation technology are urgently
Exploitation.
The content of the invention
The invention discloses " a kind of Ilex Latifolia Thunb is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology ".This technique can be with
Retain the polarity and nonpolar active ingredient in Ilex Latifolia Thunb medicinal material while to greatest extent, it is to avoid medicinal material is processed in existing medicine materical crude slice
With the loss of caused active ingredient and the decline of medical material quanlity in storage and transport process, pollution of the medicinal material by mould etc. is reduced, to true
The steady quality and clinical safety for protecting Ilex Latifolia Thunb medicine materical crude slice effectively have great importance.
To achieve these goals, the technical scheme is that：
Its tender leaf is gathered in Ilex Latifolia Thunb picking time, fresh squeezing is taken advantage of.In the dregs of a decoction after squeezing, the water of 1 ~ 5 times of amount of addition, stirring 5 ~
30min, juice is taken with plate and frame filter press press filtration.The remaining dregs of a decoction press extracting juice again.Merge three concoctions, with 40 ~ 120 mesh screens,
Obtain Ilex Latifolia Thunb concoction.It is 1.05 ~ 1.30 that obtained Ilex Latifolia Thunb concoction is concentrated under reduced pressure into relative density under the conditions of 40 ~ 75 DEG C
Medicinal extract, and by its in 40 ~ 70 DEG C vacuum drying 4 ~ 8 hours after crushed 60 ~ 120 mesh sieves, be vacuum-packed, produce Ilex Latifolia Thunb it is fresh squeezing
It is dried in vacuo powder decoction pieces.
On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, medicine materical crude slice manufacturer, the date of manufacture,
The information such as Contents of Main Components, meridian distribution of property and flavor, major function, usage and dosage, toxic side effect and contraindication.Ilex Latifolia Thunb is enclosed in bag
Thin layer differentiate collection of illustrative plates and/or efficient liquid phase characteristic spectrum, be used as " identity card " of product.In addition, in the packaging bag of product,
Quick Response Code is printed on, can be linked by scanning and obtain the former plant photo of product, medicinal material photo, medicine materical crude slice photo, character and micro-
The information such as diagnostic characteristics.
The present invention is advantageous in that：
The Ilex Latifolia Thunb of fresh collection, cleans and is directly squeezed after washing, filter, be concentrated under reduced pressure, being dried in vacuo, resulting powder drink
Piece, the active ingredient in medicinal material can be retained to greatest extent.This medicine materical crude slice volume greatly subtracts compared to traditional medicine materical crude slice volume
It is small, vacuum packaging so that prepared slice quality is more stablized, beneficial to accumulating and it is clinical adjust, with very significant social effect and
Economic implications.
Embodiment
Embodiment 1
By the Ilex Latifolia Thunb tender leaf of fresh collection, clean, wash quickly, take advantage of using fresh herb squeezer pressure extracting juice.The gained dregs of a decoction add 3 times amount
Drinking water, stirs 20min, plate and frame filter press pressure extracting juice.The remaining dregs of a decoction press extracting juice with squeezer again.By above-mentioned 3 medicines
Juice merges, with 100 mesh sieve net filtrations.Filtrate decompression is concentrated, and temperature is set as 65 DEG C.It is in medicinal extract relative density obtained by concentration
When 1.15, it is transferred in vacuum drying chamber, is dried 8 hours in 60 DEG C, 60 mesh sieves are crossed after crushing, pack, is added packed by 1kg/ bags
Antioxidant and drier, Vacuum Package.
Embodiment 2
By the Ilex Latifolia Thunb tender leaf of fresh collection, clean, wash quickly, take advantage of using fresh herb squeezer pressure extracting juice.The gained dregs of a decoction add 5 times amount
Drinking water, stirs 30min, plate and frame filter press pressure extracting juice.The remaining dregs of a decoction press extracting juice with squeezer again.By above-mentioned 3 medicines
Juice merges, with 80 mesh sieve net filtrations.Filtrate decompression is concentrated, and temperature is set as 70 DEG C.It is in medicinal extract relative density obtained by concentration
When 1.10, it is transferred in vacuum drying chamber, is dried 6 hours in 65 DEG C, 60 mesh sieves are crossed after crushing, pack, is added packed by 1kg/ bags
Antioxidant and drier, Vacuum Package.
Above example, only illustrates the technological thought of this invention, it is impossible to whereby limit protection scope of the present invention all
It is any change done on the basis of technical scheme according to technological thought proposed by the present invention, each falls within what the present invention was protected
Within the scope of.
Claims (2)
1. a kind of Ilex Latifolia Thunb is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology, it is characterised in that：Adopted in Ilex Latifolia Thunb picking time
Collect its tender leaf, take advantage of fresh squeezing, the dregs of a decoction add the water of 1 ~ 5 times of amount, stir 5 ~ 30min, and plate and frame filter press press filtration takes juice, the remaining dregs of a decoction
Extracting juice is pressed again, merges three concoctions, and 40 ~ 120 mesh screens obtain Ilex Latifolia Thunb concoction.
2. a kind of Ilex Latifolia Thunb according to claim 1 is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology, its feature exists
In：Obtained Ilex Latifolia Thunb concoction is concentrated under reduced pressure into the medicinal extract that relative density is 1.05 ~ 1.30 under the conditions of 40 ~ 75 DEG C, and will
It crushed 60 ~ 120 mesh sieves after being dried in vacuo 4 ~ 8 hours in 40 ~ 70 DEG C, was vacuum-packed, and produces fresh squeeze of Ilex Latifolia Thunb and is dried in vacuo
Powder decoction pieces.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710464536.2A CN107233367A (en) | 2017-06-19 | 2017-06-19 | A kind of Ilex Latifolia Thunb is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710464536.2A CN107233367A (en) | 2017-06-19 | 2017-06-19 | A kind of Ilex Latifolia Thunb is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107233367A true CN107233367A (en) | 2017-10-10 |
Family
ID=59986303
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710464536.2A Pending CN107233367A (en) | 2017-06-19 | 2017-06-19 | A kind of Ilex Latifolia Thunb is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
Country Status (1)
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|---|---|
| CN (1) | CN107233367A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105213451A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Taraxaci fresh squeezing vacuum drying powder decoction pieces and preparation technology thereof |
| CN105998167A (en) * | 2016-07-23 | 2016-10-12 | 徐自升 | Vacuum-dried powdery medicinal slices prepared from freshly squeezed flos sophorae and preparation process thereof |
| CN105998133A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Chinese lobelia freshly-squeezed vacuum drying powder decoction tablets and preparation process thereof |
| CN106109574A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Scutellariae Barbatae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
-
2017
- 2017-06-19 CN CN201710464536.2A patent/CN107233367A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105213451A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Taraxaci fresh squeezing vacuum drying powder decoction pieces and preparation technology thereof |
| CN105998167A (en) * | 2016-07-23 | 2016-10-12 | 徐自升 | Vacuum-dried powdery medicinal slices prepared from freshly squeezed flos sophorae and preparation process thereof |
| CN105998133A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Chinese lobelia freshly-squeezed vacuum drying powder decoction tablets and preparation process thereof |
| CN106109574A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Scutellariae Barbatae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
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| PB01 | Publication | ||
| PB01 | Publication | ||
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| WD01 | Invention patent application deemed withdrawn after publication | ||
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Application publication date: 20171010 |