CN106109574A - A kind of Herba Scutellariae Barbatae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof - Google Patents

A kind of Herba Scutellariae Barbatae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof Download PDF

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Publication number
CN106109574A
CN106109574A CN201610583174.4A CN201610583174A CN106109574A CN 106109574 A CN106109574 A CN 106109574A CN 201610583174 A CN201610583174 A CN 201610583174A CN 106109574 A CN106109574 A CN 106109574A
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China
Prior art keywords
herba scutellariae
scutellariae barbatae
decoction pieces
fresh
vacuum drying
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CN201610583174.4A
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徐漫
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/53Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
    • A61K36/539Scutellaria (skullcap)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00Medicinal preparations characterised by special physical form
    • A61K9/14Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/13Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/15Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/31Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/39Complex extraction schemes, e.g. fractionation or repeated extraction steps
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/50Methods involving additional extraction steps
    • A61K2236/51Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
  • Medicinal Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Epidemiology (AREA)
  • Chemical & Material Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Veterinary Medicine (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Neurosurgery (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Medical Informatics (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses that a kind of Herba Scutellariae Barbatae is fresh and squeeze vacuum drying powder decoction pieces and preparation technology thereof.This technique after Herba Scutellariae Barbatae medical material is gathered, clean, drip washing, cutting, and take advantage of fresh squeezing, leaching medicine juice.Medicinal residues add water stirring, filter squeezing.Concentrating under reduced pressure after the merging of gained medicine juice, vacuum drying, pulverize final vacuum packaging.Herba Scutellariae Barbatae powder decoction pieces prepared by this method, remains the polarity in medical material and nonpolar effective ingredient to greatest extent.Decoction pieces is beneficial to accumulating, convenient adjustment, and quality controllable, curative effect is reliable, to ensureing that tcm clinical curative effect has great importance.The promotion and implementation of this law, will have significant social meaning and economic benefit.

Description

A kind of Herba Scutellariae Barbatae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Scutellaria barbata decoction pieces.
Background technology
Scutellaria barbata is labiate Herba Scutellariae BarbataeScutellaria barbata D. the dry herb of Don.This product There are heat-clearing and toxic substances removing, blood circulation promoting and blood stasis dispelling, reducing swelling and alleviating pain, anticancer merit.Clinic is commonly used to treat appendicitis, hepatitis, cervical cancer, mammary gland Scorching etc.;External can treat furuncle pain, treating swelling and pain by traumatic injury etc..
The processing mode of conventional Herba Scutellariae Barbatae decoction pieces is: summer, season in autumn two gather, and removes impurity, cleans, dries, then pack Accumulating.This type of prepared herbal medicine in small pieces ready for decoction, bulky, Hygienic Index is poor, easily pollutes and goes mouldy, quality it is difficult to ensure that, be unfavorable for joining Side adjusts and guarantees its clinical efficacy, even brings the harm of recessiveness to patient.
At present, granule pieces market also having Herba Scutellariae Barbatae medical material to make after extracting is sold.The preparation of granule pieces Process, extracts not only time consumption and energy consumption, and because conventional substantial amounts of water does solvent, the nonpolar effective ingredient in medical material is difficult to be carried Take out.Additionally, due to the Herba Scutellariae Barbatae medical material extracted also is to be dried and through long-time storage, therefore, effective ingredient Loss is also the biggest.In order to ensure Herba Scutellariae Barbatae medical material clinical effectively, steady quality, a kind of novel Herba Scutellariae Barbatae decoction pieces and Preparation technology urgently develops.
Summary of the invention
The invention discloses " a kind of Herba Scutellariae Barbatae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof ".This technique is permissible The polarity in Herba Scutellariae Barbatae medical material and nonpolar effective ingredient is retained, it is to avoid medical material is processed at existing decoction pieces while to greatest extent With loss and the decline of medical material quanlity of the effective ingredient caused in storage and transport process, reduce the medical material pollution by mycete etc., to really Steady quality and the clinical safety of protecting Herba Scutellariae Barbatae decoction pieces effectively have great importance.
To achieve these goals, the technical scheme is that
Gather its herb collection period Herba Scutellariae Barbatae, clean, washing, after cutting, take advantage of fresh squeezing.In medicinal residues after squeezing, add 1 ~ 5 The water of times amount, stirs 5 ~ 30min, with filter press filter pressing extracting juice.Remaining medicinal residues squeeze extracting juice again.Merge three medicine juice, use 40 ~ 120 mesh screen, obtain Herba Scutellariae Barbatae medicine juice.The Herba Scutellariae Barbatae medicine juice obtained is evaporated to the closeest under the conditions of 40 ~ 75 DEG C Degree is the extractum of 1.05 ~ 1.30, and by its in 40 ~ 70 DEG C vacuum drying 4 ~ 8 hours after pulverized 60 ~ 120 mesh sieves, vacuum packet Dress, obtains fresh squeezing of Herba Scutellariae Barbatae and is vacuum dried powder decoction pieces.
On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, decoction pieces manufacturer, the date of manufacture, The information such as Contents of Main Components, meridian distribution of property and flavor, function cure mainly, usage and dosage, toxic and side effects and contraindication.The included upper Herba Scutellariae Barbatae of bag Thin layer differentiate collection of illustrative plates and/or high-efficient liquid phase character collection of illustrative plates, as " identity card " of product.Additionally, in the packaging bag of product, It is printed on Quick Response Code, the acquisition former plant photo of product, medical material photo, decoction pieces photo, character and micro-can be linked by scanning The information such as diagnostic characteristics.
The invention have benefit that:
The Herba Scutellariae Barbatae medical material of fresh collection, directly squeeze after cleaning washing, filter, concentrating under reduced pressure, vacuum drying, obtained powder End decoction pieces, can retain the effective ingredient in medical material to greatest extent.This decoction pieces volume compares to tradition decoction pieces volume significantly Ground reduces, vacuum packaging so that prepared slice quality is more stable, and beneficially accumulating and clinic is adjusted, and has very significantly society's meaning Justice and economic implications.
Detailed description of the invention
Embodiment 1
By the Herba Scutellariae Barbatae medical material of fresh collection, clean, wash silt with water, be cut into the section of 3cm, take advantage of the squeezing of using fresh herb squeezer and take Juice.Gained medicinal residues add the drinking water of 3 times amount, stir 20min, filter press squeezing extracting juice.Squeezer used again by remaining medicinal residues Squeezing extracting juice.Above-mentioned 3 medicine juice are merged, filters with 100 eye mesh screens.Filtrate reduced in volume, temperature is set as 65 DEG C.Concentrating When gained extractum relative density is 1.15, transfer in vacuum drying oven, be dried 8 hours in 60 DEG C, after pulverizing, cross 60 mesh sieves, dress Bag, 1kg/ bag, add packed antioxidant and desiccant, Vacuum Package.
Embodiment 2
By the Herba Scutellariae Barbatae medical material of fresh collection, clean, wash silt with water, be cut into the section of 6cm, take advantage of the squeezing of using fresh herb squeezer and take Juice.Gained medicinal residues add the drinking water of 5 times amount, stir 30min, filter press squeezing extracting juice.Squeezer used again by remaining medicinal residues Squeezing extracting juice.Above-mentioned 3 medicine juice are merged, filters with 80 eye mesh screens.Filtrate reduced in volume, temperature is set as 70 DEG C.Concentrating When gained extractum relative density is 1.10, transfer in vacuum drying oven, be dried 6 hours in 65 DEG C, after pulverizing, cross 60 mesh sieves, dress Bag, 1kg/ bag, add packed antioxidant and desiccant, Vacuum Package.
Above example, is only the technological thought that this invention is described, it is impossible to limit protection scope of the present invention whereby all It is the technological thought proposed according to the present invention, any change done on the basis of technical scheme, each fall within present invention protection Within the scope of.

Claims (2)

1. fresh squeezing of Herba Scutellariae Barbatae is vacuum dried powder decoction pieces and preparation technology thereof, it is characterised in that: adopt collection period Herba Scutellariae Barbatae Collect its herb, clean, washing, after cutting, take advantage of fresh squeezing, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, filter press Filter pressing extracting juice, remaining medicinal residues squeeze extracting juice again, merge three medicine juice, 40 ~ 120 mesh screen, obtain Herba Scutellariae Barbatae medicine juice.
A kind of Herba Scutellariae Barbatae the most according to claim 1 is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof, and its feature exists In: the Herba Scutellariae Barbatae medicine juice obtained is evaporated under the conditions of 40 ~ 75 DEG C the extractum that relative density is 1.05 ~ 1.30, and will It pulverized 60 ~ 120 mesh sieves after being vacuum dried 4 ~ 8 hours in 40 ~ 70 DEG C, vacuum packaging, obtains fresh squeezing of Herba Scutellariae Barbatae and is vacuum dried Powder decoction pieces.
CN201610583174.4A 2016-07-24 2016-07-24 A kind of Herba Scutellariae Barbatae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof Pending CN106109574A (en)

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107233367A (en) * 2017-06-19 2017-10-10 徐漫 A kind of Ilex Latifolia Thunb is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology
CN107334814A (en) * 2017-08-25 2017-11-10 芜湖天成普阳中药科技有限公司 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Longtube Ground Ivy Herb
CN107362197A (en) * 2017-08-25 2017-11-21 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Herba Lycopi
CN107362182A (en) * 2017-08-25 2017-11-21 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of phoenix-tail fern
CN107375348A (en) * 2017-08-25 2017-11-24 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of scouring rush
CN107485642A (en) * 2017-08-25 2017-12-19 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Sculellaria barbata
CN107485641A (en) * 2017-08-25 2017-12-19 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of elscholtiza
CN107714753A (en) * 2017-08-25 2018-02-23 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of gynostemma pentaphylla

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105193894A (en) * 2015-11-14 2015-12-30 芜湖天成普阳中药科技有限公司 Freshly squeezed vacuum drying cholla stem powdery decoction pieces and preparation process thereof
CN105194009A (en) * 2015-11-14 2015-12-30 芜湖天成普阳中药科技有限公司 Freshly squeezed vacuum drying spreading hedyotis herb powdery decoction pieces and preparation process thereof
CN105213451A (en) * 2015-11-14 2016-01-06 芜湖天成普阳中药科技有限公司 A kind of Herba Taraxaci fresh squeezing vacuum drying powder decoction pieces and preparation technology thereof
CN105213740A (en) * 2015-11-14 2016-01-06 芜湖天成普阳中药科技有限公司 A kind of Aloe fresh squeezing vacuum drying powder decoction pieces and preparation technology thereof
CN105213445A (en) * 2015-11-14 2016-01-06 芜湖天成普阳中药科技有限公司 A kind of Herba Portulacae fresh squeezing vacuum drying powder decoction pieces and preparation technology thereof
CN105287861A (en) * 2015-11-22 2016-02-03 徐漫 Freshly-squeezed paulownia flower vacuum-dried powdery decoction piece and preparation technology thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105193894A (en) * 2015-11-14 2015-12-30 芜湖天成普阳中药科技有限公司 Freshly squeezed vacuum drying cholla stem powdery decoction pieces and preparation process thereof
CN105194009A (en) * 2015-11-14 2015-12-30 芜湖天成普阳中药科技有限公司 Freshly squeezed vacuum drying spreading hedyotis herb powdery decoction pieces and preparation process thereof
CN105213451A (en) * 2015-11-14 2016-01-06 芜湖天成普阳中药科技有限公司 A kind of Herba Taraxaci fresh squeezing vacuum drying powder decoction pieces and preparation technology thereof
CN105213740A (en) * 2015-11-14 2016-01-06 芜湖天成普阳中药科技有限公司 A kind of Aloe fresh squeezing vacuum drying powder decoction pieces and preparation technology thereof
CN105213445A (en) * 2015-11-14 2016-01-06 芜湖天成普阳中药科技有限公司 A kind of Herba Portulacae fresh squeezing vacuum drying powder decoction pieces and preparation technology thereof
CN105287861A (en) * 2015-11-22 2016-02-03 徐漫 Freshly-squeezed paulownia flower vacuum-dried powdery decoction piece and preparation technology thereof

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107233367A (en) * 2017-06-19 2017-10-10 徐漫 A kind of Ilex Latifolia Thunb is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology
CN107334814A (en) * 2017-08-25 2017-11-10 芜湖天成普阳中药科技有限公司 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Longtube Ground Ivy Herb
CN107362197A (en) * 2017-08-25 2017-11-21 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Herba Lycopi
CN107362182A (en) * 2017-08-25 2017-11-21 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of phoenix-tail fern
CN107375348A (en) * 2017-08-25 2017-11-24 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of scouring rush
CN107485642A (en) * 2017-08-25 2017-12-19 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Sculellaria barbata
CN107485641A (en) * 2017-08-25 2017-12-19 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of elscholtiza
CN107714753A (en) * 2017-08-25 2018-02-23 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of gynostemma pentaphylla

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Application publication date: 20161116