CN105193894A - Freshly squeezed vacuum drying cholla stem powdery decoction pieces and preparation process thereof - Google Patents
Freshly squeezed vacuum drying cholla stem powdery decoction pieces and preparation process thereof Download PDFInfo
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- CN105193894A CN105193894A CN201510774367.3A CN201510774367A CN105193894A CN 105193894 A CN105193894 A CN 105193894A CN 201510774367 A CN201510774367 A CN 201510774367A CN 105193894 A CN105193894 A CN 105193894A
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- radix
- decoction pieces
- caulis opuntiae
- opuntiae dillenii
- vacuum drying
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Abstract
The invention discloses freshly squeezed vacuum drying cholla stem powdery decoction pieces and a preparation process thereof. The process is characterized by harvesting the medicinal material cholla stem, then cleaning, selecting and drip-washing cholla stem, squeezing cholla stem while cholla stem is fresh and taking the juice after filtration; adding water to the dregs, stirring the dregs and carrying out filtering and squeezing; mixing the obtained juice and then carrying out vacuum concentration, carrying out vacuum drying and carrying out vacuum packaging after grinding. The cholla stem powdery decoction pieces prepared by the method furthest retain the polar and nonpolar active ingredients in the medicinal material, are easy to store and transport and convenient to regulate, are controllable in quality, have reliable curative effects and have great significance in guaranteeing the clinical effects of traditional Chinese medicines. Popularization and implementation of the method has remarkable social significance and economic benefits.
Description
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Chinese medicine Radix et Caulis Opuntiae Dillenii decoction pieces.
Background technology
Chinese medicine Radix et Caulis Opuntiae Dillenii is Cactaeous plants Radix et Caulis Opuntiae Dillenii
opuntiastricta(Haw.) Haw.var.
dillenii(Ker-Gawl.) the dry meat stem of Benson.This product has promoting flow of QI and blood, effect of heat-clearing and toxic substances removing.Be mainly used in dysentery, cough, acute mastitis, the treatment of scald etc.
The processing mode of common Radix et Caulis Opuntiae Dillenii decoction pieces is: after medical material is gathered, and removing impurity, is cut into block, dries, then accumulating of packing.This type of prepared herbal medicine in small pieces ready for decoction, bulky, Hygienic Index is poor, is easy to pollute and go mouldy, and quality is difficult to ensure, is unfavorable for that formula is adjusted and guarantees its clinical efficacy, even brings recessive harm to patient.In addition, because Radix et Caulis Opuntiae Dillenii is fleshy stem, be difficult to dry; And the Radix et Caulis Opuntiae Dillenii dried has much small thorn, can fly upward with the wind in atmosphere, be easy to be inhaled into, or prick skin and difficulty is found, bring to production and processing personnel and bother.Therefore, in order to ensure the safety of operator, also in order to clinical effective, the steady quality of Radix et Caulis Opuntiae Dillenii medical material, a kind of novel Radix et Caulis Opuntiae Dillenii decoction pieces and preparation technology thereof urgently develop.
Summary of the invention
The present invention discloses " a kind of Radix et Caulis Opuntiae Dillenii fresh squeezing vacuum drying powder decoction pieces and preparation technology thereof ".This technique can retain polarity in Radix et Caulis Opuntiae Dillenii medical material and nonpolar effective ingredient to greatest extent simultaneously, the loss of effective ingredient avoiding medical material to cause in existing decoction pieces processing and storage and transport process and the decline of medical material quanlity, reduce the pollution of medical material by mycete etc., the steady quality and clinical safety guaranteeing Radix et Caulis Opuntiae Dillenii decoction pieces is effectively had great importance.
To achieve these goals, technical scheme of the present invention is:
Gather its herb collection period at Radix et Caulis Opuntiae Dillenii, clean, after washing, take advantage of fresh squeezing.In medicinal residues after squeezing, add the water of 1 ~ 5 times amount, stir 5 ~ 30min, with filter press filter pressing extracting juice.Remaining medicinal residues squeeze extracting juice again.Merge three medicine juice, with 40 ~ 120 mesh screen.Filtrate buchner funnel, double-layer filter paper sucking filtration, obtains Radix et Caulis Opuntiae Dillenii medicine juice.The Radix et Caulis Opuntiae Dillenii medicine juice obtained is evaporated to the extractum that relative density is 1.05 ~ 1.30 under 40 ~ 75 DEG C of conditions, and it was pulverized 60 ~ 120 mesh sieves after 4 ~ 8 hours, vacuum packaging in 40 ~ 70 DEG C of vacuum dryings, obtain Radix et Caulis Opuntiae Dillenii fresh squeezing vacuum drying powder decoction pieces.
On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, decoction pieces manufacturer, date of manufacture, Contents of Main Components, meridian distribution of property and flavor, function cure mainly, the information such as usage and dosage, toxic and side effects and contraindication.TLC distinguish collection of illustrative plates and/or the high-efficient liquid phase character collection of illustrative plates of Radix et Caulis Opuntiae Dillenii is enclosed, as " identity card " of product in bag.In addition, in the packaging bag of product, be printed on Quick Response Code, the information such as former plant photo, medical material photo, decoction pieces photo, character and the microscopical identification feature obtaining product can be linked by scanning.
Usefulness of the present invention is:
The Radix et Caulis Opuntiae Dillenii medical material of fresh collection, direct squeezing, filtration, concentrating under reduced pressure, vacuum drying after cleaning washing, the powder decoction pieces obtained, can retain the effective ingredient in medical material to greatest extent.This decoction pieces volume compares to traditional decoction pieces volume and reduces widely, and vacuum packaging, makes prepared slice quality more stable, is beneficial to accumulating and clinical adjustment, has very significant social meaning and economic implications.
Detailed description of the invention
Embodiment 1
By the Radix et Caulis Opuntiae Dillenii medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add the drinking water of 3 times amount, stir 20min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.Above-mentioned 3 medicine juice are merged, filters with 100 eye mesh screens.Filtrate buchner funnel, double-layer filter paper sucking filtration.Gained takes out filtrate reduced in volume, and temperature is set as 65 DEG C.When concentrated gained extractum relative density is 1.15, transfer in vacuum drying oven, in 60 DEG C of dryings 8 hours, cross 60 mesh sieves after pulverizing, pack, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package.
Embodiment 2
By the Radix et Caulis Opuntiae Dillenii medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add the drinking water of 5 times amount, stir 30min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.Above-mentioned 3 medicine juice are merged, filters with 80 eye mesh screens.Filtrate buchner funnel, double-layer filter paper sucking filtration.Gained takes out filtrate reduced in volume, and temperature is set as 70 DEG C.When concentrated gained extractum relative density is 1.10, transfer in vacuum drying oven, in 65 DEG C of dryings 6 hours, cross 60 mesh sieves after pulverizing, pack, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package.
Above embodiment, is only the technological thought that this invention is described, can not limit the every technological thought proposed according to the present invention of protection scope of the present invention whereby, any change that technical scheme basis is done, all falls within the scope of protection of the invention.
Claims (2)
1. Radix et Caulis Opuntiae Dillenii fresh squeezing vacuum drying powder decoction pieces and a preparation technology thereof, is characterized in that: gather its fleshy stem collection period at Radix et Caulis Opuntiae Dillenii, clean, washing, take advantage of fresh squeezing, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, filter press filter pressing extracting juice, remaining medicinal residues squeeze extracting juice again, merge three medicine juice, 40 ~ 120 mesh screen, filtrate uses buchner funnel sucking filtration, obtains Radix et Caulis Opuntiae Dillenii medicine juice.
2. a kind of Radix et Caulis Opuntiae Dillenii fresh squeezing vacuum drying powder decoction pieces according to claim 1 and preparation technology thereof, it is characterized in that: the Radix et Caulis Opuntiae Dillenii medicine juice obtained in claim 1 is evaporated to the extractum that relative density is 1.05 ~ 1.30 under 40 ~ 75 DEG C of conditions, and it was pulverized 60 ~ 120 mesh sieves in 40 ~ 70 DEG C of vacuum dryings after 4 ~ 8 hours, vacuum packaging, obtains Radix et Caulis Opuntiae Dillenii fresh squeezing vacuum drying powder decoction pieces.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510774367.3A CN105193894A (en) | 2015-11-14 | 2015-11-14 | Freshly squeezed vacuum drying cholla stem powdery decoction pieces and preparation process thereof |
Applications Claiming Priority (1)
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| CN201510774367.3A CN105193894A (en) | 2015-11-14 | 2015-11-14 | Freshly squeezed vacuum drying cholla stem powdery decoction pieces and preparation process thereof |
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| CN105193894A true CN105193894A (en) | 2015-12-30 |
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| CN201510774367.3A Pending CN105193894A (en) | 2015-11-14 | 2015-11-14 | Freshly squeezed vacuum drying cholla stem powdery decoction pieces and preparation process thereof |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105998133A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Chinese lobelia freshly-squeezed vacuum drying powder decoction tablets and preparation process thereof |
| CN106074657A (en) * | 2016-07-23 | 2016-11-09 | 徐漫 | A kind of Folium Isatidis is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
| CN106109723A (en) * | 2016-07-23 | 2016-11-16 | 徐漫 | A kind of Herba Verbenae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
| CN106109574A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Scutellariae Barbatae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
| CN106109544A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Euphorbiae Humifusae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
| CN107157935A (en) * | 2017-06-20 | 2017-09-15 | 徐漫 | A kind of acalypha copperleaf is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107320527A (en) * | 2017-08-25 | 2017-11-07 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of mulberry leaf |
| CN107441137A (en) * | 2017-08-25 | 2017-12-08 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of tussilago |
| CN107648329A (en) * | 2016-07-23 | 2018-02-02 | 徐漫 | A kind of hairyvein agrimony is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN108095101A (en) * | 2018-02-07 | 2018-06-01 | 习水红四渡仙人掌产业有限公司 | A kind of cactus medicine materical crude slice with healthcare function and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1076623A (en) * | 1993-03-09 | 1993-09-29 | 沈阳药学院 | Cactus preparation and preparation method thereof |
| CN1507805A (en) * | 2002-12-18 | 2004-06-30 | 烟台市泰丰种植养殖科技有限公司 | Cactus juice and preparing method thereof |
| CN102911283A (en) * | 2012-11-09 | 2013-02-06 | 中国科学院烟台海岸带研究所 | Novel technology capable of extracting inulin through pressing method |
-
2015
- 2015-11-14 CN CN201510774367.3A patent/CN105193894A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1076623A (en) * | 1993-03-09 | 1993-09-29 | 沈阳药学院 | Cactus preparation and preparation method thereof |
| CN1507805A (en) * | 2002-12-18 | 2004-06-30 | 烟台市泰丰种植养殖科技有限公司 | Cactus juice and preparing method thereof |
| CN102911283A (en) * | 2012-11-09 | 2013-02-06 | 中国科学院烟台海岸带研究所 | Novel technology capable of extracting inulin through pressing method |
Non-Patent Citations (3)
| Title |
|---|
| 傅超美等: "《中药药剂学》", 31 August 2014, 中国医药科技出版社 * |
| 南京药学院药剂学教研组: "《药剂学》", 31 May 1962, 人民卫生出版社 * |
| 郭宏昌: "《中草药抗肿瘤便览》", 30 November 2014, 新疆人民卫生出版社 * |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105998133A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Chinese lobelia freshly-squeezed vacuum drying powder decoction tablets and preparation process thereof |
| CN106074657A (en) * | 2016-07-23 | 2016-11-09 | 徐漫 | A kind of Folium Isatidis is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
| CN106109723A (en) * | 2016-07-23 | 2016-11-16 | 徐漫 | A kind of Herba Verbenae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
| CN107648329A (en) * | 2016-07-23 | 2018-02-02 | 徐漫 | A kind of hairyvein agrimony is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN106109574A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Scutellariae Barbatae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
| CN106109544A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Euphorbiae Humifusae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
| CN107157935A (en) * | 2017-06-20 | 2017-09-15 | 徐漫 | A kind of acalypha copperleaf is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107320527A (en) * | 2017-08-25 | 2017-11-07 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of mulberry leaf |
| CN107441137A (en) * | 2017-08-25 | 2017-12-08 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of tussilago |
| CN108095101A (en) * | 2018-02-07 | 2018-06-01 | 习水红四渡仙人掌产业有限公司 | A kind of cactus medicine materical crude slice with healthcare function and preparation method thereof |
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Application publication date: 20151230 |
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