CN102911283A - Novel technology capable of extracting inulin through pressing method - Google Patents
Novel technology capable of extracting inulin through pressing method Download PDFInfo
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- CN102911283A CN102911283A CN2012104440815A CN201210444081A CN102911283A CN 102911283 A CN102911283 A CN 102911283A CN 2012104440815 A CN2012104440815 A CN 2012104440815A CN 201210444081 A CN201210444081 A CN 201210444081A CN 102911283 A CN102911283 A CN 102911283A
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- jerusalem artichoke
- inulin
- juice
- extracting solution
- slag
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- JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 title claims abstract description 42
- 229920001202 Inulin Polymers 0.000 title claims abstract description 38
- 229940029339 inulin Drugs 0.000 title claims abstract description 38
- 238000005516 engineering process Methods 0.000 title abstract description 5
- 238000003825 pressing Methods 0.000 title abstract 2
- 235000003230 Helianthus tuberosus Nutrition 0.000 claims abstract description 52
- 240000008892 Helianthus tuberosus Species 0.000 claims abstract description 52
- 238000000034 method Methods 0.000 claims abstract description 29
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 27
- 239000002893 slag Substances 0.000 claims abstract description 26
- 239000000284 extract Substances 0.000 claims abstract description 14
- 238000001728 nano-filtration Methods 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000012535 impurity Substances 0.000 claims abstract description 11
- 239000012528 membrane Substances 0.000 claims abstract description 11
- 238000003756 stirring Methods 0.000 claims abstract description 11
- 238000001035 drying Methods 0.000 claims abstract description 8
- 238000001914 filtration Methods 0.000 claims abstract description 8
- 238000010612 desalination reaction Methods 0.000 claims abstract description 7
- 239000012065 filter cake Substances 0.000 claims abstract description 6
- 239000000725 suspension Substances 0.000 claims abstract description 6
- 230000001954 sterilising effect Effects 0.000 claims abstract description 3
- 239000012610 weak anion exchange resin Substances 0.000 claims abstract description 3
- 230000008569 process Effects 0.000 claims description 13
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 10
- 239000011347 resin Substances 0.000 claims description 10
- 229920005989 resin Polymers 0.000 claims description 10
- 238000003801 milling Methods 0.000 claims description 7
- 238000001125 extrusion Methods 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 5
- 238000005507 spraying Methods 0.000 claims description 5
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims description 4
- 235000011941 Tilia x europaea Nutrition 0.000 claims description 4
- 239000004571 lime Substances 0.000 claims description 4
- 239000012141 concentrate Substances 0.000 claims description 2
- 238000004659 sterilization and disinfection Methods 0.000 claims description 2
- 238000000605 extraction Methods 0.000 abstract description 16
- 238000005265 energy consumption Methods 0.000 abstract description 4
- 238000004061 bleaching Methods 0.000 abstract 1
- 239000012607 strong cation exchange resin Substances 0.000 abstract 1
- 235000013305 food Nutrition 0.000 description 5
- 150000001768 cations Chemical class 0.000 description 4
- 125000000129 anionic group Chemical group 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 239000000706 filtrate Substances 0.000 description 3
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000007598 dipping method Methods 0.000 description 2
- 239000008103 glucose Substances 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 235000007542 Cichorium intybus Nutrition 0.000 description 1
- 244000298479 Cichorium intybus Species 0.000 description 1
- 206010009944 Colon cancer Diseases 0.000 description 1
- 206010010774 Constipation Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 229930091371 Fructose Natural products 0.000 description 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- 239000005715 Fructose Substances 0.000 description 1
- 208000008589 Obesity Diseases 0.000 description 1
- LPQOADBMXVRBNX-UHFFFAOYSA-N ac1ldcw0 Chemical compound Cl.C1CN(C)CCN1C1=C(F)C=C2C(=O)C(C(O)=O)=CN3CCSC1=C32 LPQOADBMXVRBNX-UHFFFAOYSA-N 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 208000029742 colonic neoplasm Diseases 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 235000013325 dietary fiber Nutrition 0.000 description 1
- BJHIKXHVCXFQLS-UYFOZJQFSA-N fructose group Chemical group OCC(=O)[C@@H](O)[C@H](O)[C@H](O)CO BJHIKXHVCXFQLS-UYFOZJQFSA-N 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 235000004213 low-fat Nutrition 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 235000020824 obesity Nutrition 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 239000006041 probiotic Substances 0.000 description 1
- 235000018291 probiotics Nutrition 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000035755 proliferation Effects 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 238000000108 ultra-filtration Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
A novel technology capable of extracting inulin through a pressing method comprises the following steps: 1, performing juice squeezing Jerusalem artichoke which is cleaned and peeled, and respectively collecting Jerusalem artichoke juice and Jerusalem artichoke slag; 2, adding the Jerusalem artichoke slag in water for stirring and further extracting, and filtering to obtain an extract and Jerusalem artichoke slag filter cakes; 3, combining the Jerusalem artichoke juice and the extract, and filtering to remove suspension insoluble impurities so as to obtain a total extract; and 4, allowing the total extract to be subjected to edulcoration, bleaching and filtering, and adopting a nanofiltration membrane to perform concentration; sterilizing the concentrated solution after being subjected to desalination by strong cation exchange resin and weak anion exchange resin; and drying the sterilized solution to obtain the inulin. The method greatly reduces energy consumption and water consumption during the inulin extraction process, at the same time, the inulin extraction rate can reach more than 85 percent, the inulin is pure in colour, the purity is higher than or equal to 92 percent, and ash content is less than or equal to 0.25 percent, therefore, the comprehensive economic benefit is higher.
Description
Technical field
The present invention relates to the new resource food processing technique field, particularly produce the method for inulin with Jerusalem artichoke raw material.
Background technology
Inulin (Inulin) derives from the plants such as jerusalem artichoke, witloof, is a kind of functional Polylevulosan, also is unique water-soluble dietary fibre.Inulin is to be connected with β-(2,1) glycosidic link by D-fructofuranose molecule to generate, and major part is fructose on this chain, and a glucose is arranged endways, makes inulin have different character.Inulin has reducing blood-fat, improves intestinal environment, promotes proliferation of probiotics, anti-ly treats constipation, prevent colon cancer, promotion mineral absorption, obesity prevention, do not cause and can be used as the physiological functions such as diabetes patient by blood glucose fluctuation.Inulin has been accessory substance by more than 20 state approval in the world as a kind of functional ingredient of pure natural, is widely used in milk-product, beverage, low-fat low-calorie food, bakes and banks up with earth in food, the protective foods.China Ministry of Health was approved as new resource food with inulin in 2009.
The inulin processing technology mainly contains hot dipping extraction of the juice, two carbon method and the coupling of resin purification method, ultra-filtration technique, countercurrent extraction technology etc.In actually operating, hot dipping extraction of the juice efficient is low, water consumption is large; The decolouring of two carbon method can cause a large amount of wastes of material; Resin purification adopts reinforcing yin essence resin cation (R.C.) and weak zwitterion resin to be used in conjunction the purpose that reaches desalination usually, and material can be caused damage by resin absorption, affects the inulin yield.Although countercurrent extraction technology efficient is higher, facility investment is higher, and energy consumption is higher in the equipment running process.In a word, traditional technology at extraction yield, take off monose, decolour, go the aspect such as mineral substance to have some problems, have the shortcomings such as water consumption is large, power consumption is higher, extraction yield is lower, operation is grown, cost is higher.The application of the countercurrent extraction technology of inulin in inulin extracts is a much progress of industry, but also has the higher shortcoming of energy consumption.
Summary of the invention
The purpose of this invention is to provide a kind of technique of producing inulin, solve the shortcomings such as the prior art water consumption is large, power consumption is higher, extraction yield is lower, operation is long, cost is higher.
Technical scheme of the present invention may further comprise the steps:
(1), will clean jerusalem artichoke rear jerusalem artichoke juice and the jerusalem artichoke slag collected respectively of squeezing the juice of decortication;
(2), the jerusalem artichoke slag added entry stir to extract, filter and obtain extracting solution and jerusalem artichoke slag filter cake;
(3), merge jerusalem artichoke juice and extracting solution, remove by filter the suspension insoluble impurities and obtain total extracting solution;
(4), total extracting solution passed through removal of impurities, decolouring, filtration successively after, adopt nanofiltration membrane to concentrate; Sterilize after concentrated solution process strong cation-exchanging resin and the weak anion exchange resin desalination; Solution after the sterilization carries out obtaining inulin after the drying.
Such scheme also comprises following optimal way:
Described step (1) is squeezed the juice and is adopted the screw extrusion juice extractor.
Described step (2) water is pure water, and its add-on is no more than the twice of jerusalem artichoke slag weight; The temperature of stir extracting is that 70-100 ℃, time are 20-80 minute.
Lime carbonating method is adopted in removal of impurities in the described step (4), and the activated carbon decolorizing method is adopted in decolouring, and nanofiltration membrane adopts the daltonian nanofiltration membrane of molecular weight cut-off 200-300, is used for removing small molecular weight impurity and moisture; The described dry spraying drying that adopts,
Described lime carbonating method is: add solid Ca(OH in total extracting solution)
2, regulate pH value 10.0, stirred 30 minutes, then pass into CO
2Gas reaches till 7.0 pH value; Described activated carbon decolorizing method is: adding accounts for total extracting solution gross weight 2 ‰ gacs, decolours 30 minutes; Inulin concentration was 20% after described nanofiltration membrane was concentrated.
The present invention is under the prerequisite of the higher inulin extraction yield of maintenance, technological process is mainly extracted inulin with the normal temperature milling process, inulin extraction process Simple fast in early stage, do not use a large amount of hot water in the technological process, therefore greatly reduce energy consumption and water consumption in the inulin leaching process, the inulin extraction yield can reach more than 85% simultaneously, the inulin color that obtains is pure, purity 〉=92%, ash content≤0.25%, so overall economic efficiency is higher.
Embodiment
The present invention is described further below in conjunction with specific embodiment.
Embodiment 1
The bright jerusalem artichoke of 10kg is cleaned decortication; The jerusalem artichoke of cleaning after peeling is sent into the screw extrusion juice extractor, collect respectively jerusalem artichoke juice and jerusalem artichoke slag; Obtain 6.8kg jerusalem artichoke juice and 3.0kg jerusalem artichoke slag (step such as decortication has loss); The jerusalem artichoke slag is added in the extraction still, and 75 ℃ the pure water that adds again 1.5kg stirs and extracts 75min, and press filtration obtains extracting solution and jerusalem artichoke slag filter cake; Merge jerusalem artichoke juice and jerusalem artichoke slag extracting solution, remove by filter the suspension insoluble impurities, add Ca(OH)
2Solid stirs that (pH value keeps 10.0) passes into CO after 30 minutes
2Gas makes pH value reach 7.0, add again 2 ‰ gacs, decoloured 30 minutes, filter, it is about 20% that filtrate is concentrated into inulin concentration through nanofiltration (200 dalton), and concentrated solution is after strong cation and the desalination of weakly anionic resin exchange column, spraying drying, obtain white inulin powder 1.1kg, purity 93%, ash content 0.2%.
Embodiment 2
The bright jerusalem artichoke of 15kg is cleaned decortication; The jerusalem artichoke of cleaning after peeling is sent into the screw extrusion juice extractor, collect respectively jerusalem artichoke juice and jerusalem artichoke slag; Obtain 10.5kg jerusalem artichoke juice and 4.2kg jerusalem artichoke slag (step such as decortication has loss); The jerusalem artichoke slag of gained adds in the extraction still in the step 3, and the pure water that adds again 85 ℃ of 4.2kg stirs and extracts 50min, and press filtration obtains extracting solution and jerusalem artichoke slag filter cake; Merge jerusalem artichoke juice and jerusalem artichoke slag extracting solution, remove by filter the suspension insoluble impurities, add Ca(OH)
2Solid stirs that (pH value keeps 10.0) passes into CO after 30 minutes
2Gas makes pH value reach 7.0, add again 2 ‰ gacs, decoloured 30 minutes, filter, it is about 20% that filtrate is concentrated into inulin concentration through nanofiltration (200 dalton), and concentrated solution is after strong cation and the desalination of weakly anionic resin exchange column, spraying drying, obtain white inulin powder 1.7kg, purity 92%, ash content 0.25%.
Embodiment 3
The bright jerusalem artichoke of 8kg is cleaned decortication; The jerusalem artichoke of cleaning after peeling is sent into the screw extrusion juice extractor, collect respectively jerusalem artichoke juice and jerusalem artichoke slag; Obtain 5.4kg jerusalem artichoke juice and 2.5kg jerusalem artichoke slag (step such as decortication has loss); The jerusalem artichoke slag of gained adds in the extraction still in the step 3, and the pure water that adds again 95 ℃ of 5.0kg stirs and extracts 25min, and press filtration obtains extracting solution and jerusalem artichoke slag filter cake; Merge jerusalem artichoke juice and jerusalem artichoke slag extracting solution, remove by filter the suspension insoluble impurities, add Ca(OH)
2Solid stirs that (pH value keeps 10.0) passes into CO after 30 minutes
2Gas makes pH value reach 7.0, add again 2 ‰ gacs, decoloured 30 minutes, filter, it is about 20% that filtrate is concentrated into inulin concentration through nanofiltration (200 dalton), and concentrated solution is after strong cation and the desalination of weakly anionic resin exchange column, spraying drying, obtain white inulin powder 0.85kg, purity 94%, ash content 0.18%.
Embodiment 4
Keep only nanofiltration membrane being changed into molecular weight cut-off 300 daltonian nanofiltration membrane on the constant basis of embodiment 1 other technological processs; Obtain white inulin powder 1.2kg, purity 92.5%, ash content 0.22%.
Above-described embodiment 1-4 only is exemplary embodiments of the present invention, and those skilled in the art can technical scheme according to the present invention make simple adjustment fully, but identical with flesh and blood of the present invention, therefore falls within protection scope of the present invention equally.
Claims (5)
1. a milling process extracts the inulin novel process, it is characterized in that concrete steps are:
(1), will clean jerusalem artichoke rear jerusalem artichoke juice and the jerusalem artichoke slag collected respectively of squeezing the juice of decortication;
(2), the jerusalem artichoke slag added entry stir to extract, filter and obtain extracting solution and jerusalem artichoke slag filter cake;
(3), merge jerusalem artichoke juice and extracting solution, remove by filter the suspension insoluble impurities and obtain total extracting solution;
(4), total extracting solution passed through removal of impurities, decolouring, filtration successively after, adopt nanofiltration membrane to concentrate; Sterilize after concentrated solution process strong cation-exchanging resin and the weak anion exchange resin desalination; Solution after the sterilization carries out obtaining inulin after the drying.
2. milling process according to claim 1 extracts the inulin novel process, it is characterized in that, described step (1) is squeezed the juice and adopted the screw extrusion juice extractor.
3. milling process according to claim 1 and 2 extracts the inulin novel process, it is characterized in that described step (2) water is pure water, and its add-on is no more than the twice of jerusalem artichoke slag weight; The temperature of stir extracting is that 70-100 ℃, time are 20-80 minute.
4. milling process according to claim 1 and 2 extracts the inulin novel process, it is characterized in that, lime carbonating method is adopted in removal of impurities in the described step (4), and the activated carbon decolorizing method is adopted in decolouring, and nanofiltration membrane adopts the daltonian nanofiltration membrane of molecular weight cut-off 200-300; The described dry spraying drying that adopts.
5. milling process according to claim 4 extracts the inulin novel process, it is characterized in that described lime carbonating method is: add solid Ca(OH in total extracting solution)
2, regulate pH value 10.0, stirred 30 minutes, then pass into CO
2Gas reaches till 7.0 pH value; Described activated carbon decolorizing method is: adding accounts for total extracting solution gross weight 2 ‰ gacs, decolours 30 minutes; Inulin concentration was 20% after described nanofiltration membrane was concentrated.
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| CN201210444081.5A CN102911283B (en) | 2012-11-09 | 2012-11-09 | Novel technology capable of extracting inulin through squeezing method |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103923231A (en) * | 2014-04-18 | 2014-07-16 | 中国科学院烟台海岸带研究所 | Method for continuously preparing inulin and pectin by using jerusalem artichoke and/or endives |
| CN104987434A (en) * | 2015-07-15 | 2015-10-21 | 中国科学院烟台海岸带研究所 | Method for extracting inulin by medium-low-temperature water |
| CN105193894A (en) * | 2015-11-14 | 2015-12-30 | 芜湖天成普阳中药科技有限公司 | Freshly squeezed vacuum drying cholla stem powdery decoction pieces and preparation process thereof |
| CN105384851A (en) * | 2015-11-10 | 2016-03-09 | 军株（大连）生物产业有限公司 | Extraction method for producing inulin by cichorium intybus |
| CN106617115A (en) * | 2017-02-20 | 2017-05-10 | 湖南华诚生物资源股份有限公司 | Method for separating soluble dietary fibers from Momordica grosvenori production waste liquid |
| CN106674383A (en) * | 2016-12-30 | 2017-05-17 | 晨光生物科技集团股份有限公司 | Industrial method for rapidly and efficiently producing inulin |
| CN108467441A (en) * | 2018-04-25 | 2018-08-31 | 厦门欣赛科技有限公司 | A kind of inulin preparation method and preparation system |
| CN107602731B (en) * | 2017-10-09 | 2019-12-20 | 晨光生物科技集团股份有限公司 | Industrial production method for extracting inulin from jerusalem artichoke |
| CN110845550A (en) * | 2019-12-03 | 2020-02-28 | 中国科学院青岛生物能源与过程研究所 | Deep desalination and purification method of glycerol glucoside |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103923231A (en) * | 2014-04-18 | 2014-07-16 | 中国科学院烟台海岸带研究所 | Method for continuously preparing inulin and pectin by using jerusalem artichoke and/or endives |
| CN103923231B (en) * | 2014-04-18 | 2016-04-27 | 中国科学院烟台海岸带研究所 | A kind of method utilizing jerusalem artichoke and/or witloof continuous production inulin and pectin |
| CN104987434A (en) * | 2015-07-15 | 2015-10-21 | 中国科学院烟台海岸带研究所 | Method for extracting inulin by medium-low-temperature water |
| CN105384851A (en) * | 2015-11-10 | 2016-03-09 | 军株（大连）生物产业有限公司 | Extraction method for producing inulin by cichorium intybus |
| CN105193894A (en) * | 2015-11-14 | 2015-12-30 | 芜湖天成普阳中药科技有限公司 | Freshly squeezed vacuum drying cholla stem powdery decoction pieces and preparation process thereof |
| CN106674383A (en) * | 2016-12-30 | 2017-05-17 | 晨光生物科技集团股份有限公司 | Industrial method for rapidly and efficiently producing inulin |
| CN106674383B (en) * | 2016-12-30 | 2019-05-14 | 晨光生物科技集团股份有限公司 | A kind of industrial method quickly, efficiently producing inulin |
| CN106617115A (en) * | 2017-02-20 | 2017-05-10 | 湖南华诚生物资源股份有限公司 | Method for separating soluble dietary fibers from Momordica grosvenori production waste liquid |
| CN107602731B (en) * | 2017-10-09 | 2019-12-20 | 晨光生物科技集团股份有限公司 | Industrial production method for extracting inulin from jerusalem artichoke |
| CN108467441A (en) * | 2018-04-25 | 2018-08-31 | 厦门欣赛科技有限公司 | A kind of inulin preparation method and preparation system |
| CN110845550A (en) * | 2019-12-03 | 2020-02-28 | 中国科学院青岛生物能源与过程研究所 | Deep desalination and purification method of glycerol glucoside |
| CN110845550B (en) * | 2019-12-03 | 2021-03-19 | 中国科学院青岛生物能源与过程研究所 | Deep desalination and purification method of glycerol glucoside |
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