CN105213459A - A kind of Radix et Caulis Opuntiae Dillenii fresh squeezing lyophilization powder decoction pieces and preparation technology thereof - Google Patents
A kind of Radix et Caulis Opuntiae Dillenii fresh squeezing lyophilization powder decoction pieces and preparation technology thereof Download PDFInfo
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- CN105213459A CN105213459A CN201510774358.4A CN201510774358A CN105213459A CN 105213459 A CN105213459 A CN 105213459A CN 201510774358 A CN201510774358 A CN 201510774358A CN 105213459 A CN105213459 A CN 105213459A
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- radix
- caulis opuntiae
- opuntiae dillenii
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Abstract
The present invention discloses a kind of Radix et Caulis Opuntiae Dillenii fresh squeezing lyophilization powder decoction pieces and preparation technology thereof.This technique, after Radix et Caulis Opuntiae Dillenii medical material is gathered, to clean, drip washing, and takes advantage of fresh squeezing, leaching medicine juice.Medicinal residues add water stirring again, filter squeezing.Concentrating under reduced pressure after gained medicine juice merges, lyophilization, collects lyophilized products, after crushed vacuum packaging.The Radix et Caulis Opuntiae Dillenii powder decoction pieces that this legal system is standby, remains the polarity in medical material and nonpolar effective ingredient to greatest extent simultaneously.Decoction pieces is beneficial to accumulating, convenient adjustment, and quality controllable, curative effect is reliable, has great importance to guarantee tcm clinical curative effect.The promotion and implementation of this law, will have significant social meaning and economic benefit.
Description
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Chinese medicine Radix et Caulis Opuntiae Dillenii decoction pieces.
Background technology
Chinese medicine Radix et Caulis Opuntiae Dillenii is Cactaeous plants Radix et Caulis Opuntiae Dillenii
opuntiastricta(Haw.) Haw.var.
dillenii(Ker-Gawl.) the dry meat stem of Benson.This product has promoting flow of QI and blood, effect of heat-clearing and toxic substances removing.Be mainly used in dysentery, cough, acute mastitis, the treatment of scald etc.
The processing mode of common Radix et Caulis Opuntiae Dillenii decoction pieces is: after medical material is gathered, and removing impurity, is cut into block, dries, then accumulating of packing.This type of prepared herbal medicine in small pieces ready for decoction, bulky, Hygienic Index is poor, is easy to pollute and go mouldy, and quality is difficult to ensure, is unfavorable for that formula is adjusted and guarantees its clinical efficacy, even brings recessive harm to patient.In addition, because Radix et Caulis Opuntiae Dillenii is fleshy stem, be difficult to dry; And the Radix et Caulis Opuntiae Dillenii dried has much small thorn, can fly upward with the wind in atmosphere, be easy to be inhaled into, or prick skin and difficulty is found, bring to production and processing personnel and bother.Therefore, in order to ensure the safety of operator, also in order to clinical effective, the steady quality of Radix et Caulis Opuntiae Dillenii medical material, a kind of novel Radix et Caulis Opuntiae Dillenii decoction pieces and preparation technology thereof urgently develop.
Summary of the invention
The present invention discloses " a kind of Radix et Caulis Opuntiae Dillenii fresh squeezing lyophilization powder decoction pieces and preparation technology thereof ".This technique can retain polarity in Radix et Caulis Opuntiae Dillenii medical material and nonpolar effective ingredient to greatest extent, the loss of effective ingredient avoiding medical material to cause in existing decoction pieces processing and storage and transport process and the decline of medical material quanlity, reduce the pollution of medical material by mycete etc., the steady quality and clinical safety guaranteeing Radix et Caulis Opuntiae Dillenii decoction pieces is effectively had great importance.
To achieve these goals, technical scheme of the present invention is:
Gather its herb collection period at Radix et Caulis Opuntiae Dillenii, clean, after washing, take advantage of fresh squeezing, medicinal residues add the water of 1 ~ 5 times amount, and stir 5 ~ 30min, filter press filter pressing extracting juice, remaining medicinal residues squeeze extracting juice again, and merge three medicine juice, 40 ~ 120 mesh screen, obtain Radix et Caulis Opuntiae Dillenii medicine juice.The Radix et Caulis Opuntiae Dillenii medicine juice obtained is evaporated to the extractum that relative density is 1.05 ~ 1.25 under 40 ~ 75 DEG C of conditions, and this extractum is freezed 6 ~ 24 hours in-20 ~-80 DEG C of refrigerators, lyophilization again, pressure is 0.06 ~ 0.09MPa, and temperature is-15 ~-40 DEG C, and cooling time is 12 ~ 48 hours, after collecting lyophilized products, through pulverizing, sieving, packing.
On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, decoction pieces manufacturer, date of manufacture, Contents of Main Components, meridian distribution of property and flavor, function cure mainly, the information such as usage and dosage, toxic and side effects and contraindication.TLC distinguish collection of illustrative plates and/or the high-efficient liquid phase character collection of illustrative plates of Radix et Caulis Opuntiae Dillenii is enclosed, as " identity card " of product in bag.In addition, in the packaging bag of product, be printed on Quick Response Code, the information such as former plant photo, medical material photo, decoction pieces photo, character and the microscopical identification feature obtaining product can be linked by scanning.
Usefulness of the present invention is:
The Radix et Caulis Opuntiae Dillenii medical material of fresh collection, direct squeezing, filtration, concentrating under reduced pressure, lyophilization after cleaning washing, the powder decoction pieces obtained, can retain the effective ingredient in medical material to greatest extent.This decoction pieces volume compares to traditional decoction pieces volume and reduces widely, and vacuum packaging, makes prepared slice quality more stable, is beneficial to accumulating and clinical adjustment, has very significant social meaning and economic implications.
Detailed description of the invention
Embodiment 1
By the Radix et Caulis Opuntiae Dillenii medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add the tap water of 3 times amount, stir 20min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.Above-mentioned 3 medicine juice are merged, filters with 100 eye mesh screens.Filtrate reduced in volume, temperature is set as 65 DEG C.When concentrated gained extractum relative density is 1.15, extractum is freezed 6 hours in-80 DEG C of refrigerators.Take out east knot thing, lyophilization, pressure is 0.09Mpa, and temperature is-20 DEG C, dry 24 hours.Take out lyophilized products, pulverize at low temperature, cross 80 mesh sieves, moisture is not higher than 12%, and pack, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, labeling.
Embodiment 2
By the Radix et Caulis Opuntiae Dillenii medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add the tap water of 5 times amount, stir 30min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.Above-mentioned 3 medicine juice are merged, filters with 80 eye mesh screens.Filtrate reduced in volume, temperature is set as 70 DEG C.When concentrated gained extractum relative density is 1.10, extractum is freezed 8 hours in-80 DEG C of refrigerators.Take out east knot thing, lyophilization, pressure is 0.08Mpa, and temperature is-40 DEG C, dry 48 hours.Take out lyophilized products, pulverize at low temperature, cross 60 mesh sieves, moisture is not higher than 12%, and pack, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, labeling.
Above embodiment, is only the technological thought that this invention is described, can not limit the every technological thought proposed according to the present invention of protection scope of the present invention whereby, any change that technical scheme basis is done, all falls within the scope of protection of the invention.
Claims (2)
1. a Radix et Caulis Opuntiae Dillenii fresh squeezing lyophilization powder decoction pieces and preparation technology thereof, it is characterized in that: gather its herb collection period at Radix et Caulis Opuntiae Dillenii, clean, after washing, take advantage of fresh squeezing, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, filter press filter pressing extracting juice, remaining medicinal residues squeeze extracting juice again, merge three medicine juice, 60 ~ 120 mesh screen, obtain Radix et Caulis Opuntiae Dillenii medicine juice.
2. a kind of Radix et Caulis Opuntiae Dillenii according to claim 1 fresh squeezing lyophilization powder decoction pieces and preparation technology thereof, it is characterized in that: the Radix et Caulis Opuntiae Dillenii medicine juice obtained is evaporated to the extractum that relative density is 1.05 ~ 1.25 under 40 ~ 75 DEG C of conditions, and this extractum is freezed 6 ~ 24 hours in-20 ~-80 DEG C of refrigerators, then lyophilization, pressure is 0.06 ~ 0.09MPa, temperature is-15 ~-40 DEG C, cooling time is 12 ~ 48 hours, after collecting lyophilized products, through pulverizing, sieve, pack.
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| CN201510774358.4A CN105213459A (en) | 2015-11-14 | 2015-11-14 | A kind of Radix et Caulis Opuntiae Dillenii fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
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| CN201510774358.4A CN105213459A (en) | 2015-11-14 | 2015-11-14 | A kind of Radix et Caulis Opuntiae Dillenii fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105998130A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Folium Isatidis freshly-pressed lyophilized powdery decoction pieces and preparation process thereof |
| CN105998132A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Chinese lobelia freshly-squeezed freeze drying powder decoction tablets and preparation process thereof |
| CN105998395A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Herba Verbenae freshly squeezed freeze drying powder decoction piece and preparation technology thereof |
| CN106109545A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Euphorbiae Humifusae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
| CN106214741A (en) * | 2016-07-24 | 2016-12-14 | 徐漫 | A kind of Herba Scutellariae Barbatae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
| CN107213187A (en) * | 2017-06-20 | 2017-09-29 | 徐漫 | A kind of acalypha copperleaf is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107233385A (en) * | 2017-06-22 | 2017-10-10 | 徐漫 | A kind of motherwort is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107320582A (en) * | 2017-08-25 | 2017-11-07 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of Chinese violet |
| CN107375380A (en) * | 2017-08-25 | 2017-11-24 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of tussilago |
| CN107485646A (en) * | 2017-08-25 | 2017-12-19 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of mulberry leaf |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105998130A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Folium Isatidis freshly-pressed lyophilized powdery decoction pieces and preparation process thereof |
| CN105998132A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Chinese lobelia freshly-squeezed freeze drying powder decoction tablets and preparation process thereof |
| CN105998395A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Herba Verbenae freshly squeezed freeze drying powder decoction piece and preparation technology thereof |
| CN106109545A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Euphorbiae Humifusae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
| CN106214741A (en) * | 2016-07-24 | 2016-12-14 | 徐漫 | A kind of Herba Scutellariae Barbatae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
| CN107213187A (en) * | 2017-06-20 | 2017-09-29 | 徐漫 | A kind of acalypha copperleaf is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107233385A (en) * | 2017-06-22 | 2017-10-10 | 徐漫 | A kind of motherwort is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
| CN107320582A (en) * | 2017-08-25 | 2017-11-07 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of Chinese violet |
| CN107375380A (en) * | 2017-08-25 | 2017-11-24 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of tussilago |
| CN107485646A (en) * | 2017-08-25 | 2017-12-19 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of mulberry leaf |
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