CN106109624A - A kind of Herba Potentillae Discoloris fresh squeezing spray-dried powders decoction pieces and preparation technology thereof - Google Patents
A kind of Herba Potentillae Discoloris fresh squeezing spray-dried powders decoction pieces and preparation technology thereof Download PDFInfo
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- CN106109624A CN106109624A CN201610612451.XA CN201610612451A CN106109624A CN 106109624 A CN106109624 A CN 106109624A CN 201610612451 A CN201610612451 A CN 201610612451A CN 106109624 A CN106109624 A CN 106109624A
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- herba potentillae
- potentillae discoloris
- decoction pieces
- spray
- dried
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
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- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Veterinary Medicine (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Alternative & Traditional Medicine (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Medical Informatics (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of Herba Potentillae Discoloris fresh squeezing spray-dried powders decoction pieces and preparation technology thereof.This technique after Herba Potentillae Discoloris medical material is gathered, clean, drip washing, cutting, and take advantage of fresh squeezing, leaching medicine juice.Medicinal residues add water stirring, filter squeezing.Concentrating under reduced pressure after the merging of gained medicine juice, is spray-dried, and collects spray drying product, is vacuum-packed after crushed.Herba Potentillae Discoloris powder decoction pieces prepared by this method, remains the polarity in medical material and nonpolar effective ingredient to greatest extent.Decoction pieces is beneficial to accumulating, convenient adjustment, and quality controllable, curative effect is reliable, to ensureing that tcm clinical curative effect has great importance.The promotion and implementation of this law, will have significant social meaning and economic benefit.
Description
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Chinese medicine Herba Potentillae Discoloris decoction pieces.
Background technology
Chinese medicine Herba Potentillae Discoloris is Rosaceae potentilla plants Herba Potentillae DiscolorisPotentilla discolorBge. dry herb
Or aerial parts.This product heat-clearing and toxic substances removing, cooling blood for hemostasis, can be used to treat dysentery, diarrhoea, leucorrhea, malaria, have blood in stool, bloody dysentery stomachache,
The diseases such as bleeding hemorrhoids.
The processing mode of common Herba Potentillae Discoloris decoction pieces is: summer, season in autumn two gather, and removes impurity, dries, then accumulating of packing.
This type of prepared herbal medicine in small pieces ready for decoction, bulky, Hygienic Index is poor, easily pollutes and goes mouldy, quality it is difficult to ensure that, be unfavorable for that formula is adjusted
With guarantee its clinical efficacy, even to patient bring recessiveness harm.
At present, granule pieces market also having Herba Potentillae Discoloris medical material to make after extracting is sold.The preparation of granule pieces
Process, extracts not only time consumption and energy consumption, and because conventional substantial amounts of water does solvent, the nonpolar effective ingredient in medical material is difficult to be carried
Take out.Additionally, due to the Herba Potentillae Discoloris medical material extracted also is to be dried and through long-time storage, therefore, effective ingredient
Loss is also the biggest.In order to ensure Herba Potentillae Discoloris medical material clinical effectively, steady quality, a kind of novel Herba Potentillae Discoloris decoction pieces and
Preparation technology urgently develops.
Summary of the invention
The invention discloses " a kind of Herba Potentillae Discoloris fresh squeezing spray-dried powders decoction pieces and preparation technology thereof ".This technique is permissible
The polarity in Herba Potentillae Discoloris medical material and nonpolar effective ingredient is retained, it is to avoid medical material is processed at existing decoction pieces while to greatest extent
With loss and the decline of medical material quanlity of the effective ingredient caused in storage and transport process, reduce the medical material pollution by mycete etc., to really
Steady quality and the clinical safety of protecting Herba Potentillae Discoloris decoction pieces effectively have great importance.
To achieve these goals, the technical scheme is that
Gather its herb collection period in Herba Potentillae Discoloris, clean, washing, after cutting, take advantage of fresh squeezing.Gained medicinal residues add 1 ~ 5 times amount
Water, stir 5 ~ 30min, filter press filter pressing extracting juice.Remaining medicinal residues are squeezed extracting juice again.Merge three medicine juice, with 40 ~
120 mesh screen, obtain Herba Potentillae Discoloris medicine juice.The Herba Potentillae Discoloris medicine juice obtained is evaporated to relative density under the conditions of 40 ~ 75 DEG C
Being the concentrated solution of 1.02 ~ 1.15, and be spray-dried by this concentrated solution, intake air temperature is set as 90 ~ 140 DEG C, air outlet temperature
It is 80 ~ 110 DEG C, collects desciccate, cross 60 ~ 100 mesh sieves after pulverizing, be vacuum-packed.
On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, decoction pieces manufacturer, the date of manufacture,
The information such as Contents of Main Components, meridian distribution of property and flavor, function cure mainly, usage and dosage, toxic and side effects and contraindication.Herba Potentillae Discoloris is enclosed in Dai
Thin layer differentiate collection of illustrative plates and/or high-efficient liquid phase character collection of illustrative plates, as " identity card " of product.Additionally, in the packaging bag of product,
It is printed on Quick Response Code, the acquisition former plant photo of product, medical material photo, decoction pieces photo, character and micro-can be linked by scanning
The information such as diagnostic characteristics.
The invention have benefit that:
The Herba Potentillae Discoloris medical material of fresh collection, directly squeezes after cleaning washing, filters, concentrating under reduced pressure, spray drying, obtained powder
End decoction pieces, can retain the effective ingredient in medical material to greatest extent.This decoction pieces volume compares to tradition decoction pieces volume significantly
Ground reduces, vacuum packaging so that prepared slice quality is more stable, and beneficially accumulating and clinic is adjusted, and has very significantly society's meaning
Justice and economic implications.
Detailed description of the invention
Embodiment 1
By the Herba Potentillae Discoloris medical material of fresh collection, clean, wash silt with water, be cut into 3cm section, take advantage of using fresh herb squeezer squeezing extracting juice.
Gained medicinal residues add the tap water of 3 times amount, stir 20min, filter press squeezing extracting juice.Remaining medicinal residues squeeze with squeezer again
Extracting juice.Above-mentioned 3 medicine juice are merged, filters with 100 eye mesh screens.Filtrate reduced in volume, temperature is set as 65 DEG C.Concentrating gained
When extractum relative density is 1.05, being spray-dried, intake air temperature is 140 DEG C, and air outlet temperature is 100 DEG C, collects spray drying thing,
Low-temperature grinding, crosses 80 mesh sieves, and moisture is not higher than 12%, packs, 1kg/ bag, adds packed antioxidant and desiccant, vacuum seal
Dress, labeling.
Embodiment 2
By the Herba Potentillae Discoloris medical material of fresh collection, clean, wash silt with water, be cut into 6cm section, take advantage of using fresh herb squeezer squeezing extracting juice.
Gained medicinal residues add the tap water of 5 times amount, stir 30min, filter press squeezing extracting juice.Remaining medicinal residues squeeze with squeezer again
Extracting juice.Above-mentioned 3 medicine juice are merged, filters with 80 eye mesh screens.Filtrate reduced in volume, temperature is set as 70 DEG C.Concentrating gained
When extractum relative density is 1.10, being spray-dried, intake air temperature is 120 DEG C, and air outlet temperature is 90 DEG C, collects spray drying thing,
Low-temperature grinding, crosses 60 mesh sieves, and moisture is not higher than 12%, packs, 1kg/ bag, adds packed antioxidant and desiccant, vacuum seal
Dress, labeling.
Above example, is only the technological thought that this invention is described, it is impossible to limit protection scope of the present invention whereby all
It is the technological thought proposed according to the present invention, any change done on the basis of technical scheme, each fall within present invention protection
Within the scope of.
Claims (2)
1. a Herba Potentillae Discoloris fresh squeezing spray-dried powders decoction pieces and preparation technology thereof, it is characterised in that: adopt collection period in Herba Potentillae Discoloris
Collect its herb, clean, washing, after cutting, take advantage of fresh squeezing, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, filter press
Filter pressing extracting juice, remaining medicinal residues squeeze extracting juice again, merge three medicine juice, 40 ~ 120 mesh screen, obtain Herba Potentillae Discoloris medicine juice.
A kind of Herba Potentillae Discoloris fresh squeezing spray-dried powders decoction pieces the most according to claim 1 and preparation technology thereof, its feature exists
In: the Herba Potentillae Discoloris medicine juice obtained is evaporated under the conditions of 40 ~ 75 DEG C the concentrated solution that relative density is 1.02 ~ 1.15, and
Being spray-dried by this concentrated solution, intake air temperature is set as 90 ~ 140 DEG C, and air outlet temperature is 80 ~ 110 DEG C, collects to be dried and produces
Thing, crosses 60 ~ 100 mesh sieves, is vacuum-packed after pulverizing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610612451.XA CN106109624A (en) | 2016-07-31 | 2016-07-31 | A kind of Herba Potentillae Discoloris fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610612451.XA CN106109624A (en) | 2016-07-31 | 2016-07-31 | A kind of Herba Potentillae Discoloris fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
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| Publication Number | Publication Date |
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| CN106109624A true CN106109624A (en) | 2016-11-16 |
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| CN201610612451.XA Pending CN106109624A (en) | 2016-07-31 | 2016-07-31 | A kind of Herba Potentillae Discoloris fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107157934A (en) * | 2017-06-19 | 2017-09-15 | 徐漫 | A kind of Ilex Latifolia Thunb is fresh to squeeze spray-dried powders medicine materical crude slice and its preparation technology |
| CN107224456A (en) * | 2017-06-18 | 2017-10-03 | 徐漫 | A kind of wrinkled giant hyssop is fresh to squeeze spray-dried powders medicine materical crude slice and its preparation technology |
| CN107362180A (en) * | 2017-08-25 | 2017-11-21 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of lycopodium calvatum |
| CN107375541A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of field pennycress |
| CN107375565A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of pipewort |
| CN107441132A (en) * | 2017-08-25 | 2017-12-08 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of geranium wilfordii |
| CN107485645A (en) * | 2017-08-25 | 2017-12-19 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of mulberry leaf |
| CN107485638A (en) * | 2017-08-25 | 2017-12-19 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of lopseed |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105213450A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Taraxaci fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
-
2016
- 2016-07-31 CN CN201610612451.XA patent/CN106109624A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105213450A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Taraxaci fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107224456A (en) * | 2017-06-18 | 2017-10-03 | 徐漫 | A kind of wrinkled giant hyssop is fresh to squeeze spray-dried powders medicine materical crude slice and its preparation technology |
| CN107157934A (en) * | 2017-06-19 | 2017-09-15 | 徐漫 | A kind of Ilex Latifolia Thunb is fresh to squeeze spray-dried powders medicine materical crude slice and its preparation technology |
| CN107362180A (en) * | 2017-08-25 | 2017-11-21 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of lycopodium calvatum |
| CN107375541A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of field pennycress |
| CN107375565A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of pipewort |
| CN107441132A (en) * | 2017-08-25 | 2017-12-08 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of geranium wilfordii |
| CN107485645A (en) * | 2017-08-25 | 2017-12-19 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of mulberry leaf |
| CN107485638A (en) * | 2017-08-25 | 2017-12-19 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of lopseed |
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Application publication date: 20161116 |