CN106109596A - A kind of Herba Plantaginis is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof - Google Patents

A kind of Herba Plantaginis is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof Download PDF

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Publication number
CN106109596A
CN106109596A CN201610582888.3A CN201610582888A CN106109596A CN 106109596 A CN106109596 A CN 106109596A CN 201610582888 A CN201610582888 A CN 201610582888A CN 106109596 A CN106109596 A CN 106109596A
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China
Prior art keywords
herba plantaginis
decoction pieces
vacuum drying
fresh
preparation technology
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CN201610582888.3A
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Chinese (zh)
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徐自升
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Individual
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Individual
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Priority to CN201610582888.3A priority Critical patent/CN106109596A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/68Plantaginaceae (Plantain Family)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00Medicinal preparations characterised by special physical form
    • A61K9/14Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/13Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/17Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/31Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/39Complex extraction schemes, e.g. fractionation or repeated extraction steps
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/50Methods involving additional extraction steps
    • A61K2236/51Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Medical Informatics (AREA)
  • Botany (AREA)
  • Biotechnology (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses that a kind of Herba Plantaginis is fresh and squeeze vacuum drying powder decoction pieces and preparation technology thereof.This technique, after Herba Plantaginis medical material is gathered, cleans, drip washing, and takes advantage of fresh squeezing, leaching medicine juice.Medicinal residues add water stirring, filter squeezing.Concentrating under reduced pressure after the merging of gained medicine juice, vacuum drying, pulverize final vacuum packaging.Plantain Herb decoction pieces prepared by this method, remains the polarity in medical material and nonpolar effective ingredient to greatest extent.Decoction pieces is beneficial to accumulating, convenient adjustment, and quality controllable, curative effect is reliable, to ensureing that tcm clinical curative effect has great importance.The promotion and implementation of this law, will have significant social meaning and economic benefit.

Description

A kind of Herba Plantaginis is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Chinese medicine Herba Plantaginis decoction pieces.
Background technology
Chinese medicine Plantaginaceae plant Herba PlantaginisPlantago asiaticaOr Plantago depressa Willd L.Plantago depressa Willd. dry herb.This product has clearing away heat and promoting diuresis, eliminates the phlegm, removing heat from blood, effect of removing toxic substances.For the puckery pain of pyretic stranguria, edema oliguria, Diarrhea due to summer heat and dampness, phlegm-heat cough, hematemesis and epistaxis, carbuncle sore tumefacting virus etc..
The processing mode of conventional Herba Plantaginis decoction pieces is: summer excavates, and removes silt, dries, then accumulating of packing.This type of grass Medicine decoction pieces, bulky, Hygienic Index is poor, easily pollutes and goes mouldy, quality it is difficult to ensure that, be unfavorable for formula adjust and guarantee Its clinical efficacy, even brings the harm of recessiveness to patient.
At present, granule pieces market also having Herba Plantaginis medical material to make after extracting is sold.The preparation of granule pieces Process, extracts not only time consumption and energy consumption, and because conventional substantial amounts of water does solvent, the nonpolar effective ingredient in medical material is difficult to be carried Take out.Additionally, due to the Herba Plantaginis medical material extracted also is to be dried and through long-time storage, therefore, effective ingredient Loss is also the biggest.In order to ensure Herba Plantaginis medical material clinical effectively, steady quality, a kind of novel Herba Plantaginis decoction pieces and Preparation technology urgently develops.
Summary of the invention
The invention discloses " a kind of Herba Plantaginis is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof ".This technique is permissible The polarity in Herba Plantaginis medical material and nonpolar effective ingredient is retained, it is to avoid medical material is processed at existing decoction pieces while to greatest extent With loss and the decline of medical material quanlity of the effective ingredient caused in storage and transport process, reduce the medical material pollution by mycete etc., to really Steady quality and the clinical safety of protecting Herba Plantaginis decoction pieces effectively have great importance.
To achieve these goals, the technical scheme is that
Gather its herb collection period Herba Plantaginis, clean, after washing, take advantage of fresh squeezing.In medicinal residues after squeezing, add 1 ~ 5 times amount Water, stir 5 ~ 30min, with filter press filter pressing extracting juice.Remaining medicinal residues squeeze extracting juice again.Merge three medicine juice, with 40 ~ 120 mesh screen, obtain Herba Plantaginis medicine juice.The Herba Plantaginis medicine juice obtained is evaporated to relative density under the conditions of 40 ~ 75 DEG C Be the extractum of 1.05 ~ 1.30, and by its in 40 ~ 70 DEG C vacuum drying 4 ~ 8 hours after pulverized 60 ~ 120 mesh sieves, vacuum packaging, Obtain fresh squeezing of Herba Plantaginis and be vacuum dried powder decoction pieces.
On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, decoction pieces manufacturer, the date of manufacture, The information such as Contents of Main Components, meridian distribution of property and flavor, function cure mainly, usage and dosage, toxic and side effects and contraindication.The included upper Herba Plantaginis of bag Thin layer differentiate collection of illustrative plates and/or high-efficient liquid phase character collection of illustrative plates, as " identity card " of product.Additionally, in the packaging bag of product, It is printed on Quick Response Code, the acquisition former plant photo of product, medical material photo, decoction pieces photo, character and micro-can be linked by scanning The information such as diagnostic characteristics.
The invention have benefit that:
The Herba Plantaginis medical material of fresh collection, directly squeeze after cleaning washing, filter, concentrating under reduced pressure, vacuum drying, obtained powder End decoction pieces, can retain the effective ingredient in medical material to greatest extent.This decoction pieces volume compares to tradition decoction pieces volume significantly Ground reduces, vacuum packaging so that prepared slice quality is more stable, and beneficially accumulating and clinic is adjusted, and has very significantly society's meaning Justice and economic implications.
Detailed description of the invention
Embodiment 1
By the Herba Plantaginis medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add 3 The drinking water of times amount, stirs 20min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.By above-mentioned 3 times medicine juice merges, and filters with 100 eye mesh screens.Filtrate reduced in volume, temperature is set as 65 DEG C.Concentrating, gained extractum is the closeest When degree is 1.15, transfer in vacuum drying oven, be dried 8 hours in 60 DEG C, cross 60 mesh sieves, pack, 1kg/ bag after pulverizing, add Packed antioxidant and desiccant, Vacuum Package.
Embodiment 2
By the Herba Plantaginis medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add 5 The drinking water of times amount, stirs 30min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.By above-mentioned 3 times medicine juice merges, and filters with 80 eye mesh screens.Filtrate reduced in volume, temperature is set as 70 DEG C.Concentrating gained extractum relative density When being 1.10, transfer in vacuum drying oven, be dried 6 hours in 65 DEG C, cross 60 mesh sieves, pack, 1kg/ bag after pulverizing, add bag Dress antioxidant and desiccant, Vacuum Package.
Above example, is only the technological thought that this invention is described, it is impossible to limit protection scope of the present invention whereby all It is the technological thought proposed according to the present invention, any change done on the basis of technical scheme, each fall within present invention protection Within the scope of.

Claims (2)

1. fresh squeezing of Herba Plantaginis is vacuum dried powder decoction pieces and preparation technology thereof, it is characterised in that: adopt collection period Herba Plantaginis Collecting its herb, clean, after washing, take advantage of fresh squeezing, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, filter press filter pressing Extracting juice, remaining medicinal residues squeeze extracting juice again, merge three medicine juice, 40 ~ 120 mesh screen, obtain Herba Plantaginis medicine juice.
A kind of Herba Plantaginis the most according to claim 1 is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof, and its feature exists In: the Herba Plantaginis medicine juice obtained in claim 1 is evaporated under the conditions of 40 ~ 75 DEG C relative density is 1.05 ~ 1.30 Extractum, and by its in 40 ~ 70 DEG C vacuum drying 4 ~ 8 hours after pulverized 60 ~ 120 mesh sieves, vacuum packaging, obtain Herba Plantaginis fresh Squeeze vacuum drying powder decoction pieces.
CN201610582888.3A 2016-07-23 2016-07-23 A kind of Herba Plantaginis is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof Pending CN106109596A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610582888.3A CN106109596A (en) 2016-07-23 2016-07-23 A kind of Herba Plantaginis is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610582888.3A CN106109596A (en) 2016-07-23 2016-07-23 A kind of Herba Plantaginis is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof

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CN106109596A true CN106109596A (en) 2016-11-16

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107334814A (en) * 2017-08-25 2017-11-10 芜湖天成普阳中药科技有限公司 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Longtube Ground Ivy Herb
CN107375542A (en) * 2017-08-25 2017-11-24 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of field pennycress
CN107412473A (en) * 2017-08-25 2017-12-01 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of pipewort
CN107432884A (en) * 2017-08-25 2017-12-05 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Canton love-pea vine
CN107432883A (en) * 2017-08-25 2017-12-05 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of lopseed
CN107441149A (en) * 2017-08-25 2017-12-08 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of wolf's milk
CN107456473A (en) * 2017-08-25 2017-12-12 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of gerbera
CN107485653A (en) * 2017-08-25 2017-12-19 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of potentilla discolor

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105213451A (en) * 2015-11-14 2016-01-06 芜湖天成普阳中药科技有限公司 A kind of Herba Taraxaci fresh squeezing vacuum drying powder decoction pieces and preparation technology thereof

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105213451A (en) * 2015-11-14 2016-01-06 芜湖天成普阳中药科技有限公司 A kind of Herba Taraxaci fresh squeezing vacuum drying powder decoction pieces and preparation technology thereof

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107334814A (en) * 2017-08-25 2017-11-10 芜湖天成普阳中药科技有限公司 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Longtube Ground Ivy Herb
CN107375542A (en) * 2017-08-25 2017-11-24 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of field pennycress
CN107412473A (en) * 2017-08-25 2017-12-01 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of pipewort
CN107432884A (en) * 2017-08-25 2017-12-05 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Canton love-pea vine
CN107432883A (en) * 2017-08-25 2017-12-05 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of lopseed
CN107441149A (en) * 2017-08-25 2017-12-08 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of wolf's milk
CN107456473A (en) * 2017-08-25 2017-12-12 徐漫 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of gerbera
CN107485653A (en) * 2017-08-25 2017-12-19 徐自升 A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of potentilla discolor

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