CN105998209A - Plantain freshly-pressed spray-dried powdery detection pieces and preparation process thereof - Google Patents
Plantain freshly-pressed spray-dried powdery detection pieces and preparation process thereof Download PDFInfo
- Publication number
- CN105998209A CN105998209A CN201610582904.9A CN201610582904A CN105998209A CN 105998209 A CN105998209 A CN 105998209A CN 201610582904 A CN201610582904 A CN 201610582904A CN 105998209 A CN105998209 A CN 105998209A
- Authority
- CN
- China
- Prior art keywords
- herba plantaginis
- spray
- dried
- decoction pieces
- plantain
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/68—Plantaginaceae (Plantain Family)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/16—Agglomerates; Granulates; Microbeadlets ; Microspheres; Pellets; Solid products obtained by spray drying, spray freeze drying, spray congealing,(multiple) emulsion solvent evaporation or extraction
- A61K9/1605—Excipients; Inactive ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization
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- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Epidemiology (AREA)
- Medicinal Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Alternative & Traditional Medicine (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Medical Informatics (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses plantain freshly-pressed spray-dried powdery detection pieces and a preparation process thereof. The process includes: collecting plantain herb, cleaning and selecting, washing by spraying, pressing when it is fresh, and filtering to obtain decoction; adding water to residue, stirring, filtering, and pressing; combining decoctions, concentrating under reduced pressure, drying by spraying, collecting a spray-dried product, crushing, and packaging by vacuum. The plantain herb powdery decoction pieces enable polar and nonpolar effective ingredients in medicinal materials to be maximally retained; the decoction pieces are easy to store and transport, convenient to dose, controllable in quality and reliable in therapeutic effect and are significant in ensuring clinical therapeutic effects of traditional Chinese medicines. The process can be popularized to provide significant social meaning and economic benefit.
Description
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Chinese medicine Herba Plantaginis decoction pieces.
Background technology
Chinese medicine Plantaginaceae plant Herba PlantaginisPlantago asiaticaOr Plantago depressa Willd L.Plantago depressa
Willd. dry herb.This product has clearing away heat and promoting diuresis, eliminates the phlegm, removing heat from blood, effect of removing toxic substances.For the puckery pain of pyretic stranguria, edema oliguria,
Diarrhea due to summer heat and dampness, phlegm-heat cough, hematemesis and epistaxis, carbuncle sore tumefacting virus etc..
The processing mode of conventional Herba Plantaginis decoction pieces is: summer excavates, and removes silt, dries, then accumulating of packing.This type of grass
Medicine decoction pieces, bulky, Hygienic Index is poor, easily pollutes and goes mouldy, quality it is difficult to ensure that, be unfavorable for formula adjust and guarantee
Its clinical efficacy, even brings the harm of recessiveness to patient.
At present, granule pieces market also having Herba Plantaginis medical material to make after extracting is sold.The preparation of granule pieces
Process, extracts not only time consumption and energy consumption, and because conventional substantial amounts of water does solvent, the nonpolar effective ingredient in medical material is difficult to be carried
Take out.Additionally, due to the Herba Plantaginis medical material extracted also is to be dried and through long-time storage, therefore, effective ingredient
Loss is also the biggest.In order to ensure Herba Plantaginis medical material clinical effectively, steady quality, a kind of novel Herba Plantaginis decoction pieces and
Preparation technology urgently develops.
Summary of the invention
The invention discloses " a kind of Herba Plantaginis fresh squeezing spray-dried powders decoction pieces and preparation technology thereof ".This technique is permissible
The polarity in Herba Plantaginis medical material and nonpolar effective ingredient is retained, it is to avoid medical material is processed at existing decoction pieces while to greatest extent
With loss and the decline of medical material quanlity of the effective ingredient caused in storage and transport process, reduce the medical material pollution by mycete etc., to really
Steady quality and the clinical safety of protecting Herba Plantaginis decoction pieces effectively have great importance.
To achieve these goals, the technical scheme is that
Gather its herb collection period Herba Plantaginis, clean, after washing, take advantage of fresh squeezing.Gained medicinal residues add the water of 1 ~ 5 times amount,
Stirring 5 ~ 30min, filter press filter pressing extracting juice.Remaining medicinal residues are squeezed extracting juice again.Merge three medicine juice, with 40 ~ 120 mesh sieves
Filter, obtain Herba Plantaginis medicine juice.The Herba Plantaginis medicine juice obtained is evaporated under the conditions of 40 ~ 75 DEG C relative density be 1.02 ~
The concentrated solution of 1.15, and this concentrated solution is spray-dried, intake air temperature is set as 90 ~ 140 DEG C, and air outlet temperature is 80 ~ 110
DEG C, collect desciccate, cross 60 ~ 100 mesh sieves after pulverizing, be vacuum-packed.
On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, decoction pieces manufacturer, the date of manufacture,
The information such as Contents of Main Components, meridian distribution of property and flavor, function cure mainly, usage and dosage, toxic and side effects and contraindication.The included upper Herba Plantaginis of bag
Thin layer differentiate collection of illustrative plates and/or high-efficient liquid phase character collection of illustrative plates, as " identity card " of product.Additionally, in the packaging bag of product,
It is printed on Quick Response Code, the acquisition former plant photo of product, medical material photo, decoction pieces photo, character and micro-can be linked by scanning
The information such as diagnostic characteristics.
The invention have benefit that:
The Herba Plantaginis medical material of fresh collection, directly squeezes after cleaning washing, filters, concentrating under reduced pressure, spray drying, obtained powder
End decoction pieces, can retain the effective ingredient in medical material to greatest extent.This decoction pieces volume compares to tradition decoction pieces volume significantly
Ground reduces, vacuum packaging so that prepared slice quality is more stable, and beneficially accumulating and clinic is adjusted, and has very significantly society's meaning
Justice and economic implications.
Detailed description of the invention
Embodiment 1
By the Herba Plantaginis medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add 3
The tap water of times amount, stirs 20min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.By above-mentioned
3 times medicine juice merges, and filters with 100 eye mesh screens.Filtrate reduced in volume, temperature is set as 65 DEG C.Concentrating, gained extractum is the closeest
When degree is 1.05, being spray-dried, intake air temperature is 140 DEG C, and air outlet temperature is 100 DEG C, collection spray drying thing, low-temperature grinding,
Crossing 80 mesh sieves, moisture is not higher than 12%, packs, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, and labeling is i.e.
Can.
Embodiment 2
By the Herba Plantaginis medical material of fresh collection, clean, wash silt with water, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add 5
The tap water of times amount, stirs 30min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.By above-mentioned
3 times medicine juice merges, and filters with 80 eye mesh screens.Filtrate reduced in volume, temperature is set as 70 DEG C.Concentrating gained extractum relative density
When being 1.10, being spray-dried, intake air temperature is 120 DEG C, and air outlet temperature is 90 DEG C, collects spray drying thing, low-temperature grinding, crosses 60
Mesh sieve, moisture is not higher than 12%, packs, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, labeling.
Above example, is only the technological thought that this invention is described, it is impossible to limit protection scope of the present invention whereby all
It is the technological thought proposed according to the present invention, any change done on the basis of technical scheme, each fall within present invention protection
Within the scope of.
Claims (2)
1. a Herba Plantaginis fresh squeezing spray-dried powders decoction pieces and preparation technology thereof, it is characterised in that: adopt collection period Herba Plantaginis
Collecting its herb, clean, after washing, take advantage of fresh squeezing, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, filter press filter pressing
Extracting juice, remaining medicinal residues squeeze extracting juice again, merge three medicine juice, 40 ~ 120 mesh screen, obtain Herba Plantaginis medicine juice.
A kind of Herba Plantaginis fresh squeezing spray-dried powders decoction pieces the most according to claim 1 and preparation technology thereof, its feature exists
In: the Herba Plantaginis medicine juice obtained is evaporated under the conditions of 40 ~ 75 DEG C the concentrated solution that relative density is 1.02 ~ 1.15, and
Being spray-dried by this concentrated solution, intake air temperature is set as 90 ~ 140 DEG C, and air outlet temperature is 80 ~ 110 DEG C, collects to be dried and produces
Thing, crosses 60 ~ 100 mesh sieves, is vacuum-packed after pulverizing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610582904.9A CN105998209A (en) | 2016-07-23 | 2016-07-23 | Plantain freshly-pressed spray-dried powdery detection pieces and preparation process thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610582904.9A CN105998209A (en) | 2016-07-23 | 2016-07-23 | Plantain freshly-pressed spray-dried powdery detection pieces and preparation process thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105998209A true CN105998209A (en) | 2016-10-12 |
Family
ID=57117070
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610582904.9A Pending CN105998209A (en) | 2016-07-23 | 2016-07-23 | Plantain freshly-pressed spray-dried powdery detection pieces and preparation process thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105998209A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107157934A (en) * | 2017-06-19 | 2017-09-15 | 徐漫 | A kind of Ilex Latifolia Thunb is fresh to squeeze spray-dried powders medicine materical crude slice and its preparation technology |
| CN107362180A (en) * | 2017-08-25 | 2017-11-21 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of lycopodium calvatum |
| CN107375541A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of field pennycress |
| CN107375565A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of pipewort |
| CN107412304A (en) * | 2017-08-25 | 2017-12-01 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of eclipta |
| CN107485638A (en) * | 2017-08-25 | 2017-12-19 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of lopseed |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105213450A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Taraxaci fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
-
2016
- 2016-07-23 CN CN201610582904.9A patent/CN105998209A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105213450A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Taraxaci fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107157934A (en) * | 2017-06-19 | 2017-09-15 | 徐漫 | A kind of Ilex Latifolia Thunb is fresh to squeeze spray-dried powders medicine materical crude slice and its preparation technology |
| CN107362180A (en) * | 2017-08-25 | 2017-11-21 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of lycopodium calvatum |
| CN107375541A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of field pennycress |
| CN107375565A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of pipewort |
| CN107412304A (en) * | 2017-08-25 | 2017-12-01 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of eclipta |
| CN107485638A (en) * | 2017-08-25 | 2017-12-19 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of lopseed |
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20161012 |
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