CN105362528A - Folium Aloes fresh-squeezed spray-dried powder decoction pieces and preparation method thereof - Google Patents
Folium Aloes fresh-squeezed spray-dried powder decoction pieces and preparation method thereof Download PDFInfo
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- CN105362528A CN105362528A CN201510774370.5A CN201510774370A CN105362528A CN 105362528 A CN105362528 A CN 105362528A CN 201510774370 A CN201510774370 A CN 201510774370A CN 105362528 A CN105362528 A CN 105362528A
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- decoction pieces
- aloe
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- squeezed
- medicine
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/886—Aloeaceae (Aloe family), e.g. aloe vera
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
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- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses Folium aloes fresh-squeezed spray-dried powder decoction pieces and a preparation method thereof. In the process, Folium Aloes is purified, selected and washed after being harvested and is squeezed and filtered when it is fresh to obtain medicine juice; medicine residue is stirred with water and is filtered and squeezed; the medicine juices obtained are combined and concentrated under reduced pressure and are freeze-dried to obtain a freeze-dried product that is crushed and vacuum packaged. The Folium Aloes powder decoction pieces prepared by the method allow polar and non-polar effective ingredients in herbs to be retained to maximum extent; the decoction pieces are easy to storage and transport and convenient to dispense, have controllable quality and reliable therapeutic effect and are significant to ensuring traditional Chinese medicine clinical therapeutic effect. The popularization and implementation of the method has significant social implication and economic benefits.
Description
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Chinese medicine Aloe decoction pieces.
Background technology
Chinese medicine Aloe is liliaceous plant Aloe vulgaris
aloebarbadensisthe dry product of concentrated juice of Miller leaf.This product has relieving constipation by purgation, purging liver-fire, and parasite killing treats effect of infantile malnutrition, and for pyrolysis constipation, infantile convulsion is twitched, young waiter in a wineshop or an inn's infantile malnutrition, external treatment tinea skin ulcer etc.
The processing mode of conventional Aloe decoction pieces is: after being gathered by its leaf, remove crust, get its juice, decocting and concentrating forms.This method is long for heat time heating time, and comparatively large to the destruction of effective ingredient, finished product presents brownish black bulk.In addition, also containing a large amount of effective ingredient in the leaf skin abandoned.In order to ensure clinical effective, the steady quality of Aloe medical material, a kind of novel Aloe decoction pieces and preparation technology thereof urgently develop.
Summary of the invention
The present invention discloses " a kind of Aloe fresh squeezing spray-dried powders decoction pieces and preparation technology thereof ".This technique can retain polarity in Aloe medical material and nonpolar effective ingredient to greatest extent simultaneously, the loss of effective ingredient avoiding medical material to cause in existing decoction pieces processing and storage and transport process and the decline of medical material quanlity, reduce the pollution of medical material by mycete etc., the steady quality and clinical safety guaranteeing Aloe decoction pieces is effectively had great importance.
To achieve these goals, technical scheme of the present invention is:
Gather its meat blade collection period Aloe, clean, washing, after cutting, gross weight takes advantage of fresh squeezing.Add the water of 1 ~ 5 times amount in gained medicinal residues, stir 5 ~ 30min, filter press filter pressing extracting juice.Remaining medicinal residues are squeezed extracting juice again.Merge three medicine juice, with 40 ~ 120 mesh screen, obtain Aloe medicine juice.The Aloe medicine juice obtained is evaporated to the concentrated solution that relative density is 1.02 ~ 1.15 under 40 ~ 75 DEG C of conditions, and by this concentrated solution spraying dry, intake air temperature is set as 90 ~ 140 DEG C, air outlet temperature is 80 ~ 110 DEG C, collect desciccate, 60 ~ 100 mesh sieves are crossed, vacuum packaging after pulverizing.
On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, decoction pieces manufacturer, date of manufacture, Contents of Main Components, meridian distribution of property and flavor, function cure mainly, the information such as usage and dosage, toxic and side effects and contraindication.TLC distinguish collection of illustrative plates and/or the high-efficient liquid phase character collection of illustrative plates of Aloe is enclosed, as " identity card " of product in bag.In addition, in the packaging bag of product, be printed on Quick Response Code, the information such as former plant photo, medical material photo, decoction pieces photo, character and the microscopical identification feature obtaining product can be linked by scanning.
Usefulness of the present invention is:
The Aloe medical material of fresh collection, direct squeezing, filtration, concentrating under reduced pressure, spraying dry after cleaning washing, the powder decoction pieces obtained, can retain the effective ingredient in medical material to greatest extent.This decoction pieces volume compares to traditional decoction pieces volume and reduces widely, and vacuum packaging, makes prepared slice quality more stable, is beneficial to accumulating and clinical adjustment, has very significant social meaning and economic implications.
Detailed description of the invention
Embodiment 1
By the aloe leaf of fresh collection, clean, with water wash, be cut into the section of 5cm, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add the tap water of 3 times amount, stir 20min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.Above-mentioned 3 medicine juice are merged, filters with 100 eye mesh screens.Filtrate reduced in volume, temperature is set as 65 DEG C.When concentrated gained extractum relative density is 1.05, spraying dry, intake air temperature is 140 DEG C, and air outlet temperature is 100 DEG C, collects spray dry, pulverize at low temperature, crosses 80 mesh sieves, and moisture, not higher than 12%, packs, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, labeling.
Embodiment 2
By the Aloe medical material of fresh collection, clean, with water wash, be cut into the section of 3cm, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add the tap water of 5 times amount, stir 30min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.Above-mentioned 3 medicine juice are merged, filters with 80 eye mesh screens.Filtrate reduced in volume, temperature is set as 70 DEG C.When concentrated gained extractum relative density is 1.10, spraying dry, intake air temperature is 120 DEG C, and air outlet temperature is 90 DEG C, collects spray dry, pulverize at low temperature, crosses 60 mesh sieves, and moisture, not higher than 12%, packs, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, labeling.
Above embodiment, is only the technological thought that this invention is described, can not limit the every technological thought proposed according to the present invention of protection scope of the present invention whereby, any change that technical scheme basis is done, all falls within the scope of protection of the invention.
Claims (2)
1. an Aloe fresh squeezing spray-dried powders decoction pieces and preparation technology thereof, it is characterized in that: after the meat blade of Aloe is gathered, with water wash, cutting, take advantage of fresh squeezing, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, filter press filter pressing extracting juice, remaining medicinal residues squeeze extracting juice again, merge three medicine juice, 40 ~ 120 mesh screen, obtain Aloe medicine juice.
2. a kind of Aloe fresh squeezing spray-dried powders decoction pieces according to claim 1 and preparation technology thereof, it is characterized in that: the Aloe medicine juice obtained in claim 1 is evaporated to the concentrated solution that relative density is 1.02 ~ 1.15 under 40 ~ 75 DEG C of conditions, and by this concentrated solution spraying dry, intake air temperature is set as 90 ~ 140 DEG C, air outlet temperature is 80 ~ 110 DEG C, collect desciccate, cross 60 ~ 100 mesh sieves after pulverizing, vacuum packaging.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510774370.5A CN105362528A (en) | 2015-11-14 | 2015-11-14 | Folium Aloes fresh-squeezed spray-dried powder decoction pieces and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510774370.5A CN105362528A (en) | 2015-11-14 | 2015-11-14 | Folium Aloes fresh-squeezed spray-dried powder decoction pieces and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105362528A true CN105362528A (en) | 2016-03-02 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510774370.5A Pending CN105362528A (en) | 2015-11-14 | 2015-11-14 | Folium Aloes fresh-squeezed spray-dried powder decoction pieces and preparation method thereof |
Country Status (1)
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| CN (1) | CN105362528A (en) |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105998242A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Herba Agrimoniae freshly-pressed spray-dried powdery decoction pieces and preparation process thereof |
| CN105998131A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Chinese lobelia freshly-squeezed spray drying powder decoction tablets and preparation process thereof |
| CN105998108A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Folium Isatidis freshly-pressed spray-dried powdery decoction pieces and preparation process thereof |
| CN106109543A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Euphorbiae Humifusae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
| CN106109724A (en) * | 2016-07-23 | 2016-11-16 | 徐漫 | A kind of Herba Verbenae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
| CN107157934A (en) * | 2017-06-19 | 2017-09-15 | 徐漫 | A kind of Ilex Latifolia Thunb is fresh to squeeze spray-dried powders medicine materical crude slice and its preparation technology |
| CN107243019A (en) * | 2017-06-22 | 2017-10-13 | 徐漫 | A kind of motherwort is fresh to squeeze spray-dried powders medicine materical crude slice and its preparation technology |
| CN107320567A (en) * | 2017-08-25 | 2017-11-07 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of bittersweet |
| CN107375378A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of gerbera |
| CN107375397A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of fringed pink |
| CN107441136A (en) * | 2017-08-25 | 2017-12-08 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of eupatorium |
| CN107485645A (en) * | 2017-08-25 | 2017-12-19 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of mulberry leaf |
-
2015
- 2015-11-14 CN CN201510774370.5A patent/CN105362528A/en active Pending
Non-Patent Citations (1)
| Title |
|---|
| 孟胜男等: "《药剂学》", 30 September 2011 * |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105998242A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Herba Agrimoniae freshly-pressed spray-dried powdery decoction pieces and preparation process thereof |
| CN105998131A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Chinese lobelia freshly-squeezed spray drying powder decoction tablets and preparation process thereof |
| CN105998108A (en) * | 2016-07-23 | 2016-10-12 | 徐漫 | Folium Isatidis freshly-pressed spray-dried powdery decoction pieces and preparation process thereof |
| CN106109724A (en) * | 2016-07-23 | 2016-11-16 | 徐漫 | A kind of Herba Verbenae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
| CN106109543A (en) * | 2016-07-24 | 2016-11-16 | 徐漫 | A kind of Herba Euphorbiae Humifusae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof |
| CN107157934A (en) * | 2017-06-19 | 2017-09-15 | 徐漫 | A kind of Ilex Latifolia Thunb is fresh to squeeze spray-dried powders medicine materical crude slice and its preparation technology |
| CN107243019A (en) * | 2017-06-22 | 2017-10-13 | 徐漫 | A kind of motherwort is fresh to squeeze spray-dried powders medicine materical crude slice and its preparation technology |
| CN107320567A (en) * | 2017-08-25 | 2017-11-07 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of bittersweet |
| CN107375378A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of gerbera |
| CN107375397A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of fringed pink |
| CN107441136A (en) * | 2017-08-25 | 2017-12-08 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of eupatorium |
| CN107485645A (en) * | 2017-08-25 | 2017-12-19 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing spray-dried powders medicine materical crude slice of mulberry leaf |
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Application publication date: 20160302 |
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