CN105998395A - Herba Verbenae freshly squeezed freeze drying powder decoction piece and preparation technology thereof - Google Patents
Herba Verbenae freshly squeezed freeze drying powder decoction piece and preparation technology thereof Download PDFInfo
- Publication number
- CN105998395A CN105998395A CN201610582755.6A CN201610582755A CN105998395A CN 105998395 A CN105998395 A CN 105998395A CN 201610582755 A CN201610582755 A CN 201610582755A CN 105998395 A CN105998395 A CN 105998395A
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- China
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- herba verbenae
- preparation technology
- decoction piece
- powder decoction
- medicine juice
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- 238000004108 freeze drying Methods 0.000 title claims abstract description 13
- 238000005516 engineering process Methods 0.000 title claims abstract description 10
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 239000000843 powder Substances 0.000 title claims abstract description 8
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 20
- 239000003814 drug Substances 0.000 claims abstract description 14
- 230000008901 benefit Effects 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims abstract description 5
- 238000005406 washing Methods 0.000 claims abstract description 4
- 238000005520 cutting process Methods 0.000 claims abstract description 3
- 238000001816 cooling Methods 0.000 claims description 2
- 238000003825 pressing Methods 0.000 claims description 2
- 239000004615 ingredient Substances 0.000 abstract description 6
- 238000000034 method Methods 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 3
- 238000012856 packing Methods 0.000 abstract description 2
- 230000000717 retained effect Effects 0.000 abstract description 2
- 238000001914 filtration Methods 0.000 abstract 2
- 230000007012 clinical effect Effects 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 238000007710 freezing Methods 0.000 abstract 1
- 230000008014 freezing Effects 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 238000010298 pulverizing process Methods 0.000 abstract 1
- 239000012567 medical material Substances 0.000 description 13
- 239000000047 product Substances 0.000 description 8
- 239000003963 antioxidant agent Substances 0.000 description 2
- 230000003078 antioxidant effect Effects 0.000 description 2
- 239000002274 desiccant Substances 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 238000002372 labelling Methods 0.000 description 2
- 201000004792 malaria Diseases 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000004806 packaging method and process Methods 0.000 description 2
- 239000008399 tap water Substances 0.000 description 2
- 235000020679 tap water Nutrition 0.000 description 2
- 206010000077 Abdominal mass Diseases 0.000 description 1
- 201000000736 Amenorrhea Diseases 0.000 description 1
- 206010001928 Amenorrhoea Diseases 0.000 description 1
- 208000005171 Dysmenorrhea Diseases 0.000 description 1
- 206010013935 Dysmenorrhoea Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010023126 Jaundice Diseases 0.000 description 1
- 206010030113 Oedema Diseases 0.000 description 1
- 206010068319 Oropharyngeal pain Diseases 0.000 description 1
- 201000007100 Pharyngitis Diseases 0.000 description 1
- 241001073567 Verbenaceae Species 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 231100000540 amenorrhea Toxicity 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000002934 diuretic Substances 0.000 description 1
- 230000001882 diuretic effect Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 238000009461 vacuum packaging Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/85—Verbenaceae (Verbena family)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61J—CONTAINERS SPECIALLY ADAPTED FOR MEDICAL OR PHARMACEUTICAL PURPOSES; DEVICES OR METHODS SPECIALLY ADAPTED FOR BRINGING PHARMACEUTICAL PRODUCTS INTO PARTICULAR PHYSICAL OR ADMINISTERING FORMS; DEVICES FOR ADMINISTERING FOOD OR MEDICINES ORALLY; BABY COMFORTERS; DEVICES FOR RECEIVING SPITTLE
- A61J3/00—Devices or methods specially adapted for bringing pharmaceutical products into particular physical or administering forms
- A61J3/02—Devices or methods specially adapted for bringing pharmaceutical products into particular physical or administering forms into the form of powders
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/19—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles lyophilised, i.e. freeze-dried, solutions or dispersions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation or decoction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization
Landscapes
- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Chemical & Material Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
- Engineering & Computer Science (AREA)
- Epidemiology (AREA)
- Alternative & Traditional Medicine (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Medical Informatics (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a Herba Verbenae freshly squeezed freeze drying powder decoction piece and a preparation technology thereof. The preparation technology comprises the following steps: after Herba Verbenae is harvested, cleanly selecting, washing in a dripping manner and cutting into chunks, freshly squeezing, and filtering to obtain medicine juice; adding water in medicinal residues and stirring, filtering and squeezing; and merging the medicine juice, concentrating under reduced pressure, drying in a freezing manner, collecting a freeze-drying product, pulverizing the freeze-drying product, and packing under vacuum. In the Herba Verbenae powder decoction piece prepared by the method, polar and nonpolar effective ingredients in medicinal materials are retained to a maximum extent. The decoction piece is stored and conveyed conveniently, is convenient to adjust, controllable in quality and reliable in curative effect, and has important significance on guaranteeing of the traditional Chinese medicine clinical effects. If the preparation technology is popularized and implemented, social significance and economic benefit are remarkable.
Description
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Chinese medicine Herba Verbenae decoction pieces.
Background technology
Chinese medicine Herba Verbenae is Verbenaceae Herba VerbenaeVerbena officinalis L. dry aerial parts.This product has effect of promoting blood circulation to remove blood stasis, removing toxic substances, diuretic, jaundice eliminating, preventing the attack (or recurrence) of malaria, for the treatment of abdominal mass accumulation, dysmenorrhea amenorrhea, sore throat, edema, malaria etc..
The processing mode of conventional Herba Verbenae decoction pieces is: tap when 6 ~ August, the flowers are in blossom, removes impurity, dries, then accumulating of packing.This type of prepared herbal medicine in small pieces ready for decoction, bulky, Hygienic Index is poor, easily pollutes and goes mouldy, quality it is difficult to ensure that, be unfavorable for that formula is adjusted and guarantees its clinical efficacy, even bring the harm of recessiveness to patient.
At present, granule pieces market also having Herba Verbenae medical material to make after extracting is sold.The preparation process of granule pieces, extracts not only time consumption and energy consumption, and because conventional substantial amounts of water does solvent, the nonpolar effective ingredient in medical material is difficult to be extracted.Additionally, due to the Herba Verbenae medical material extracted also is to be dried and store through long-time, therefore, the loss of effective ingredient is also the biggest.In order to ensure clinical effective, the steady quality of Herba Verbenae medical material, a kind of novel Herba Verbenae decoction pieces and preparation technology thereof urgently develop.
Summary of the invention
The invention discloses " a kind of Herba Verbenae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof ".This technique can retain the polarity in Herba Verbenae medical material and nonpolar effective ingredient to greatest extent, avoid the loss of effective ingredient and the decline of medical material quanlity that medical material causes in the processing of existing decoction pieces and storage and transport process, the steady quality and clinical safety guaranteeing Herba Verbenae decoction pieces, by the pollution of mycete etc., is effectively had great importance by minimizing medical material.
To achieve these goals, the technical scheme is that
Gathering its herb collection period Herba Verbenae, clean, washing, after cutting, taking advantage of fresh squeezing, medicinal residues add the water of 1 ~ 5 times amount, stir 5 ~ 30min, filter press filter pressing extracting juice, remaining medicinal residues squeeze extracting juice again, merge three medicine juice, 40 ~ 120 mesh screen, obtain Herba Verbenae medicine juice.The Herba Verbenae medicine juice obtained is evaporated to the extractum that relative density is 1.05 ~ 1.25 under the conditions of 40 ~ 75 DEG C, and this extractum is freezed 6 ~ 24 hours in-20 ~-80 DEG C of refrigerators, lyophilization again, pressure is 0.06 ~ 0.09MPa, and temperature is-15 ~-40 DEG C, and cooling time is 12 ~ 48 hours, after collecting lyophilized products, size-reduced, sieve, pack.
On the label of product packaging bags, the information such as the name of an article in printing, medicinal part, planting site, decoction pieces manufacturer, date of manufacture, Contents of Main Components, meridian distribution of property and flavor, function cure mainly, usage and dosage, toxic and side effects and contraindication.The thin layer of the included upper Herba Verbenae of bag differentiates collection of illustrative plates and/or high-efficient liquid phase character collection of illustrative plates, as " identity card " of product.Additionally, in the packaging bag of product, be printed on Quick Response Code, the information such as former plant photo, medical material photo, decoction pieces photo, character and microscopical identification feature obtaining product can be linked by scanning.
The invention have benefit that:
The Herba Verbenae medical material of fresh collection, directly squeeze after cleaning washing, filter, concentrating under reduced pressure, lyophilization, obtained powder decoction pieces, the effective ingredient in medical material can be retained to greatest extent.This decoction pieces volume compares to tradition decoction pieces volume and is greatly reduced, vacuum packaging so that prepared slice quality is more stable, and beneficially accumulating and clinical adjustment, have the most significant social meaning and economic implications.
Detailed description of the invention
Embodiment 1
By the Herba Verbenae medical material of fresh collection, clean, wash silt with water, be cut into the section of 3cm, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add the tap water of 3 times amount, stir 20min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.Above-mentioned 3 medicine juice are merged, filters with 100 eye mesh screens.Filtrate reduced in volume, temperature is set as 65 DEG C.When concentrating gained extractum relative density and being 1.15, extractum is freezed in-80 DEG C of refrigerators 6 hours.Taking out east knot thing, lyophilization, pressure is 0.09Mpa, and temperature is-20 DEG C, is dried 24 hours.Taking out lyophilized products, low-temperature grinding, cross 80 mesh sieves, moisture is not higher than 12%, packs, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, labeling.
Embodiment 2
By the Herba Verbenae medical material of fresh collection, clean, wash silt with water, be cut into the section of 3cm, take advantage of using fresh herb squeezer squeezing extracting juice.Gained medicinal residues add the tap water of 5 times amount, stir 30min, filter press squeezing extracting juice.Remaining medicinal residues squeeze extracting juice with squeezer again.Above-mentioned 3 medicine juice are merged, filters with 80 eye mesh screens.Filtrate reduced in volume, temperature is set as 70 DEG C.When concentrating gained extractum relative density and being 1.10, extractum is freezed in-80 DEG C of refrigerators 8 hours.Taking out east knot thing, lyophilization, pressure is 0.08Mpa, and temperature is-40 DEG C, is dried 48 hours.Taking out lyophilized products, low-temperature grinding, cross 60 mesh sieves, moisture is not higher than 12%, packs, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, labeling.
Above example, is only the technological thought that this invention is described, it is impossible to limiting the every technological thought proposed according to the present invention of protection scope of the present invention whereby, any change done on the basis of technical scheme, within each falling within the scope of protection of the invention.
Claims (2)
1. a Herba Verbenae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof, it is characterised in that: gather its herb collection period Herba Verbenae, clean, washing, after cutting, taking advantage of fresh squeezing, medicinal residues add the water of 1 ~ 5 times amount, stirring 5 ~ 30min, filter press filter pressing extracting juice, remaining medicinal residues squeeze extracting juice again, merge three medicine juice, 40 ~ 120 mesh screen, obtain Herba Verbenae medicine juice.
A kind of Herba Verbenae fresh squeezing lyophilization powder decoction pieces the most according to claim 1 and preparation technology thereof, it is characterized in that: the Herba Verbenae medicine juice obtained is evaporated to the extractum that relative density is 1.05 ~ 1.25 under the conditions of 40 ~ 75 DEG C, and this extractum is freezed 6 ~ 24 hours in-20 ~-80 DEG C of refrigerators, then lyophilization, pressure is 0.06 ~ 0.09MPa, temperature is-15 ~-40 DEG C, cooling time is 12 ~ 48 hours, after collecting lyophilized products, size-reduced, sieve, pack.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610582755.6A CN105998395A (en) | 2016-07-23 | 2016-07-23 | Herba Verbenae freshly squeezed freeze drying powder decoction piece and preparation technology thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610582755.6A CN105998395A (en) | 2016-07-23 | 2016-07-23 | Herba Verbenae freshly squeezed freeze drying powder decoction piece and preparation technology thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105998395A true CN105998395A (en) | 2016-10-12 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610582755.6A Pending CN105998395A (en) | 2016-07-23 | 2016-07-23 | Herba Verbenae freshly squeezed freeze drying powder decoction piece and preparation technology thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN105998395A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107375564A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of pipewort |
| CN107412302A (en) * | 2017-08-25 | 2017-12-01 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of eclipta |
| CN107412291A (en) * | 2017-08-25 | 2017-12-01 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of geranium wilfordii |
| CN107441143A (en) * | 2017-08-25 | 2017-12-08 | 徐漫 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of gynostemma pentaphylla |
| CN107485660A (en) * | 2017-08-25 | 2017-12-19 | 芜湖天成普阳中药科技有限公司 | A kind of tangerine leaf is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105213552A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Hedyotidis Diffusae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
| CN105213661A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Aloe fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
| CN105213459A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Radix et Caulis Opuntiae Dillenii fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
| CN105213453A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Taraxaci fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
-
2016
- 2016-07-23 CN CN201610582755.6A patent/CN105998395A/en active Pending
Patent Citations (4)
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| CN105213552A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Hedyotidis Diffusae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
| CN105213661A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Aloe fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
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| CN105213453A (en) * | 2015-11-14 | 2016-01-06 | 芜湖天成普阳中药科技有限公司 | A kind of Herba Taraxaci fresh squeezing lyophilization powder decoction pieces and preparation technology thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107375564A (en) * | 2017-08-25 | 2017-11-24 | 徐漫 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of pipewort |
| CN107412302A (en) * | 2017-08-25 | 2017-12-01 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of eclipta |
| CN107412291A (en) * | 2017-08-25 | 2017-12-01 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of geranium wilfordii |
| CN107441143A (en) * | 2017-08-25 | 2017-12-08 | 徐漫 | A kind of fresh preparation technology for squeezing freeze-dried powder medicine materical crude slice of gynostemma pentaphylla |
| CN107485660A (en) * | 2017-08-25 | 2017-12-19 | 芜湖天成普阳中药科技有限公司 | A kind of tangerine leaf is fresh to squeeze freeze-dried powder medicine materical crude slice and its preparation technology |
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Application publication date: 20161012 |