CN103992469B - 聚碳酸酯及其成型物 - Google Patents
聚碳酸酯及其成型物 Download PDFInfo
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- CN103992469B CN103992469B CN201410244465.1A CN201410244465A CN103992469B CN 103992469 B CN103992469 B CN 103992469B CN 201410244465 A CN201410244465 A CN 201410244465A CN 103992469 B CN103992469 B CN 103992469B
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- polycarbonate
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- dihydroxy compound
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- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims abstract description 58
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims abstract description 29
- 235000019253 formic acid Nutrition 0.000 claims abstract description 29
- 238000006068 polycondensation reaction Methods 0.000 claims description 91
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 42
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 26
- 239000000203 mixture Substances 0.000 claims description 11
- 238000002844 melting Methods 0.000 claims description 10
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- 150000005690 diesters Chemical class 0.000 claims description 3
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- 238000003756 stirring Methods 0.000 description 101
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- 229960002479 isosorbide Drugs 0.000 description 59
- KLDXJTOLSGUMSJ-JGWLITMVSA-N Isosorbide Chemical compound O[C@@H]1CO[C@@H]2[C@@H](O)CO[C@@H]21 KLDXJTOLSGUMSJ-JGWLITMVSA-N 0.000 description 54
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- 239000007864 aqueous solution Substances 0.000 description 11
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 11
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- 125000001931 aliphatic group Chemical group 0.000 description 7
- FJDQFPXHSGXQBY-UHFFFAOYSA-L caesium carbonate Chemical compound [Cs+].[Cs+].[O-]C([O-])=O FJDQFPXHSGXQBY-UHFFFAOYSA-L 0.000 description 7
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- NNBZCPXTIHJBJL-UHFFFAOYSA-N decalin Chemical compound C1CCCC2CCCCC21 NNBZCPXTIHJBJL-UHFFFAOYSA-N 0.000 description 5
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- 150000003839 salts Chemical class 0.000 description 5
- QPFMBZIOSGYJDE-UHFFFAOYSA-N 1,1,2,2-tetrachloroethane Chemical compound ClC(Cl)C(Cl)Cl QPFMBZIOSGYJDE-UHFFFAOYSA-N 0.000 description 4
- HEDRZPFGACZZDS-MICDWDOJSA-N Trichloro(2H)methane Chemical compound [2H]C(Cl)(Cl)Cl HEDRZPFGACZZDS-MICDWDOJSA-N 0.000 description 4
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- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 3
- 238000005160 1H NMR spectroscopy Methods 0.000 description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 3
- JKIJEFPNVSHHEI-UHFFFAOYSA-N Phenol, 2,4-bis(1,1-dimethylethyl)-, phosphite (3:1) Chemical compound CC(C)(C)C1=CC(C(C)(C)C)=CC=C1OP(OC=1C(=CC(=CC=1)C(C)(C)C)C(C)(C)C)OC1=CC=C(C(C)(C)C)C=C1C(C)(C)C JKIJEFPNVSHHEI-UHFFFAOYSA-N 0.000 description 3
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- RVIZJROSQMQZCG-UHFFFAOYSA-N adamantane-1,2-diol Chemical compound C1C(C2)CC3CC1C(O)C2(O)C3 RVIZJROSQMQZCG-UHFFFAOYSA-N 0.000 description 3
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- 125000004429 atom Chemical group 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- VTYYLEPIZMXCLO-UHFFFAOYSA-L calcium carbonate Substances [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 3
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- KLDXJTOLSGUMSJ-UNTFVMJOSA-N (3s,3ar,6s,6ar)-2,3,3a,5,6,6a-hexahydrofuro[3,2-b]furan-3,6-diol Chemical compound O[C@H]1CO[C@@H]2[C@@H](O)CO[C@@H]21 KLDXJTOLSGUMSJ-UNTFVMJOSA-N 0.000 description 2
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- PDXRQENMIVHKPI-UHFFFAOYSA-N cyclohexane-1,1-diol Chemical compound OC1(O)CCCCC1 PDXRQENMIVHKPI-UHFFFAOYSA-N 0.000 description 2
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- UKMSUNONTOPOIO-UHFFFAOYSA-N docosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCC(O)=O UKMSUNONTOPOIO-UHFFFAOYSA-N 0.000 description 2
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- 125000000623 heterocyclic group Chemical group 0.000 description 2
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- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 description 2
- UQDUPQYQJKYHQI-UHFFFAOYSA-N methyl laurate Chemical compound CCCCCCCCCCCC(=O)OC UQDUPQYQJKYHQI-UHFFFAOYSA-N 0.000 description 2
- 239000012046 mixed solvent Substances 0.000 description 2
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- IPJIKGJKMCILGV-UHFFFAOYSA-N imidazo[1,2-a]pyridin-6-ylboronic acid Chemical compound C1=C(B(O)O)C=CC2=NC=CN21 IPJIKGJKMCILGV-UHFFFAOYSA-N 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
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- XUGNVMKQXJXZCD-UHFFFAOYSA-N isopropyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(C)C XUGNVMKQXJXZCD-UHFFFAOYSA-N 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- XIXADJRWDQXREU-UHFFFAOYSA-M lithium acetate Chemical compound [Li+].CC([O-])=O XIXADJRWDQXREU-UHFFFAOYSA-M 0.000 description 1
- 229940031993 lithium benzoate Drugs 0.000 description 1
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 description 1
- 229910052808 lithium carbonate Inorganic materials 0.000 description 1
- 229910000032 lithium hydrogen carbonate Inorganic materials 0.000 description 1
- 229910003002 lithium salt Inorganic materials 0.000 description 1
- 159000000002 lithium salts Chemical class 0.000 description 1
- HGPXWXLYXNVULB-UHFFFAOYSA-M lithium stearate Chemical compound [Li+].CCCCCCCCCCCCCCCCCC([O-])=O HGPXWXLYXNVULB-UHFFFAOYSA-M 0.000 description 1
- LDJNSLOKTFFLSL-UHFFFAOYSA-M lithium;benzoate Chemical compound [Li+].[O-]C(=O)C1=CC=CC=C1 LDJNSLOKTFFLSL-UHFFFAOYSA-M 0.000 description 1
- HQRPHMAXFVUBJX-UHFFFAOYSA-M lithium;hydrogen carbonate Chemical compound [Li+].OC([O-])=O HQRPHMAXFVUBJX-UHFFFAOYSA-M 0.000 description 1
- UEGPKNKPLBYCNK-UHFFFAOYSA-L magnesium acetate Chemical compound [Mg+2].CC([O-])=O.CC([O-])=O UEGPKNKPLBYCNK-UHFFFAOYSA-L 0.000 description 1
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- 235000011285 magnesium acetate Nutrition 0.000 description 1
- 229940069446 magnesium acetate Drugs 0.000 description 1
- QWDJLDTYWNBUKE-UHFFFAOYSA-L magnesium bicarbonate Chemical compound [Mg+2].OC([O-])=O.OC([O-])=O QWDJLDTYWNBUKE-UHFFFAOYSA-L 0.000 description 1
- 229910000022 magnesium bicarbonate Inorganic materials 0.000 description 1
- 239000002370 magnesium bicarbonate Substances 0.000 description 1
- 235000014824 magnesium bicarbonate Nutrition 0.000 description 1
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 239000001095 magnesium carbonate Substances 0.000 description 1
- 229910000021 magnesium carbonate Inorganic materials 0.000 description 1
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 description 1
- 239000000347 magnesium hydroxide Substances 0.000 description 1
- 229910001862 magnesium hydroxide Inorganic materials 0.000 description 1
- 159000000003 magnesium salts Chemical class 0.000 description 1
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- 230000014759 maintenance of location Effects 0.000 description 1
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- KPTPYMHWVGAEGG-UHFFFAOYSA-M methyl(triphenyl)azanium;hydroxide Chemical compound [OH-].C=1C=CC=CC=1[N+](C=1C=CC=CC=1)(C)C1=CC=CC=C1 KPTPYMHWVGAEGG-UHFFFAOYSA-M 0.000 description 1
- DNIAPMSPPWPWGF-UHFFFAOYSA-N monopropylene glycol Natural products CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 1
- ODKLEQPZOCJQMT-UHFFFAOYSA-N n,n-diethylpyridin-4-amine Chemical compound CCN(CC)C1=CC=NC=C1 ODKLEQPZOCJQMT-UHFFFAOYSA-N 0.000 description 1
- WLFOHIVICZSIKG-UHFFFAOYSA-N n,n-dimethyl-1h-imidazol-2-amine Chemical compound CN(C)C1=NC=CN1 WLFOHIVICZSIKG-UHFFFAOYSA-N 0.000 description 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
- RIWRFSMVIUAEBX-UHFFFAOYSA-N n-methyl-1-phenylmethanamine Chemical compound CNCC1=CC=CC=C1 RIWRFSMVIUAEBX-UHFFFAOYSA-N 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- SSDSCDGVMJFTEQ-UHFFFAOYSA-N octadecyl 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CCCCCCCCCCCCCCCCCCOC(=O)CCC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 SSDSCDGVMJFTEQ-UHFFFAOYSA-N 0.000 description 1
- AXRSHKZFNKUGQB-UHFFFAOYSA-N octyl diphenyl phosphite Chemical compound C=1C=CC=CC=1OP(OCCCCCCCC)OC1=CC=CC=C1 AXRSHKZFNKUGQB-UHFFFAOYSA-N 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
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- 235000019809 paraffin wax Nutrition 0.000 description 1
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- 235000019271 petrolatum Nutrition 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- SMIZARYCGYRDGF-UHFFFAOYSA-N phenyl dipropan-2-yl phosphite Chemical compound CC(C)OP(OC(C)C)OC1=CC=CC=C1 SMIZARYCGYRDGF-UHFFFAOYSA-N 0.000 description 1
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 1
- 235000021317 phosphate Nutrition 0.000 description 1
- 150000004714 phosphonium salts Chemical group 0.000 description 1
- XRBCRPZXSCBRTK-UHFFFAOYSA-N phosphonous acid Chemical compound OPO XRBCRPZXSCBRTK-UHFFFAOYSA-N 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
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- 229920002223 polystyrene Polymers 0.000 description 1
- 229920000166 polytrimethylene carbonate Polymers 0.000 description 1
- 235000011056 potassium acetate Nutrition 0.000 description 1
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- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 235000011181 potassium carbonates Nutrition 0.000 description 1
- TYJJADVDDVDEDZ-UHFFFAOYSA-M potassium hydrogencarbonate Chemical compound [K+].OC([O-])=O TYJJADVDDVDEDZ-UHFFFAOYSA-M 0.000 description 1
- 229940086066 potassium hydrogencarbonate Drugs 0.000 description 1
- 229940114930 potassium stearate Drugs 0.000 description 1
- ANBFRLKBEIFNQU-UHFFFAOYSA-M potassium;octadecanoate Chemical compound [K+].CCCCCCCCCCCCCCCCCC([O-])=O ANBFRLKBEIFNQU-UHFFFAOYSA-M 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 235000013772 propylene glycol Nutrition 0.000 description 1
- 229940093625 propylene glycol monostearate Drugs 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 238000001226 reprecipitation Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 235000003441 saturated fatty acids Nutrition 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 1
- 239000004299 sodium benzoate Substances 0.000 description 1
- 235000010234 sodium benzoate Nutrition 0.000 description 1
- 229960003885 sodium benzoate Drugs 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- HLBBKKJFGFRGMU-UHFFFAOYSA-M sodium formate Chemical compound [Na+].[O-]C=O HLBBKKJFGFRGMU-UHFFFAOYSA-M 0.000 description 1
- 235000019254 sodium formate Nutrition 0.000 description 1
- RYYKJJJTJZKILX-UHFFFAOYSA-M sodium octadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- LJFWQNJLLOFIJK-UHFFFAOYSA-N solvent violet 13 Chemical group C1=CC(C)=CC=C1NC1=CC=C(O)C2=C1C(=O)C1=CC=CC=C1C2=O LJFWQNJLLOFIJK-UHFFFAOYSA-N 0.000 description 1
- 239000001587 sorbitan monostearate Substances 0.000 description 1
- 235000011076 sorbitan monostearate Nutrition 0.000 description 1
- 229940035048 sorbitan monostearate Drugs 0.000 description 1
- 125000006850 spacer group Chemical group 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 229910000018 strontium carbonate Inorganic materials 0.000 description 1
- UUCCCPNEFXQJEL-UHFFFAOYSA-L strontium dihydroxide Chemical compound [OH-].[OH-].[Sr+2] UUCCCPNEFXQJEL-UHFFFAOYSA-L 0.000 description 1
- 229910001866 strontium hydroxide Inorganic materials 0.000 description 1
- 159000000008 strontium salts Chemical class 0.000 description 1
- WJMMDJOFTZAHHS-UHFFFAOYSA-L strontium;carbonic acid;carbonate Chemical compound [Sr+2].OC([O-])=O.OC([O-])=O WJMMDJOFTZAHHS-UHFFFAOYSA-L 0.000 description 1
- RXSHXLOMRZJCLB-UHFFFAOYSA-L strontium;diacetate Chemical compound [Sr+2].CC([O-])=O.CC([O-])=O RXSHXLOMRZJCLB-UHFFFAOYSA-L 0.000 description 1
- FRKHZXHEZFADLA-UHFFFAOYSA-L strontium;octadecanoate Chemical compound [Sr+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O FRKHZXHEZFADLA-UHFFFAOYSA-L 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
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- ISIJQEHRDSCQIU-UHFFFAOYSA-N tert-butyl 2,7-diazaspiro[4.5]decane-7-carboxylate Chemical compound C1N(C(=O)OC(C)(C)C)CCCC11CNCC1 ISIJQEHRDSCQIU-UHFFFAOYSA-N 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- 229940073455 tetraethylammonium hydroxide Drugs 0.000 description 1
- LRGJRHZIDJQFCL-UHFFFAOYSA-M tetraethylazanium;hydroxide Chemical compound [OH-].CC[N+](CC)(CC)CC LRGJRHZIDJQFCL-UHFFFAOYSA-M 0.000 description 1
- UWHCKJMYHZGTIT-UHFFFAOYSA-N tetraethylene glycol Chemical compound OCCOCCOCCOCCO UWHCKJMYHZGTIT-UHFFFAOYSA-N 0.000 description 1
- ZJKOMXZUJBYOOK-UHFFFAOYSA-M tetraphenylazanium;hydroxide Chemical compound [OH-].C1=CC=CC=C1[N+](C=1C=CC=CC=1)(C=1C=CC=CC=1)C1=CC=CC=C1 ZJKOMXZUJBYOOK-UHFFFAOYSA-M 0.000 description 1
- LPSKDVINWQNWFE-UHFFFAOYSA-M tetrapropylazanium;hydroxide Chemical compound [OH-].CCC[N+](CCC)(CCC)CCC LPSKDVINWQNWFE-UHFFFAOYSA-M 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 description 1
- BDZBKCUKTQZUTL-UHFFFAOYSA-N triethyl phosphite Chemical compound CCOP(OCC)OCC BDZBKCUKTQZUTL-UHFFFAOYSA-N 0.000 description 1
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 1
- RXJKFRMDXUJTEX-UHFFFAOYSA-N triethylphosphine Chemical compound CCP(CC)CC RXJKFRMDXUJTEX-UHFFFAOYSA-N 0.000 description 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 1
- IGNTWNVBGLNYDV-UHFFFAOYSA-N triisopropylphosphine Chemical compound CC(C)P(C(C)C)C(C)C IGNTWNVBGLNYDV-UHFFFAOYSA-N 0.000 description 1
- BJAARRARQJZURR-UHFFFAOYSA-N trimethylazanium;hydroxide Chemical compound O.CN(C)C BJAARRARQJZURR-UHFFFAOYSA-N 0.000 description 1
- HADKRTWCOYPCPH-UHFFFAOYSA-M trimethylphenylammonium hydroxide Chemical compound [OH-].C[N+](C)(C)C1=CC=CC=C1 HADKRTWCOYPCPH-UHFFFAOYSA-M 0.000 description 1
- CNUJLMSKURPSHE-UHFFFAOYSA-N trioctadecyl phosphite Chemical compound CCCCCCCCCCCCCCCCCCOP(OCCCCCCCCCCCCCCCCCC)OCCCCCCCCCCCCCCCCCC CNUJLMSKURPSHE-UHFFFAOYSA-N 0.000 description 1
- QOQNJVLFFRMJTQ-UHFFFAOYSA-N trioctyl phosphite Chemical compound CCCCCCCCOP(OCCCCCCCC)OCCCCCCCC QOQNJVLFFRMJTQ-UHFFFAOYSA-N 0.000 description 1
- XZZNDPSIHUTMOC-UHFFFAOYSA-N triphenyl phosphate Chemical compound C=1C=CC=CC=1OP(OC=1C=CC=CC=1)(=O)OC1=CC=CC=C1 XZZNDPSIHUTMOC-UHFFFAOYSA-N 0.000 description 1
- KCTAHLRCZMOTKM-UHFFFAOYSA-N tripropylphosphane Chemical compound CCCP(CCC)CCC KCTAHLRCZMOTKM-UHFFFAOYSA-N 0.000 description 1
- MGMXGCZJYUCMGY-UHFFFAOYSA-N tris(4-nonylphenyl) phosphite Chemical compound C1=CC(CCCCCCCCC)=CC=C1OP(OC=1C=CC(CCCCCCCCC)=CC=1)OC1=CC=C(CCCCCCCCC)C=C1 MGMXGCZJYUCMGY-UHFFFAOYSA-N 0.000 description 1
- QQBLOZGVRHAYGT-UHFFFAOYSA-N tris-decyl phosphite Chemical compound CCCCCCCCCCOP(OCCCCCCCCCC)OCCCCCCCCCC QQBLOZGVRHAYGT-UHFFFAOYSA-N 0.000 description 1
- DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
- PXXNTAGJWPJAGM-UHFFFAOYSA-N vertaline Natural products C1C2C=3C=C(OC)C(OC)=CC=3OC(C=C3)=CC=C3CCC(=O)OC1CC1N2CCCC1 PXXNTAGJWPJAGM-UHFFFAOYSA-N 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
- 239000013585 weight reducing agent Substances 0.000 description 1
- LRXTYHSAJDENHV-UHFFFAOYSA-H zinc phosphate Chemical class [Zn+2].[Zn+2].[Zn+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O LRXTYHSAJDENHV-UHFFFAOYSA-H 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/20—General preparatory processes
- C08G64/30—General preparatory processes using carbonates
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/13—Hollow or container type article [e.g., tube, vase, etc.]
- Y10T428/1352—Polymer or resin containing [i.e., natural or synthetic]
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyesters Or Polycarbonates (AREA)
- Liquid Crystal (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2007322491 | 2007-12-13 | ||
| JP2007-322490 | 2007-12-13 | ||
| JP2007322490 | 2007-12-13 | ||
| JP2007-322491 | 2007-12-13 | ||
| CN200880119869.0A CN101896535B (zh) | 2007-12-13 | 2008-12-10 | 聚碳酸酯的制造方法 |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200880119869.0A Division CN101896535B (zh) | 2007-12-13 | 2008-12-10 | 聚碳酸酯的制造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103992469A CN103992469A (zh) | 2014-08-20 |
| CN103992469B true CN103992469B (zh) | 2018-03-16 |
Family
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410244465.1A Active CN103992469B (zh) | 2007-12-13 | 2008-12-10 | 聚碳酸酯及其成型物 |
| CN200880119869.0A Active CN101896535B (zh) | 2007-12-13 | 2008-12-10 | 聚碳酸酯的制造方法 |
| CN201410244698.1A Active CN104017199B (zh) | 2007-12-13 | 2008-12-10 | 聚碳酸酯及其制造方法 |
Family Applications After (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200880119869.0A Active CN101896535B (zh) | 2007-12-13 | 2008-12-10 | 聚碳酸酯的制造方法 |
| CN201410244698.1A Active CN104017199B (zh) | 2007-12-13 | 2008-12-10 | 聚碳酸酯及其制造方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US8445624B2 (https=) |
| EP (3) | EP2952536B1 (https=) |
| JP (3) | JP4697295B2 (https=) |
| KR (1) | KR101285525B1 (https=) |
| CN (3) | CN103992469B (https=) |
| TW (3) | TWI428369B (https=) |
| WO (1) | WO2009075305A1 (https=) |
Families Citing this family (62)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5001110B2 (ja) * | 2007-10-04 | 2012-08-15 | 帝人株式会社 | ポリカーボネート樹脂およびその製造方法 |
| EP2952536B1 (en) * | 2007-12-13 | 2021-02-24 | Mitsubishi Chemical Corporation | Polycarbonate and molded article |
| CN103351463B (zh) * | 2008-11-28 | 2016-01-06 | 三菱化学株式会社 | 聚碳酸酯树脂、聚碳酸酯树脂组合物、光学膜和聚碳酸酯树脂成型品 |
| EP2371877B1 (en) * | 2008-11-28 | 2026-04-29 | Mitsubishi Chemical Corporation | Polycarbonate resin, polycarbonate resin composition, optical film, and polycarbonate resin molded article |
| US8399598B2 (en) * | 2009-04-16 | 2013-03-19 | Teijin Limited | Copolycarbonate and process for producing the same |
| CN103319706A (zh) * | 2009-11-30 | 2013-09-25 | 三菱化学株式会社 | 聚碳酸酯树脂及其制造方法 |
| JP5895339B2 (ja) * | 2009-12-11 | 2016-03-30 | 三菱化学株式会社 | ポリカーボネート樹脂 |
| JP5978554B2 (ja) * | 2009-12-22 | 2016-08-24 | 三菱化学株式会社 | ポリカーボネート樹脂組成物及び成形品 |
| JP5978555B2 (ja) * | 2010-01-07 | 2016-08-24 | 三菱化学株式会社 | ポリカーボネート樹脂組成物及びその成形品 |
| JP5966251B2 (ja) * | 2010-03-26 | 2016-08-10 | 三菱化学株式会社 | ポリカーボネート樹脂組成物及び成形品 |
| JP5502556B2 (ja) * | 2010-03-30 | 2014-05-28 | 大王製紙株式会社 | シリカ複合粒子の製造方法 |
| JP5486377B2 (ja) * | 2010-03-31 | 2014-05-07 | 大王製紙株式会社 | シリカ複合混合無機粒子の製造方法及びシリカ複合混合無機粒子 |
| ES2698840T3 (es) | 2010-04-14 | 2019-02-06 | Mitsubishi Chem Corp | Policarbonato diol, procedimiento para producir el mismo, y poliuretano y composición polimérica curable por radiación actínica ambos formados utilizando el mismo |
| US9018334B2 (en) | 2010-04-14 | 2015-04-28 | Dow Global Technologies Llc | Polycarbonate polyols and polyurethanes made therefrom |
| KR101801580B1 (ko) | 2010-05-27 | 2017-11-27 | 미쯔비시 케미컬 주식회사 | 폴리카보네이트 수지 및 그것으로 이루어지는 투명 필름 |
| JP2012067294A (ja) * | 2010-08-25 | 2012-04-05 | Mitsubishi Chemicals Corp | ポリカーボネート樹脂組成物及び成形品 |
| JP2012067287A (ja) * | 2010-08-26 | 2012-04-05 | Mitsubishi Chemicals Corp | 樹脂成形品 |
| JP5786556B2 (ja) * | 2010-08-26 | 2015-09-30 | 三菱化学株式会社 | 樹脂成形品の製造方法 |
| JP6044058B2 (ja) * | 2010-08-31 | 2016-12-14 | 三菱化学株式会社 | ポリカーボネート樹脂組成物及び成形品 |
| EP2662396B1 (en) * | 2011-01-07 | 2023-06-07 | Mitsubishi Chemical Corporation | Production method of polycarbonate |
| WO2012111718A1 (ja) * | 2011-02-16 | 2012-08-23 | 三菱化学株式会社 | ポリカーボネート樹脂組成物及び成形品 |
| JP5895581B2 (ja) * | 2011-02-16 | 2016-03-30 | 三菱化学株式会社 | ポリカーボネート樹脂組成物及び成形品 |
| CN103476828B (zh) * | 2011-03-30 | 2016-11-23 | 三菱化学株式会社 | 聚碳酸酯树脂的制造方法 |
| JP5987406B2 (ja) * | 2011-03-30 | 2016-09-07 | 三菱化学株式会社 | ポリカーボネート樹脂の製造方法 |
| KR101898306B1 (ko) * | 2011-03-30 | 2018-09-12 | 미쯔비시 케미컬 주식회사 | 폴리카보네이트 수지의 제조 방법 |
| JP5906887B2 (ja) * | 2011-03-30 | 2016-04-20 | 三菱化学株式会社 | ポリカーボネート樹脂の製造方法 |
| WO2012133855A1 (ja) * | 2011-03-31 | 2012-10-04 | 三菱化学株式会社 | ポリカーボネート樹脂の製造方法 |
| CN103476561B (zh) * | 2011-03-31 | 2017-03-08 | 三菱化学株式会社 | 聚碳酸酯树脂的制造方法、聚碳酸酯树脂、聚碳酸酯树脂制膜及聚碳酸酯树脂颗粒的制造方法 |
| WO2012133237A1 (ja) * | 2011-03-31 | 2012-10-04 | 三菱化学株式会社 | ポリカーボネート樹脂の製造方法、ポリカーボネート樹脂、ポリカーボネート樹脂フィルム、並びにポリカーボネート樹脂ペレットおよびポリカーボネート樹脂フィルムの製造方法 |
| JP5857852B2 (ja) * | 2011-03-31 | 2016-02-10 | 三菱化学株式会社 | ポリカーボネートの製造方法、ポリカーボネートペレットおよび透明フィルム |
| CN103459464B (zh) | 2011-03-31 | 2016-04-20 | 三菱化学株式会社 | 聚碳酸酯的制造方法以及聚碳酸酯颗粒 |
| WO2012133854A1 (ja) | 2011-03-31 | 2012-10-04 | 三菱化学株式会社 | ポリカーボネート樹脂の製造方法 |
| CN103459463B (zh) * | 2011-03-31 | 2015-09-30 | 三菱化学株式会社 | 聚碳酸酯的制造方法以及透明薄膜 |
| CN103562264B (zh) | 2011-05-30 | 2016-08-17 | 三菱化学株式会社 | 聚碳酸酯多元醇的制造方法及使用该聚碳酸酯多元醇的聚氨酯 |
| JP2013084584A (ja) * | 2011-09-30 | 2013-05-09 | Mitsubishi Chemicals Corp | Ｌｅｄ照明用部材 |
| JP2013103977A (ja) * | 2011-11-11 | 2013-05-30 | Mitsubishi Rayon Co Ltd | 重合体または重合体溶液の製造方法、重合体、重合体溶液 |
| TW201341424A (zh) * | 2011-12-28 | 2013-10-16 | Mitsubishi Gas Chemical Co | 高分子量聚碳酸酯樹脂之連續製造方法 |
| EP2818499B1 (en) | 2012-02-20 | 2022-01-12 | Mitsubishi Chemical Corporation | Resin composition and molded body of same |
| JP6167570B2 (ja) * | 2012-03-30 | 2017-07-26 | 三菱ケミカル株式会社 | 芳香族ポリカーボネートの製造方法及び製造設備 |
| JP2013209581A (ja) * | 2012-03-30 | 2013-10-10 | Mitsubishi Chemicals Corp | 成形体 |
| DE102012103296A1 (de) * | 2012-04-17 | 2013-10-17 | List Holding Ag | Verfahren zur Herstellung von Formkörpern |
| JP6213462B2 (ja) | 2012-05-18 | 2017-10-18 | 三菱瓦斯化学株式会社 | 高分子量ポリカーボネート樹脂の連続製造方法 |
| JP5974682B2 (ja) * | 2012-07-02 | 2016-08-23 | 三菱化学株式会社 | ポリカーボネートの製造方法 |
| JP2014080602A (ja) * | 2012-09-26 | 2014-05-08 | Mitsubishi Chemicals Corp | ポリカーボネート樹脂 |
| JP6179318B2 (ja) * | 2012-09-26 | 2017-08-16 | 三菱ケミカル株式会社 | ポリカーボネート樹脂の製造方法 |
| JP2014074106A (ja) * | 2012-10-03 | 2014-04-24 | Mitsubishi Chemicals Corp | ポリカーボネート樹脂の製造方法、ポリカーボネート樹脂ペレットおよび延伸フィルム |
| JP2014077059A (ja) * | 2012-10-10 | 2014-05-01 | Mitsubishi Chemicals Corp | ポリカーボネート樹脂の製造方法及びポリカーボネート樹脂の製造装置 |
| EP2915849B1 (en) * | 2012-11-05 | 2018-03-28 | Idemitsu Kosan Co., Ltd. | Polycarbonate resin composition and molded article |
| JP6154337B2 (ja) * | 2013-02-20 | 2017-06-28 | 帝人株式会社 | ポリカーボネート共重合体 |
| JP2015187204A (ja) * | 2014-03-26 | 2015-10-29 | 三菱化学株式会社 | ポリカーボネート樹脂からなる押出成形品 |
| JP5907232B2 (ja) * | 2014-10-20 | 2016-04-26 | 三菱化学株式会社 | ポリカーボネート樹脂 |
| JP6411882B2 (ja) * | 2014-12-16 | 2018-10-24 | 帝人株式会社 | ポリカーボネート樹脂の製造方法 |
| EP3120924A1 (en) * | 2015-07-24 | 2017-01-25 | Shell Internationale Research Maatschappij B.V. | Apparatus and process for relieving pressure in a chemical plant |
| CN105218802B (zh) * | 2015-10-15 | 2017-05-10 | 宁波浙铁大风化工有限公司 | 一种聚碳酸酯的合成工艺 |
| JP2016027182A (ja) * | 2015-11-16 | 2016-02-18 | 三菱化学株式会社 | ポリカーボネートの製造方法 |
| JP2017165892A (ja) * | 2016-03-17 | 2017-09-21 | 三菱ケミカル株式会社 | 透明樹脂フィルム |
| TWI813537B (zh) * | 2016-03-30 | 2023-09-01 | 日商三菱瓦斯化學股份有限公司 | 高分子量芳香族聚碳酸酯樹脂的製造方法 |
| CN108699229B (zh) * | 2016-03-30 | 2021-09-17 | 三菱瓦斯化学株式会社 | 高分子量芳香族聚碳酸酯树脂的制造方法 |
| JP6256540B2 (ja) * | 2016-07-08 | 2018-01-10 | 三菱ケミカル株式会社 | リソグラフィー用重合体またはリソグラフィー用重合体溶液の製造方法 |
| JP7323134B2 (ja) * | 2018-01-24 | 2023-08-08 | エスケー ケミカルズ カンパニー リミテッド | バイオベースポリカーボネートエステル及びその調製方法 |
| WO2019163964A1 (ja) * | 2018-02-23 | 2019-08-29 | 帝人株式会社 | ポリカーボネート樹脂及び製造方法 |
| JP2023039907A (ja) * | 2021-09-09 | 2023-03-22 | 三菱ケミカル株式会社 | ポリカーボネートポリオール組成物 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006028441A (ja) * | 2004-07-21 | 2006-02-02 | Teijin Ltd | 脂肪族ポリカーボネートからなる光学用フィルム |
| CN101448871A (zh) * | 2006-06-19 | 2009-06-03 | 三菱化学株式会社 | 聚碳酸酯共聚物及其制造方法 |
| CN101896536A (zh) * | 2007-12-12 | 2010-11-24 | 三菱化学株式会社 | 聚碳酸酯的制造方法和聚碳酸酯成型物 |
Family Cites Families (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1079686A (en) | 1963-05-17 | 1967-08-16 | Courtaulds Ltd | Polyesters |
| JPH0784515B2 (ja) | 1978-10-19 | 1995-09-13 | ビートライス・フーズ・カンパニー | ポリカーボネートの製造方法 |
| JPS5556124A (en) | 1978-10-19 | 1980-04-24 | Beatrice Foods Co | Manufacture of polycarbonate |
| DE2938464A1 (de) * | 1979-09-22 | 1981-04-09 | Bayer Ag, 5090 Leverkusen | Thermoplastische polycarbonate, ihre herstellung und ihre verwendung als formkoerper und folien |
| JPS6312896A (ja) | 1986-07-04 | 1988-01-20 | Hitachi Ltd | ロ−タリコンプレツサの製造方法 |
| JP3197359B2 (ja) * | 1992-08-19 | 2001-08-13 | 日本ジーイープラスチックス株式会社 | 芳香族ポリカーボネートの製造法 |
| JP3160209B2 (ja) * | 1996-01-30 | 2001-04-25 | 帝人株式会社 | オキサスピロウンデカン基を含有するポリカーボネート共重合体およびその製造法 |
| DE69607929T2 (de) | 1996-01-30 | 2001-01-18 | Teijin Ltd., Osaka | Polycarbonatcopolymer das Oxaspiroundecangruppe enthält und Verfahren zu seiner Herstellung |
| JPH10101787A (ja) * | 1996-09-30 | 1998-04-21 | Teijin Ltd | ポリカーボネートおよびその製造方法 |
| JP3530706B2 (ja) * | 1997-03-28 | 2004-05-24 | 三菱化学株式会社 | 芳香族ポリカーボネートの製造方法 |
| JP2989578B2 (ja) * | 1997-04-03 | 1999-12-13 | 旭化成工業株式会社 | 芳香族ポリカーボネートの製法 |
| WO2000041985A1 (en) * | 1999-01-11 | 2000-07-20 | E.I. Du Pont De Nemours And Company | Process and products of purification of anhydrosugar alcohols |
| JP3729681B2 (ja) * | 1999-06-11 | 2005-12-21 | 日本ジーイープラスチックス株式会社 | ポリカーボネートの製造方法 |
| JP3685971B2 (ja) * | 2000-01-17 | 2005-08-24 | 三菱化学株式会社 | 芳香族ポリカーボネートの製造方法 |
| JP3694434B2 (ja) * | 2000-02-15 | 2005-09-14 | 三菱化学株式会社 | 芳香族ポリカーボネートの製造方法 |
| FR2810040B1 (fr) * | 2000-06-09 | 2004-04-09 | Roquette Freres | Procede de purification d'une composition contenant au moins un produit de deshydratation interne d'un sucre hydrogene |
| EP1640400B1 (en) | 2003-06-16 | 2010-01-20 | Teijin Limited | Polycarbonate and process for producing the same |
| CN100432119C (zh) * | 2003-06-16 | 2008-11-12 | 帝人株式会社 | 聚碳酸酯及其制备方法 |
| US7138479B2 (en) * | 2003-12-31 | 2006-11-21 | General Electric Company | Aliphatic diol polycarbonates and their preparation |
| US7132498B2 (en) * | 2004-09-27 | 2006-11-07 | General Electric Company | Process to make polycarbonate from bismethylsalicylcarbonate (BMSC) |
| WO2006041190A1 (ja) * | 2004-10-14 | 2006-04-20 | Teijin Limited | 光弾性定数の低いポリカーボネート及びそれからなるフィルム |
| WO2007013463A1 (ja) | 2005-07-26 | 2007-02-01 | Ube Industries, Ltd. | ポリカーボネート及びその製造方法 |
| JP5032013B2 (ja) * | 2005-09-06 | 2012-09-26 | 帝人株式会社 | 植物由来成分を有するポリカーボネート樹脂組成物 |
| JP2007322490A (ja) | 2006-05-30 | 2007-12-13 | Seiko Epson Corp | 画像形成装置 |
| JP2007322491A (ja) | 2006-05-30 | 2007-12-13 | Seiko Epson Corp | 画像形成装置 |
| JP5532531B2 (ja) * | 2006-06-19 | 2014-06-25 | 三菱化学株式会社 | ポリカーボネート共重合体及びその製造方法 |
| US7906612B2 (en) * | 2006-09-01 | 2011-03-15 | Teijin Limited | Plant-derived component-containing polycarbonates and process for their production |
| JP2008291055A (ja) * | 2007-05-22 | 2008-12-04 | Teijin Ltd | 末端変性ポリカーボネート樹脂組成物 |
| EP2952536B1 (en) * | 2007-12-13 | 2021-02-24 | Mitsubishi Chemical Corporation | Polycarbonate and molded article |
-
2008
- 2008-12-10 EP EP15164014.1A patent/EP2952536B1/en active Active
- 2008-12-10 JP JP2008314922A patent/JP4697295B2/ja active Active
- 2008-12-10 CN CN201410244465.1A patent/CN103992469B/zh active Active
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- 2008-12-10 CN CN200880119869.0A patent/CN101896535B/zh active Active
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-
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- 2011-01-24 JP JP2011012174A patent/JP5857406B2/ja active Active
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006028441A (ja) * | 2004-07-21 | 2006-02-02 | Teijin Ltd | 脂肪族ポリカーボネートからなる光学用フィルム |
| CN101448871A (zh) * | 2006-06-19 | 2009-06-03 | 三菱化学株式会社 | 聚碳酸酯共聚物及其制造方法 |
| CN101896536A (zh) * | 2007-12-12 | 2010-11-24 | 三菱化学株式会社 | 聚碳酸酯的制造方法和聚碳酸酯成型物 |
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