CN101677538B - 制备高纯度D‑(‑)‑N,N‑二乙基‑2‑(α‑萘氧基)丙酰胺的方法 - Google Patents

制备高纯度D‑(‑)‑N,N‑二乙基‑2‑(α‑萘氧基)丙酰胺的方法 Download PDF

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Publication number
CN101677538B
CN101677538B CN200880014709.XA CN200880014709A CN101677538B CN 101677538 B CN101677538 B CN 101677538B CN 200880014709 A CN200880014709 A CN 200880014709A CN 101677538 B CN101677538 B CN 101677538B
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diethyl
propionamide
purity
reaction
alpha
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Chinese (zh)
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CN101677538A (zh
Inventor
拉吉尼坎塔·杰得夫·什罗夫
拉吉尼坎塔·维克拉姆·什罗夫
普拉首塔姆·娜仁扎·卡瑞姆贝卡
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UPL Ltd
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United Phosphorus Ltd
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/12—Preparation of carboxylic acid amides by reactions not involving the formation of carboxamide groups
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/02—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C233/04—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with carbon atoms of carboxamide groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C07C233/05—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with carbon atoms of carboxamide groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton having the nitrogen atoms of the carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C235/00—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms
    • C07C235/02—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms having carbon atoms of carboxamide groups bound to acyclic carbon atoms and singly-bound oxygen atoms bound to the same carbon skeleton
    • C07C235/04—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms having carbon atoms of carboxamide groups bound to acyclic carbon atoms and singly-bound oxygen atoms bound to the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C235/06—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms having carbon atoms of carboxamide groups bound to acyclic carbon atoms and singly-bound oxygen atoms bound to the same carbon skeleton the carbon skeleton being acyclic and saturated having the nitrogen atoms of the carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Dentistry (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Pest Control & Pesticides (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
CN200880014709.XA 2007-05-04 2008-05-05 制备高纯度D‑(‑)‑N,N‑二乙基‑2‑(α‑萘氧基)丙酰胺的方法 Active CN101677538B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
IN858MU2007 2007-05-04
IN858/MUM/2007 2007-05-04
PCT/IN2008/000284 WO2009004642A2 (en) 2007-05-04 2008-05-05 PROCESS FOR MANUFACTURE OF HIGH PURITY D-(-)-N, N-DIETHYL-2-(α- NAPHTHOXY) PROPIONAMIDE

Publications (2)

Publication Number Publication Date
CN101677538A CN101677538A (zh) 2010-03-24
CN101677538B true CN101677538B (zh) 2017-06-06

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CN200880014709.XA Active CN101677538B (zh) 2007-05-04 2008-05-05 制备高纯度D‑(‑)‑N,N‑二乙基‑2‑(α‑萘氧基)丙酰胺的方法

Country Status (11)

Country Link
US (1) US8309765B2 (https=)
EP (1) EP2146574B2 (https=)
JP (1) JP2010526059A (https=)
KR (3) KR101335861B1 (https=)
CN (1) CN101677538B (https=)
ES (1) ES2556230T5 (https=)
HU (1) HUE026533T2 (https=)
PL (1) PL2146574T5 (https=)
RU (1) RU2458047C2 (https=)
UA (1) UA103460C2 (https=)
WO (1) WO2009004642A2 (https=)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8557293B2 (en) * 2010-08-26 2013-10-15 Scott May Sunscreen compositions for application to plants
CN102887832B (zh) * 2012-09-29 2014-07-16 西安近代化学研究所 一种水相反应合成大位阻氯乙酰胺化合物的方法
US9307765B2 (en) * 2013-03-15 2016-04-12 Upl Limited Selective weed control using D-napropamide
TR201900984T4 (tr) * 2013-03-15 2019-02-21 Upl Ltd D-napropamid kullanılarak selektif yabani ot kontrolü.
JP2017533892A (ja) * 2014-10-03 2017-11-16 ピュラック バイオケム ビー． ブイ． Ｎ，ｎ−ジアルキルラクトアミドの製造法
CN106397240A (zh) * 2015-07-29 2017-02-15 国药集团化学试剂有限公司 2-卤代乙酰胺的合成方法
US20220071205A1 (en) 2018-12-21 2022-03-10 Upl Ltd Herbicide
CA3244493A1 (en) 2021-12-29 2023-07-06 UPL Corporation Limited HERBICIDE MIXTURES
WO2025012825A1 (en) 2023-07-11 2025-01-16 Upl Mauritius Limited Herbicide safener combinations and compositions
CN119504473B (zh) * 2024-11-22 2026-04-14 国网安徽省电力有限公司电力科学研究院 一种采用六氟化硫制备敌草胺的方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3718455A (en) * 1970-07-20 1973-02-27 Stauffer Chemical Co Method of combatting weeds with {60 -naphthoxy acetamides
US3998880A (en) * 1975-08-15 1976-12-21 Stauffer Chemical Company Production of N,N-diethyl 2(α-naphthoxy)propionamide
US4668628A (en) * 1985-04-01 1987-05-26 Stauffer Chemical Company Resolution of racemic mixtures of aliphatic acid esters
US4766220A (en) * 1979-06-29 1988-08-23 Rhone-Poulenc Agrochimie Process for the preparation of optically active aryloxyalkanoic acid compounds

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU102735A1 (ru) * 1952-06-14 1955-11-30 А.П. Арендарук Способ получени пара-нитро-альфа-ацетил-амино-бета-оксипропиофенона
US3480671A (en) * 1969-01-16 1969-11-25 Stauffer Chemical Co Alpha-naphthoxy acetamide compositions
US4358612A (en) 1981-01-02 1982-11-09 Stauffer Chemical Company Process for production of α-haloalkylamides
US4548641A (en) 1982-11-15 1985-10-22 Stauffer Chemical Company Herbicides: N,N-dialkyl-2-(4-substituted-1-naphthoxy) propionamides
DE3778359D1 (de) * 1987-07-07 1992-05-21 Rhone Poulenc Sante Verfahren zur herstellung von derivaten von pristinamycin iib.
JPH01168638A (ja) * 1987-12-25 1989-07-04 Mitsui Toatsu Chem Inc 光学活性２−クロロプロピオン酸の製造方法
CN1315868C (zh) * 2005-10-14 2007-05-16 邢将军 丙－谷二肽的制造方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3718455A (en) * 1970-07-20 1973-02-27 Stauffer Chemical Co Method of combatting weeds with {60 -naphthoxy acetamides
US3998880A (en) * 1975-08-15 1976-12-21 Stauffer Chemical Company Production of N,N-diethyl 2(α-naphthoxy)propionamide
US4766220A (en) * 1979-06-29 1988-08-23 Rhone-Poulenc Agrochimie Process for the preparation of optically active aryloxyalkanoic acid compounds
US4668628A (en) * 1985-04-01 1987-05-26 Stauffer Chemical Company Resolution of racemic mixtures of aliphatic acid esters

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Synthesis and herbicidal activity of N,N-diethyl-2-(1-naphthyloxy)propionamide and its optical isomers;James H. H. Chan et al.，;《J. Agric. Food Chem.》;19750531;第23卷(第5期);第1009页右栏第4段 *

Also Published As

Publication number Publication date
UA103460C2 (ru) 2013-10-25
WO2009004642A2 (en) 2009-01-08
EP2146574A4 (en) 2012-02-29
EP2146574B1 (en) 2015-11-04
RU2458047C2 (ru) 2012-08-10
US20100144532A1 (en) 2010-06-10
KR20130087610A (ko) 2013-08-06
ES2556230T3 (es) 2016-01-14
RU2009144977A (ru) 2011-06-10
CN101677538A (zh) 2010-03-24
KR20120055724A (ko) 2012-05-31
KR101174962B1 (ko) 2012-08-20
HUE026533T2 (en) 2016-06-28
JP2010526059A (ja) 2010-07-29
US8309765B2 (en) 2012-11-13
KR101335861B1 (ko) 2013-12-02
WO2009004642A3 (en) 2009-07-02
KR20090131679A (ko) 2009-12-29
PL2146574T5 (pl) 2023-06-12
PL2146574T3 (pl) 2016-03-31
EP2146574A2 (en) 2010-01-27
ES2556230T5 (es) 2023-01-04
EP2146574B2 (en) 2022-11-02

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