CN100346234C - 调色剂用聚酯树脂、静电荷像显影用调色剂及影像形成方法 - Google Patents
调色剂用聚酯树脂、静电荷像显影用调色剂及影像形成方法 Download PDFInfo
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- CN100346234C CN100346234C CNB2003801029793A CN200380102979A CN100346234C CN 100346234 C CN100346234 C CN 100346234C CN B2003801029793 A CNB2003801029793 A CN B2003801029793A CN 200380102979 A CN200380102979 A CN 200380102979A CN 100346234 C CN100346234 C CN 100346234C
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- G—PHYSICS
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- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/087—Binders for toner particles
- G03G9/08784—Macromolecular material not specially provided for in a single one of groups G03G9/08702 - G03G9/08775
- G03G9/08793—Crosslinked polymers
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
- C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
- C08G63/123—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds the acids or hydroxy compounds containing carbocyclic rings
- C08G63/127—Acids containing aromatic rings
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
- C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
- C08G63/40—Polyesters derived from ester-forming derivatives of polycarboxylic acids or of polyhydroxy compounds, other than from esters thereof
- C08G63/42—Cyclic ethers; Cyclic carbonates; Cyclic sulfites; Cyclic orthoesters
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
- C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
- C08G63/46—Polyesters chemically modified by esterification
- C08G63/48—Polyesters chemically modified by esterification by unsaturated higher fatty oils or their acids; by resin acids
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- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/087—Binders for toner particles
- G03G9/08742—Binders for toner particles comprising macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- G03G9/08755—Polyesters
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- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/087—Binders for toner particles
- G03G9/08775—Natural macromolecular compounds or derivatives thereof
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- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/087—Binders for toner particles
- G03G9/08784—Macromolecular material not specially provided for in a single one of groups G03G9/08702 - G03G9/08775
- G03G9/08795—Macromolecular material not specially provided for in a single one of groups G03G9/08702 - G03G9/08775 characterised by their chemical properties, e.g. acidity, molecular weight, sensitivity to reactants
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- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/087—Binders for toner particles
- G03G9/08784—Macromolecular material not specially provided for in a single one of groups G03G9/08702 - G03G9/08775
- G03G9/08797—Macromolecular material not specially provided for in a single one of groups G03G9/08702 - G03G9/08775 characterised by their physical properties, e.g. viscosity, solubility, melting temperature, softening temperature, glass transition temperature
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- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Medicinal Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Developing Agents For Electrophotography (AREA)
- Fixing For Electrophotography (AREA)
Abstract
Description
实施例 | 1 | 2 | 3 | 4 | 5 | 6 |
聚酯树脂 | A | B | C | D | E | F |
酸成分[摩尔%] | ||||||
歧化松香(1) | 23 | 30 | 30 | 30 | 23 | 23 |
对苯二甲酸(2) | 77 | 70 | 70 | 70 | 47 | 77 |
间苯二甲酸(2) | 30 | |||||
醇成分[摩尔%] | ||||||
新癸酸缩水甘油酯(3) | 13 | 20 | 20 | 20 | 13 | 8 |
新戊醇(4) | 100 | 70 | 93 | 93 | 100 | 70 |
乙二醇(4) | 30 | |||||
松香缩水甘油酯 | 5 | |||||
交联成分[摩尔%] | ||||||
偏苯三酸酐 | 25 | 22.5 | 22.5 | 22.5 | 25 | |
季戊四醇 | 8.5 | |||||
特性值 | ||||||
酸价[mgKOH/g] | 47.3 | 23.3 | 28.2 | 20.3 | 35.7 | 15.7 |
羟基价[mgKOH/g] | 0.3 | 8.0 | 6.8 | 9.6 | 2.1 | 12.1 |
Tg[℃] | 60.2 | 53.6 | 50.5 | 51.7 | 52.2 | 58.9 |
软化温度[℃] | 126.1 | 130.5 | 131.5 | 131.9 | 122.1 | 135.6 |
真密度[g/cm3] | 1.19 | 1.20 | 1.17 | 1.16 | 1.19 | 1.21 |
(1)/(2)0.2~0.6 | 0.30 | 0.43 | 0.43 | 0.43 | 0.30 | 0.30 |
(3)/(4)0.05~0.4 | 0.13 | 0.20 | 0.22 | 0.22 | 0.13 | 0.11 |
比较例 | 1 | 2 | 3 | 4 | 5 |
聚酯树脂 | G | H | I | J | K |
酸成分[摩尔%] | |||||
歧化松香(1) | 50 | 10 | 20 | 30 | 23 |
对苯二甲酸(2) | 50 | 90 | 80 | 70 | 77 |
醇成分[摩尔%] | |||||
新癸酸缩水甘油酯(3) | 5 | 13 | 40 | 13 | |
新戊醇(4) | 115 | 100 | 90 | 100 | |
BPA-EO2摩尔加成物 | 100 | ||||
交联成分[摩尔%] | |||||
偏苯三酸酐 | 25 | 22.5 | 25 | 25 | 25 |
特性值 | |||||
酸价[mgKOH/g] | 7.1 | 70.5 | 27.8 | 67.6 | 33.5 |
羟基价[mgKOH/g] | 33.3 | 5.6 | 18.9 | 0.1 | 0.3 |
Tg[℃] | 46.3 | 68.2 | 43.2 | 51.7 | 62.3 |
软化温度[℃] | 113.9 | 152.7 | 102.3 | 128.3 | 142.5 |
真密度[℃] | 1.15 | 1.21 | 1.09 | 1.23 | 1.32 |
(1)/(2)0.2~0.6 | 1.00 | 0.11 | 0.25 | 0.43 | 0.30 |
(3)/(4)0.05~0.4 | 0.04 | 0.13 | 0.44 | 0.00 | - |
实施例及比较例 | 聚酯树脂 | 带电量(μC/g) | 贮存稳定性 | 实际复印试验 | ||||||
影像浓度 | 泛白 | 消耗量(g/千张) | 定影性(%) | 偏移性 | ||||||
初期 | 1万张后 | 初期 | 1万张后 | |||||||
实施例7 | 聚酯树脂A | -15.5 | ○ | 1.41 | 1.42 | 1.3 | 1.2 | 40 | 90 | ○ |
实施例8 | 聚酯树脂B | -14.2 | ○ | 1.38 | 1.38 | 1.1 | 1.0 | 39 | 91 | ○ |
实施例9 | 聚酯树脂C | -14.0 | ○ | 1.35 | 1.37 | 1.1 | 0.7 | 39 | 88 | ○ |
实施例10 | 聚酯树脂A | -16.3 | ○ | 1.39 | 1.40 | 0.5 | 0.7 | 55 | 93 | ○ |
实施例11 | 聚酯树脂D | -15.2 | ○ | 1.36 | 1.36 | 0.1 | 0.3 | 53 | 89 | ○ |
实施例12 | 聚酯树脂E | -15.6 | ○ | 1.37 | 1.37 | 0.6 | 1.0 | 50 | 95 | ○ |
实施例13 | 聚酯树脂F | -30.0 | ○ | 1.45 | 1.41 | 0.8 | 1.0 | 27 | 98 | ○ |
比较例6 | 聚酯树脂G | -9.2 | △ | 1.22 | 1.25 | 0.3 | 0.5 | 33 | 95 | × |
比较例7 | 聚酯树脂H | -20.0 | ○ | 1.44 | 1.44 | 2.0 | 2.5 | 47 | 78 | ○ |
比较例8 | 聚酯树脂I | -14.5 | × | 1.36 | 1.37 | 1.0 | 0.9 | 40 | 97 | × |
比较例9 | 聚酯树脂J | -18.7 | ○ | 1.43 | 1.44 | 1.8 | 2.3 | 59 | 90 | ○ |
比较例10 | 聚酯树脂K | -15.6 | ○ | 1.40 | 1.40 | 1.2 | 1.1 | 50 | 86 | ○ |
Claims (8)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP374941/2002 | 2002-12-25 | ||
JP2002374941A JP3780254B2 (ja) | 2002-12-25 | 2002-12-25 | トナー用ポリエステル樹脂、静電荷像現像用トナーおよび画像形成方法 |
JP3749412002 | 2002-12-25 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1711506A CN1711506A (zh) | 2005-12-21 |
CN100346234C true CN100346234C (zh) | 2007-10-31 |
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Application Number | Title | Priority Date | Filing Date |
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CNB2003801029793A Expired - Fee Related CN100346234C (zh) | 2002-12-25 | 2003-12-16 | 调色剂用聚酯树脂、静电荷像显影用调色剂及影像形成方法 |
Country Status (8)
Country | Link |
---|---|
US (1) | US7569320B2 (zh) |
EP (1) | EP1580609B1 (zh) |
JP (1) | JP3780254B2 (zh) |
KR (1) | KR20050089164A (zh) |
CN (1) | CN100346234C (zh) |
AT (1) | ATE518167T1 (zh) |
TW (1) | TWI345141B (zh) |
WO (1) | WO2004059396A1 (zh) |
Families Citing this family (29)
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JP4609263B2 (ja) * | 2005-09-22 | 2011-01-12 | 富士ゼロックス株式会社 | 静電荷像現像用トナー、静電荷像現像剤、および画像形成方法 |
EP2012185B1 (en) * | 2006-04-21 | 2013-06-05 | Kao Corporation | Toner |
EP2012184B1 (en) * | 2006-04-21 | 2013-08-21 | Kao Corporation | Toner |
EP1873183A1 (en) * | 2006-06-30 | 2008-01-02 | DSMIP Assets B.V. | Branched polyester containing powder coating composition |
US8574808B2 (en) * | 2006-07-31 | 2013-11-05 | Kao Corporation | Resin emulsion |
JP5625230B2 (ja) * | 2007-10-19 | 2014-11-19 | 株式会社リコー | トナー、並び現像剤、及び画像形成装置 |
EP2051142B1 (en) * | 2007-10-19 | 2016-10-05 | Ricoh Company, Ltd. | Toner and image forming apparatus using it |
JP5124308B2 (ja) * | 2008-02-26 | 2013-01-23 | 株式会社リコー | トナー、該トナーを用いた現像剤、トナー入り容器、プロセスカートリッジ、及び画像形成方法 |
JP4712832B2 (ja) * | 2008-06-25 | 2011-06-29 | 株式会社沖データ | 現像剤、現像剤収容体、現像装置及び画像形成装置 |
JP5061052B2 (ja) * | 2008-07-11 | 2012-10-31 | 日本ユピカ株式会社 | トナー用ポリエステル樹脂及び静電荷現像用トナー |
EP2447241A1 (en) * | 2010-10-19 | 2012-05-02 | Momentive Specialty Chemicals Research Belgium | Glycidyl esters of alpha, alpha branched neononanoic acids, synthesis and uses |
PT2630113T (pt) * | 2010-10-19 | 2020-03-03 | Momentive Specialty Chemicals Res S A | Ésteres de glicidilo de ácidos neononanóicos alfa, alfaramificados, síntese e utilizações |
EP2476672A1 (en) * | 2010-12-22 | 2012-07-18 | Momentive Specialty Chemicals Research Belgium S.A. | Glycidyl esters of alpha , alpha branched acids compositions |
KR20130103610A (ko) | 2010-12-28 | 2013-09-23 | 캐논 가부시끼가이샤 | 토너 |
CN103019060B (zh) * | 2011-09-27 | 2017-10-20 | 富士施乐株式会社 | 调色剂、显影剂、调色剂盒、处理盒、成像装置和成像方法 |
WO2013056812A1 (en) | 2011-10-19 | 2013-04-25 | Momentive Specialty Chemicals Research Belgium Sa | Acrylic polyol resins compositions |
BR112014009484A8 (pt) * | 2011-10-19 | 2018-02-06 | Hexion Inc | Composição de resinas acrílicas com função hidroxila, processo para preparar uma composição, composição aglutinante, substrato de metal ou de plástico, poliol acrílico, resina de copolímero de poliol acrílico, e, composição de revestimento |
BR112014009504A2 (pt) * | 2011-10-19 | 2017-05-09 | Momentive Specialty Chem Inc | composição de resinas de poliol poliéter, processo para preparar uma composição, composição aglutinante, substrato de metal ou de plástico, e, resina de poliéster éter |
WO2013056814A2 (en) | 2011-10-19 | 2013-04-25 | Momentive Specialty Chemicals Research Beigium S.A. | Polyether polyol resins compositions |
WO2013056816A1 (en) * | 2011-10-19 | 2013-04-25 | Momentive Specialty Chemicals Research Belgium Sa | Polyester polyol resins compositions |
JP5938894B2 (ja) * | 2011-12-22 | 2016-06-22 | 富士ゼロックス株式会社 | ポリエステル樹脂、静電荷像現像用トナー、静電荷像現像剤、トナーカートリッジ、プロセスカートリッジ、画像形成装置及び画像形成方法 |
JP5891882B2 (ja) * | 2012-03-19 | 2016-03-23 | 富士ゼロックス株式会社 | トナー用ポリエステル樹脂、静電荷像現像用トナー、静電荷像現像剤、トナーカートリッジ、プロセスカートリッジ、画像形成装置及び画像形成方法 |
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US20150234305A1 (en) * | 2014-02-19 | 2015-08-20 | Fuji Xerox Co., Ltd. | Polyester resin for toner, toner for electrostatic charge image development, and toner cartridge |
CN104231239B (zh) * | 2014-09-01 | 2016-05-04 | 湖北鼎龙化学股份有限公司 | 聚酯组合物及其制造方法、粘合树脂和静电荷图像显影用调色剂 |
JP6690545B2 (ja) * | 2015-09-07 | 2020-04-28 | 三菱ケミカル株式会社 | トナーとその製造方法 |
JP2018185472A (ja) * | 2017-04-27 | 2018-11-22 | キヤノン株式会社 | トナー |
JP2019061042A (ja) * | 2017-09-26 | 2019-04-18 | 富士ゼロックス株式会社 | 画像形成装置 |
CN108914691B (zh) * | 2018-06-04 | 2020-12-22 | 杭州杭化哈利玛化工有限公司 | 一种食品纸用阳离子松香乳液施胶剂 |
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JP2001324832A (ja) | 2000-05-16 | 2001-11-22 | Sekisui Chem Co Ltd | トナー用樹脂組成物及びトナー |
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2002
- 2002-12-25 JP JP2002374941A patent/JP3780254B2/ja not_active Expired - Fee Related
-
2003
- 2003-12-16 EP EP03778940A patent/EP1580609B1/en not_active Expired - Lifetime
- 2003-12-16 US US10/540,270 patent/US7569320B2/en not_active Expired - Fee Related
- 2003-12-16 CN CNB2003801029793A patent/CN100346234C/zh not_active Expired - Fee Related
- 2003-12-16 WO PCT/JP2003/016064 patent/WO2004059396A1/ja active Application Filing
- 2003-12-16 AT AT03778940T patent/ATE518167T1/de not_active IP Right Cessation
- 2003-12-16 KR KR1020057012044A patent/KR20050089164A/ko not_active Application Discontinuation
- 2003-12-22 TW TW092136389A patent/TWI345141B/zh not_active IP Right Cessation
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Also Published As
Publication number | Publication date |
---|---|
EP1580609B1 (en) | 2011-07-27 |
US20060084001A1 (en) | 2006-04-20 |
US7569320B2 (en) | 2009-08-04 |
ATE518167T1 (de) | 2011-08-15 |
JP2004205822A (ja) | 2004-07-22 |
JP3780254B2 (ja) | 2006-05-31 |
TW200421054A (en) | 2004-10-16 |
WO2004059396A1 (ja) | 2004-07-15 |
EP1580609A4 (en) | 2009-07-22 |
TWI345141B (en) | 2011-07-11 |
CN1711506A (zh) | 2005-12-21 |
KR20050089164A (ko) | 2005-09-07 |
EP1580609A1 (en) | 2005-09-28 |
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