WO2005120240A1 - 発酵乳の製造法及び発酵乳 - Google Patents
発酵乳の製造法及び発酵乳 Download PDFInfo
- Publication number
- WO2005120240A1 WO2005120240A1 PCT/JP2005/011089 JP2005011089W WO2005120240A1 WO 2005120240 A1 WO2005120240 A1 WO 2005120240A1 JP 2005011089 W JP2005011089 W JP 2005011089W WO 2005120240 A1 WO2005120240 A1 WO 2005120240A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- fermentation
- fermented milk
- temperature
- fermented
- dissolved oxygen
- Prior art date
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/12—Fermented milk preparations; Treatment using microorganisms or enzymes
- A23C9/123—Fermented milk preparations; Treatment using microorganisms or enzymes using only microorganisms of the genus lactobacteriaceae; Yoghurt
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/12—Fermented milk preparations; Treatment using microorganisms or enzymes
- A23C9/13—Fermented milk preparations; Treatment using microorganisms or enzymes using additives
- A23C9/1307—Milk products or derivatives; Fruit or vegetable juices; Sugars, sugar alcohols, sweeteners; Oligosaccharides; Organic acids or salts thereof or acidifying agents; Flavours, dyes or pigments; Inert or aerosol gases; Carbonation methods
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C2240/00—Use or particular additives or ingredients
- A23C2240/20—Inert gas treatment, using, e.g. noble gases or CO2, including CO2 liberated by chemical reaction; Carbonation of milk products
Definitions
- the present invention relates to a novel method for producing fermented milk in which fermentation is promoted without using a fermentation promoting substance and the like, and a novel fermented milk obtained by the method.
- Fermented milk is milk or milk containing non-fat milk solids equivalent to or higher than this, fermented with lactic acid bacteria or yeast and converted into a paste or liquid, or frozen. it can.
- One is a pre-fermentation type and the other is a post-fermentation type.
- fermented milk that has been fermented and cooled in a tank before being packed into containers is crushed and filled into a flowable individual food container.
- a fermented milk raw material mix (hereinafter referred to as “mix”) to which a certain amount of starter has been added is filled into individual food containers for distribution, such as paper containers, and then fermented in a fermentation chamber until the lactic acid acidity reaches a predetermined value. After solidification, it is cooled.
- Pre-fermentation is often used in the production of fruit darts containing pulp and drinking darts, and post-fermentation is often used in the production of so-called hard and plain types.
- the fermentation process involves adding a starter to the sterilized mix at a specified temperature, fermenting until the acidity reaches a specified value, and cooling to stop the fermentation.
- the fermentation temperature and fermentation time at this time not only affect the production efficiency of the product, but also have a large effect on the flavor and quality, so the fermentation temperature and fermentation time are set appropriately while taking those effects into account. There is a need to. For example, if you want to give the product a mild flavor, lower the fermentation temperature.
- the problem here is that, for example, when the fermentation temperature is lowered to give the product a mellow flavor, the fermentation time required to reach the specified acidity is significantly extended, and the hardness of the tissue is increased. This means that there is a problem with production efficiency and product quality, such as the low hardness that cannot be obtained during the distribution process due to the low hardness. Therefore, It has been difficult to obtain fermented milk having a mellow flavor and a hardness structure that does not collapse during the distribution process without extending the fermentation time.
- the first is to improve the efficiency of the fermentation process and reduce the fermentation time. This is thought to enable fermentation at a lower fermentation temperature than usual, in addition to the purpose of improving production efficiency.
- Second a method of selecting lactic acid bacteria that produce a substance that imparts a mild flavor.
- Third instead of devising the fermentation process, there is a method of adding a texture that requires mellowness by adding an additive that improves flavor to the product.
- a method for promoting the first fermentation a method of adding a milk protein concentrate (Japanese Patent Application Laid-Open No.
- the description about fermentation temperature including the case where fermentation is performed at low temperature is generally Although it can be recognized, the tissue is smoother than before when the fermentation time is shortened when the dissolved oxygen is reduced, and when the fermentation is performed in a shorter time than when the dissolved oxygen concentration is not reduced by lowering the fermentation temperature. There is no indication that fermented milk with a texture can be obtained.
- the invention in this case relates to a method for improving fermented milk to which peroxidase is added, and does not relate to fermented milk which does not contain additives affecting the texture as in the case of obtaining Haad-O-Dart in the method of the present invention. . Disclosure of the invention
- An object of the present invention is to provide a method for producing fermented milk in which fermentation is promoted without adding a fermentation promoting substance and the fermentation time is shortened to improve productivity.
- fermented milk can be fermented at a lower temperature than before without increasing the fermentation time. It has been achieved with the task of providing new fermented milk obtained by the method.
- the present inventors have conducted intensive studies to solve the above-mentioned problems, and as a result, in the fermented milk production process, when the fermentation was performed in a state where the dissolved oxygen concentration of the mix at the start of fermentation was reduced, a fermentation promoting substance was obtained.
- the first problem was solved by finding that the rate of increase in lactic acidity by fermentation was increased, and the time required to reach the lactic acidity at the end of fermentation was significantly shortened, even though no additives such as were used. .
- Fermentation was conducted at a lower fermentation temperature than normal with the dissolved oxygen concentration of mittens further reduced.In this case, the fermentation was completed at a fermentation time that was almost the same as that at the normal fermentation temperature. Found to reach.
- the fermented milk obtained in this way has a dense and mellow flavor that is more than the mellow flavor of fermented milk that has been fermented at low temperatures for a long time. They found that the product manufactured in No. 1 was a new fermented milk with a hard structure that would not break down, even though it could not be realized in the distribution process, and thus solved the second problem.
- the present invention has found that in the fermented milk production process, the fermentation efficiency is improved by reducing the dissolved oxygen concentration of the mix at the start of fermentation, and the characteristics of the fermented milk are reduced by the fermentation time. It is possible to reduce the fermentation temperature and to lower the fermentation temperature than usual, and as a result, it has become possible to produce new fermented milk without the conventional method.
- performing fermentation at normal temperature while reducing the dissolved oxygen concentration of mittus provides an invention related to a method for producing fermented milk that shortens the fermentation time and improves productivity, and reduces the dissolved oxygen concentration of the mix.
- Lowering the fermentation temperature below normal in a reduced state yields fermented milk with a firm, firm texture that can withstand the distribution process while having a dense and mellow flavor that could not be obtained by conventional manufacturing methods
- an invention relating to a method for producing a fermented milk that has made it possible, and a novel fermented milk obtained as a result of using the method has been brought.
- the method for producing fermented milk of the present invention has the effect of improving the productivity by shortening the fermentation time without using additives such as fermentation promoting substances when the fermentation temperature is in a normal temperature range. If the fermentation temperature is lower than normal, the required acidity can be reached in almost the same fermentation time as usual, and the fermented milk thus obtained can be obtained by fermentation at conventional low temperatures for a long time.
- New fermented milk that has a denser, more mellow flavor compared to the products produced, and maintains the firmness of the tissue that is not available in conventional products, and provides fermented milk with new value. Has an effect.
- the fermented milk in the present invention refers to "fermented milk” defined by a ministerial ordinance such as yogurt and milk.
- the present invention is achieved by reducing the concentration of dissolved oxygen in a mix at the start of fermentation.
- a method of reducing dissolved oxygen a method such as membrane treatment or gas replacement is appropriately used.
- membrane treatments include ultrafiltration (UF) membrane treatment, reverse osmosis (RO) membrane treatment, and nanofiltration (NF) membrane with intermediate properties between the two.
- the treatment is used alone or in combination of two or more.
- gas replacement a method in which dissolved oxygen is replaced with an inert gas such as nitrogen gas is exemplified.
- an inert gas such as nitrogen gas
- replacement with an inert gas is performed after the mix is prepared or after the mix is sterilized. Or by adding the lactic acid bacteria starter to the mix and then immediately.
- Mixes are prepared by heating and dissolving milk ingredients such as milk, skim milk, skim milk powder and cream, sugars, sugars, flavors, water and other ingredients commonly used in the production of fermented milk, and using stabilizers.
- a stabilizer such as gelatin
- the obtained mix is homogenized, sterilized, and cooled to a predetermined temperature (fermentation temperature).
- a lactic acid bacteria starter is inoculated, and after stirring, in the case of pre-fermentation, filling is performed in a tank to start fermentation. After the fermentation, a sugar solution or the like may be added to these mixes.
- the replacement treatment with an inert gas may be performed from the stage of preparing the raw material mix to the time after inoculating the lactic acid bacteria starter and starting fermentation.
- the B period is optional. However, since it is important that the dissolved oxygen concentration is maintained at the beginning of fermentation, it is desirable to perform the inert gas replacement immediately before and after inoculating the lactic acid bacteria starter.
- the concentration that gives practically useful results is obtained when the temperature of Mittus is 30 ° C to 40 ° C. 5 ppm or less, preferably 3 ppm or less.
- the temperature of the Mittus when it is other than the above conditions, it may be evaluated by converting to the dissolved oxygen concentration when the mix is placed under the above conditions.
- Examples of the inert gas used in this effort include nitrogen gas, argon gas, and helium gas.
- Nitrogen gas can be more preferably used as an inert "raw gas" generally used in foods.
- known methods such as a method of bubbling the inert gas directly into the mix, a method using a static mixer, and a method in which the mixture is put into a mixer together with the mix and stirred are used. it can.
- Ratatobacillus pulgaricus L. bulgaricus
- Streptococcus' thermohuinoles S. the rmo philus
- other Ratato Bacillus Rakuteisu L. 1 actis
- a mixture of Bacillus bulgaricus and L. bulgaricus S. thermo phi 1 us
- a starter based on a starter can be suitably used.
- other lactic acid bacteria such as a bacterium belonging to the genus Ratatobacillus L. gasseri or Bifidobacterium may be added depending on the fermented milk to be obtained.
- the fermentation temperature and the like may be appropriately determined in consideration of the optimum conditions of each lactic acid bacterium when importance is placed on production efficiency.
- the optimum temperature in the case of using the above-mentioned mixed starter is from 40 ° C to 44 ° C, but the fermentation time is often extended at 40 ° C, and preferably from 43 ° C to 44 ° C.
- the fermentation time can be reduced from 80% of the normal case to about 70%. This effect can be recognized regardless of the fermentation type of “pre-fermentation” and “post-fermentation”.
- the fermentation temperature should be 30 ° C to 40 ° C, preferably 32 ° C to 39 ° C, more preferably 36 ° C to 39 ° C. Low temperature conditions may be selected. When the fermentation temperature is increased to 41 ° C or more, it is difficult to impart mellowness to the product, and the product will have the same texture as a normal product.
- the fermentation time varies depending on the dissolved oxygen concentration at the start of fermentation and the fermentation temperature.However, in the case of the present invention, when the dissolved oxygen concentration at the start of fermentation is 3 ppm or less, the conventional fermentation time is between 34 ° C and 35 ° C. It is possible to reach the target acidity in the same fermentation time as when fermenting at normal fermentation temperature. If the fermentation temperature is lowered to 30 ° C Although the fermentation time is longer than usual, even in this case, compared with the case where the present method is not performed,
- the fermentation can be completed in about 60% of the time, and the effect of the method of the present invention is clear.
- the fermented milk obtained under the low-temperature fermentation conditions of the present invention as described above can impart superior characteristics to products obtained by the conventional method, especially in the case of the post-fermentation type.
- the fermented milk has a more mellow flavor than fermented milk produced at normal fermentation temperatures. Can be obtained.
- the fermented milk fermented at a low temperature according to the present invention has a hard structure without disintegration at the distribution stage, which could not be realized by conventional fermented milk fermented at a low temperature for a long time. It has a mellow flavor, but has a solid structure, making it a new and useful fermenter.
- the method of the present invention when the method of the present invention is applied to the pre-fermentation type, there is a process of crushing and filling the obtained curd in the pre-fermentation, so that the fermented milk does not finally have a hard tissue, but the crushing is roughened.
- the fermentation time is shortened when the fermentation temperature is a normal temperature even in the pre-fermentation type.
- the mellowness and tissue hardness of the fermented milk having both the mellowness and the tissue hardness of the present invention are determined by the following values measured according to the measurement manual of Neocard Meter M302 (I Techno Engineering: Former Iio Electric). Physical property values can be represented.
- the ⁇ mellowness '' of fermented milk in the method of the present invention is evaluated by measuring the penetration angle of a card knife when a 100 g weight is applied at 5 to 10 ° C. it can. Specifically, based on the measurement curve represented by the bold line shown in Fig.
- the “hardness” in the present invention is defined as the “hardness” defined as the length B of a straight line connecting the intersection of the tangents 1 and 2 and the diagonal of the recording paper in FIG.
- test examples are given to examine the effect of dissolved oxygen concentration in the mix on the increase in lactic acidity (effect on fermentation time).
- Test Example 1 The relationship between the dissolved oxygen concentration in the mix at the start of fermentation and the increase in lactic acidity was determined.
- the mix adjusted to each dissolved oxygen concentration was filled into a 1 O Oml container, and allowed to stand still fermentation in a fermentation room at about 40 ° C.
- the lactic acid acidity reached about 0.7%, 10 ° C was reached.
- a fermentation without adjusting the dissolved oxygen concentration was used.
- the dissolved oxygen concentration of Mittus at the stage of inoculation with the lactic acid bacteria starter was 8 ppm.
- FIG. 2 shows the results of changes in lactic acidity during fermentation in Test Example 1 above.
- the concentration of dissolved oxygen in the mix during fermentation that is effective for shortening the fermentation time is 5 ppm or less, preferably 3 ppm or less.
- the product of the present invention is superior in fermented milk obtained by performing long-term fermentation at low temperatures in the past in terms of "smoothness of the tongue", “mellowness of taste” and “kokumi” Became clear. It was also clear that it had a mild flavor with a similar acidity and less sourness.
- the time from 0.4% to 0.7% of the target acidity is considered as the card forming time.
- the curd formation starts earlier even if the fermentation time is shorter than that of ordinary low-temperature fermentation as a whole, and as a result, the time required for curd formation is the highest among the three examined. You can see that a lot of time has been spent. Measurement of mildness and hardness of this force dense and mild give flavor to the product t Test Example 3 commercial product believed to have been one of the causes
- the penetration angle and hardness of the four types of curd knives were measured for the sale of plain yogurt and compared with the deoxidized fermented product of the present invention at 37 ° C for 3 hours. Table 3 shows the obtained results.
- the measurement of physical properties of Yogurt can be obtained by measuring the penetration angle of the Yogurt knife with a weight of 100 g using Neocard Meter-1 M302 (I-Techno Engineering, formerly Iio Electric). The elasticity up to the break of the penetration angle curve was defined as the hardness (g), and the angle was used as a measure of smoothness (the angle was a value up to 90 °, and the smaller the value, the smoother the tissue can be judged). If the hardness of jordart measured by this measuring instrument is 40 g or more, it can be said that it is a stable structure that is not crushed by impact during transportation. Relationship between mellowness and hardness of commercial products
- Example 1 Production of pre-fermented yogurt in low-temperature fermentation
- a mixture of 78.2 kg of milk, 2.6 kg of skim milk powder and 17.2 kg of water was prepared, sterilized by heating at 95 ° C for 5 minutes, cooled to about 37 ° C, and the lactic acid bacteria starter (rata Inoculation of 2% by weight of a mixed culture of Tobacillus punoregaricus (L. bulgaricus JCM 1002 T) and Streptococcus thermophilus (S. thermo ⁇ hi 1 us ATCC 19258) was performed. Nitrogen gas was mixed and dispersed in this mix through a pipe to adjust the dissolved oxygen concentration to 3 ppm or less. A control without nitrogen gas replacement was also prepared as a control.
- the lactic acidity was calculated by titration with 0.1 N NaOH and phenolphthalein as an indicator.
- the physical properties of yogurt were measured using a Neo Card Meter M302 (I-Techno Engineering, formerly Iio Denki), and the penetration angle obtained by measuring the penetration angle of the Jodalto knife when a 100 g weight was applied.
- the elasticity up to the break of the angle curve was defined as hardness (g), and the angle was used as a measure of smoothness (the angle takes a value up to 90 °, and the smaller the value, the smoother the tissue can be judged). If the hardness of the yogurt measured by this measuring instrument is 4 Og or more, it can be said that the yarn is a stable yarn and is not broken by impact during transportation.
- the hardness in the case of the method of the present invention was 55 g and the penetration angle was 30 °
- the hardness of the conventional method was 35 g and the penetration angle was 50 °.
- the material had a hardness that was smoother and could maintain the structure at the distribution stage. It was also confirmed that the actual flavor was more dense and smoother than the conventional product.
- FIG. 3 is a diagram showing a method of reading an intrusion angle and hardness from a chart paper measured using a card meter.
- FIG. 4 is a view showing the results of examining the effect of dissolved oxygen in a fermented milk raw material mix on fermentation time.
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Abstract
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Priority Applications (8)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US11/570,356 US9161552B2 (en) | 2004-06-14 | 2005-06-10 | Process for producing fermented milk and fermented milk |
EP05751218.8A EP1759587B1 (en) | 2004-06-14 | 2005-06-10 | Process for producing fermented milk and fermented milk |
KR1020067026317A KR101221146B1 (ko) | 2004-06-14 | 2005-06-10 | 발효유의 제조법 및 발효유 |
CA2570484A CA2570484C (en) | 2004-06-14 | 2005-06-10 | Method for producing fermented milk and fermented milk |
NZ551671A NZ551671A (en) | 2004-06-14 | 2005-06-10 | Method for producing fermented milk and fermented milk by lowering the dissolved oxygen in the raw material mix |
DK05751218.8T DK1759587T3 (da) | 2004-06-14 | 2005-06-10 | Fremgangsmåde til produktion af fermenteret mælk og fermenteret mælk |
AU2005251622A AU2005251622B2 (en) | 2004-06-14 | 2005-06-10 | Process for producing fermented milk and fermented milk |
HK07109712.1A HK1104429A1 (en) | 2004-06-14 | 2007-09-06 | Process for producing fermented milk and fermented milk |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
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JP2004-176185 | 2004-06-14 | ||
JP2004176185A JP3666871B1 (ja) | 2004-06-14 | 2004-06-14 | 発酵乳の製造法及び発酵乳 |
Publications (1)
Publication Number | Publication Date |
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WO2005120240A1 true WO2005120240A1 (ja) | 2005-12-22 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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PCT/JP2005/011089 WO2005120240A1 (ja) | 2004-06-14 | 2005-06-10 | 発酵乳の製造法及び発酵乳 |
Country Status (11)
Country | Link |
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US (1) | US9161552B2 (ja) |
EP (1) | EP1759587B1 (ja) |
JP (1) | JP3666871B1 (ja) |
KR (1) | KR101221146B1 (ja) |
CN (1) | CN100399912C (ja) |
AU (1) | AU2005251622B2 (ja) |
CA (1) | CA2570484C (ja) |
DK (1) | DK1759587T3 (ja) |
HK (1) | HK1104429A1 (ja) |
NZ (2) | NZ585005A (ja) |
WO (1) | WO2005120240A1 (ja) |
Cited By (3)
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WO2007026697A1 (ja) * | 2005-08-30 | 2007-03-08 | Meiji Dairies Corporation | 発酵乳の製造方法及び発酵乳 |
CN101971880A (zh) * | 2010-11-30 | 2011-02-16 | 武汉光明乳品有限公司 | 干酪乳杆菌高含量发酵乳及其制造方法 |
EP2011401B1 (en) | 2006-04-13 | 2016-07-20 | Meiji Co., Ltd | High-snf and/or low-fat fermented milk excellent in savor and process for production thereof |
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JP3666871B1 (ja) * | 2004-06-14 | 2005-06-29 | 明治乳業株式会社 | 発酵乳の製造法及び発酵乳 |
TWI491362B (zh) * | 2006-12-01 | 2015-07-11 | Meiji Co Ltd | 發酵乳之製造方法及發酵乳 |
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TWI392457B (zh) * | 2007-02-12 | 2013-04-11 | Meiji Co Ltd | Milk fat composition with less fat and less and its manufacturing method |
JP5607022B2 (ja) * | 2009-02-25 | 2014-10-15 | 株式会社明治 | 乳糖分の少ない発酵乳及びその製造方法 |
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US9833006B2 (en) * | 2012-04-03 | 2017-12-05 | Cp Kelco Aps | Stable fermented milk products and methods |
WO2015068790A1 (ja) * | 2013-11-08 | 2015-05-14 | 株式会社明治 | 酸度上昇が抑制された発酵乳およびその製造方法 |
SG11201800428VA (en) * | 2015-07-23 | 2018-02-27 | Meiji Co Ltd | Fermented milk and method for producing same |
JPWO2018056455A1 (ja) * | 2016-09-26 | 2019-07-04 | 株式会社明治 | 超高温殺菌処理した材料を含む原料ミックスを用いた発酵乳の製造方法 |
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JP3644505B1 (ja) | 2002-12-03 | 2005-04-27 | 明治乳業株式会社 | 発酵乳の製造法及び発酵乳 |
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2004
- 2004-06-14 JP JP2004176185A patent/JP3666871B1/ja not_active Expired - Lifetime
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2005
- 2005-06-10 KR KR1020067026317A patent/KR101221146B1/ko active IP Right Grant
- 2005-06-10 CA CA2570484A patent/CA2570484C/en not_active Expired - Fee Related
- 2005-06-10 EP EP05751218.8A patent/EP1759587B1/en not_active Not-in-force
- 2005-06-10 NZ NZ585005A patent/NZ585005A/en unknown
- 2005-06-10 DK DK05751218.8T patent/DK1759587T3/da active
- 2005-06-10 WO PCT/JP2005/011089 patent/WO2005120240A1/ja not_active Application Discontinuation
- 2005-06-10 NZ NZ551671A patent/NZ551671A/en unknown
- 2005-06-10 CN CNB200580019139XA patent/CN100399912C/zh active Active
- 2005-06-10 US US11/570,356 patent/US9161552B2/en active Active
- 2005-06-10 AU AU2005251622A patent/AU2005251622B2/en not_active Ceased
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WO2007026697A1 (ja) * | 2005-08-30 | 2007-03-08 | Meiji Dairies Corporation | 発酵乳の製造方法及び発酵乳 |
JP2007060940A (ja) * | 2005-08-30 | 2007-03-15 | Meiji Milk Prod Co Ltd | 発酵乳の製造方法及び発酵乳 |
EP1929875A4 (en) * | 2005-08-30 | 2011-07-27 | Meiji Dairies Corp | PROCESS FOR THE PRODUCTION OF FERMENTED MILK AND FERMENTED MILK |
US8722119B2 (en) | 2005-08-30 | 2014-05-13 | Meiji Co., Ltd. | Process for producing fermented milk |
EP2011401B1 (en) | 2006-04-13 | 2016-07-20 | Meiji Co., Ltd | High-snf and/or low-fat fermented milk excellent in savor and process for production thereof |
EP2011401B2 (en) † | 2006-04-13 | 2022-09-07 | Meiji Co., Ltd. | High-snf and/or low-fat fermented milk excellent in savor and process for production thereof |
CN101971880A (zh) * | 2010-11-30 | 2011-02-16 | 武汉光明乳品有限公司 | 干酪乳杆菌高含量发酵乳及其制造方法 |
Also Published As
Publication number | Publication date |
---|---|
JP2005348703A (ja) | 2005-12-22 |
JP3666871B1 (ja) | 2005-06-29 |
EP1759587A4 (en) | 2009-08-19 |
HK1104429A1 (en) | 2008-01-18 |
CA2570484C (en) | 2014-03-18 |
KR101221146B1 (ko) | 2013-01-10 |
EP1759587A1 (en) | 2007-03-07 |
NZ585005A (en) | 2011-08-26 |
NZ551671A (en) | 2010-10-29 |
AU2005251622A1 (en) | 2005-12-22 |
US20070224314A1 (en) | 2007-09-27 |
CA2570484A1 (en) | 2005-12-22 |
US9161552B2 (en) | 2015-10-20 |
EP1759587B1 (en) | 2014-02-12 |
KR20070022087A (ko) | 2007-02-23 |
DK1759587T3 (da) | 2014-05-05 |
CN100399912C (zh) | 2008-07-09 |
AU2005251622B2 (en) | 2011-10-06 |
CN1972597A (zh) | 2007-05-30 |
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