RU2014134975A - Композиции жестких возобновляемых сложных полиэфиров, имеющие высокую прочность при ударе и высокое удлинение при растяжении - Google Patents
Композиции жестких возобновляемых сложных полиэфиров, имеющие высокую прочность при ударе и высокое удлинение при растяжении Download PDFInfo
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Abstract
1. Смешиваемая в расплаве термопластическая композиция, включающая:по меньшей мере один жесткий возобновляемый сложный полиэфир, температура стеклования которого составляет приблизительно 0°С или более;от приблизительно 1% масс. до приблизительно 30% масс. в пересчете на массу возобновляемого сложного полиэфира по меньшей мере одной полимерной добавки, повышающей ударную прочность;от приблизительно 0,1% масс. до приблизительно 20% масс. в пересчете на массу возобновляемого сложного полиэфира по меньшей мере одного модификатора границы раздела фаз; ипри этом термопластическая композиция имеет морфологию, в которой внутри непрерывной фазы диспергировано множество дискретных первичных доменов, причем домены содержат полимерную добавку, повышающую ударную прочность, а непрерывная фаза содержит возобновляемый сложный полиэфир, и при этом ударная прочность композиции по Изоду, определяемая при 23°С согласно стандарту ASTM D256-10 (Способ А), составляет приблизительно 0,3 Джоуля на сантиметр или более, и удлинение при растяжении в момент разрыва, определяемое при 23°С согласно стандарту ASTM D638-10, составляет приблизительно 10% или более, а также отношение температуры стеклования термопластической композиции к температуре стеклования возобновляемого сложного полиэфира составляет от приблизительно 0,7 до приблизительно 1,3.2. Термопластическая композиция по п. 1, в которой возобновляемый сложный полиэфир представляет собой полимолочную кислоту.3. Термопластическая композиция по п. 1, в которой температура стеклования возобновляемого сложного полиэфира и термопластической композиции составляет от приблизительно 50°С до приблизительно 75°С.4. Термопластическая комп
Claims (19)
1. Смешиваемая в расплаве термопластическая композиция, включающая:
по меньшей мере один жесткий возобновляемый сложный полиэфир, температура стеклования которого составляет приблизительно 0°С или более;
от приблизительно 1% масс. до приблизительно 30% масс. в пересчете на массу возобновляемого сложного полиэфира по меньшей мере одной полимерной добавки, повышающей ударную прочность;
от приблизительно 0,1% масс. до приблизительно 20% масс. в пересчете на массу возобновляемого сложного полиэфира по меньшей мере одного модификатора границы раздела фаз; и
при этом термопластическая композиция имеет морфологию, в которой внутри непрерывной фазы диспергировано множество дискретных первичных доменов, причем домены содержат полимерную добавку, повышающую ударную прочность, а непрерывная фаза содержит возобновляемый сложный полиэфир, и при этом ударная прочность композиции по Изоду, определяемая при 23°С согласно стандарту ASTM D256-10 (Способ А), составляет приблизительно 0,3 Джоуля на сантиметр или более, и удлинение при растяжении в момент разрыва, определяемое при 23°С согласно стандарту ASTM D638-10, составляет приблизительно 10% или более, а также отношение температуры стеклования термопластической композиции к температуре стеклования возобновляемого сложного полиэфира составляет от приблизительно 0,7 до приблизительно 1,3.
2. Термопластическая композиция по п. 1, в которой возобновляемый сложный полиэфир представляет собой полимолочную кислоту.
3. Термопластическая композиция по п. 1, в которой температура стеклования возобновляемого сложного полиэфира и термопластической композиции составляет от приблизительно 50°С до приблизительно 75°С.
4. Термопластическая композиция по п. 1, в которой отношение параметра растворимости возобновляемого сложного полиэфира к параметру растворимости полимерной добавки, повышающей ударную прочность, составляет от приблизительно 0,5 до приблизительно 1,5.
5. Термопластическая композиция по п. 4, в которой параметр растворимости полимерной добавки, повышающей ударную прочность, составляет от приблизительно 15 до приблизительно 30 МДж1/2/м3/2.
6. Термопластическая композиция по п. 1, в которой отношение скорости течения расплава возобновляемого сложного полиэфира к скорости течения расплава полимерной добавки, повышающей ударную прочность, составляет от приблизительно 0,2 до приблизительно 8.
7. Термопластическая композиция по п. 1, в которой отношение модуля упругости по Юнгу возобновляемого сложного полиэфира к модулю упругости по Юнгу полимерной добавки, повышающей ударную прочность, составляет от приблизительно 2 до приблизительно 500.
8. Термопластическая композиция по п. 1, в которой полимерная добавка, повышающая ударную прочность, включает полиолефин, например, пропиленовый гомополимер, сополимер пропилена и α-олефина, сополимер этилена и α-олефина или комбинацию перечисленных соединений.
9. Термопластическая композиция по п. 1, в которой кинематическая вязкость модификатора границы раздела фаз, определяемая при температуре 40°С, составляет от приблизительно 0,7 до приблизительно 200 сантиСтокс.
10. Термопластическая композиция по п. 1, в которой модификатор границы раздела фаз представляет собой гидрофобное вещество.
11. Термопластическая композиция по п. 1, в которой модификатор границы раздела фаз представляет собой кремнийорганический полимер, сополимер кремнийорганического соединения и простого полиэфира, алифатический сложный полиэфир, ароматический сложный полиэфир, алкиленгликоль, алкандиол, аминоксид, сложный эфир жирной кислоты или комбинацию перечисленных соединений.
12. Термопластическая композиция по п. 1, в которой длина дискретных доменов составляет от приблизительно 0,05 микрометров до приблизительно 30 микрометров.
13. Термопластическая композиция по п. 1, дополнительно включающая агент, улучшающий совместимость, полиэпоксидный модификатор или оба эти компонента.
14. Термопластическая композиция по п. 1, в которой композиция содержит полиэпоксидный модификатор, который включает функционализированный эпоксидом акриловый и/или метакриловый мономерный компонент, например, сополимер этилена, метилакрилата и глицидилметакрилата.
15. Термопластическая композиция по п. 1, в которой возобновляемый сложный полиэфир составляет приблизительно 70% масс. или более термопластической композиции.
16. Термопластическая композиция по п. 1, отличающаяся тем, что ударная прочность по Изоду образца композиции с надрезом, определяемая при 23°С в соответствии со стандартом ASTM D256-10 (Способ А), составляет от приблизительно 0,8 Дж/см до приблизительно 2,5 Дж/см.
17. Термопластическая композиция по п. 1, отличающаяся тем, что удлинение композиции при растяжении в момент разрыва, определяемое при 23°С в соответствии со стандартом ASTM D638-10, составляет от приблизительно 100% до приблизительно 300%.
18. Полученное литьем под давлением изделие, включающее термопластическую композицию по любому из предшествующих пунктов.
19. Полученное литьем под давлением изделие, которое сформовано из термопластической композиции, где термопластическая композиция включает приблизительно 70% масс. или более по меньшей мере одной полимолочной кислоты, температура стеклования которой составляет приблизительно 0°С или более, от приблизительно 0,1% масс. до приблизительно 30% масс. по меньшей мере одной полимерной добавки, повышающей ударную прочность, и от приблизительно 0,1% масс. до приблизительно 20% масс. по меньшей мере одного модификатора границы раздела фаз, и при этом ударная прочность по Изоду формованного изделия, определяемая при 23°С в соответствии со стандартом ASTM D256-10 (Способ А), составляет приблизительно 0,3 Джоуля на сантиметр или более, и удлинение при растяжении в момент разрыва, определяемое при 23°С в соответствии со стандартом ASTM D638-10, составляет приблизительно 10% или более.
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US13/370,869 US8975305B2 (en) | 2012-02-10 | 2012-02-10 | Rigid renewable polyester compositions having a high impact strength and tensile elongation |
US13/370,869 | 2012-02-10 | ||
PCT/IB2013/050730 WO2013118020A1 (en) | 2012-02-10 | 2013-01-28 | Rigid renewable polyester compositions having a high impact strength and tensile elongation |
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RU2014134975A true RU2014134975A (ru) | 2016-03-27 |
RU2618275C2 RU2618275C2 (ru) | 2017-05-03 |
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US (2) | US8975305B2 (ru) |
EP (1) | EP2812396B1 (ru) |
JP (1) | JP2015507055A (ru) |
KR (1) | KR102004013B1 (ru) |
CN (1) | CN104105757B (ru) |
AU (1) | AU2013217363B2 (ru) |
BR (1) | BR112014019541B1 (ru) |
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MX344653B (es) | 2017-01-03 |
RU2618275C2 (ru) | 2017-05-03 |
EP2812396A1 (en) | 2014-12-17 |
EP2812396A4 (en) | 2015-09-16 |
CN104105757A (zh) | 2014-10-15 |
US20150152261A1 (en) | 2015-06-04 |
US10144825B2 (en) | 2018-12-04 |
KR102004013B1 (ko) | 2019-07-25 |
US8975305B2 (en) | 2015-03-10 |
KR20140124764A (ko) | 2014-10-27 |
JP2015507055A (ja) | 2015-03-05 |
WO2013118020A1 (en) | 2013-08-15 |
BR112014019541A2 (pt) | 2017-06-20 |
EP2812396B1 (en) | 2019-09-04 |
BR112014019541A8 (pt) | 2017-07-11 |
CN104105757B (zh) | 2016-09-07 |
AU2013217363A1 (en) | 2014-07-24 |
MX2014009533A (es) | 2014-09-04 |
BR112014019541B1 (pt) | 2021-06-29 |
AU2013217363B2 (en) | 2016-04-07 |
US20130210983A1 (en) | 2013-08-15 |
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