KR970065526A - 이미노옥사디아진 디온기를 함유하는 이소시아네이트 삼량체, 그의 제조 방법 및 용도 - Google Patents

이미노옥사디아진 디온기를 함유하는 이소시아네이트 삼량체, 그의 제조 방법 및 용도 Download PDF

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KR970065526A
KR970065526A KR1019970010220A KR19970010220A KR970065526A KR 970065526 A KR970065526 A KR 970065526A KR 1019970010220 A KR1019970010220 A KR 1019970010220A KR 19970010220 A KR19970010220 A KR 19970010220A KR 970065526 A KR970065526 A KR 970065526A
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mole
polyisocyanate
isocyanate
formula
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KR100453869B1 (ko
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프랑크 리히터
요제프 페다인
하랄트 메르테스
칼-게르트 디리스
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볼프강 페트로비키, 만프레트 조벨
바이엘 악티엔게젤샤프트
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
    • C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
    • C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
    • C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
    • C07D251/30—Only oxygen atoms
    • C07D251/32—Cyanuric acid; Isocyanuric acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D273/00—Heterocyclic compounds containing rings having nitrogen and oxygen atoms as the only ring hetero atoms, not provided for by groups C07D261/00 - C07D271/00
    • C07D273/02—Heterocyclic compounds containing rings having nitrogen and oxygen atoms as the only ring hetero atoms, not provided for by groups C07D261/00 - C07D271/00 having two nitrogen atoms and only one oxygen atom
    • C07D273/04—Six-membered rings
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/02—Polymeric products of isocyanates or isothiocyanates of isocyanates or isothiocyanates only
    • C08G18/022—Polymeric products of isocyanates or isothiocyanates of isocyanates or isothiocyanates only the polymeric products containing isocyanurate groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
    • C08G18/78—Nitrogen
    • C08G18/7875—Nitrogen containing heterocyclic rings having at least one nitrogen atom in the ring
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
    • C08G18/78—Nitrogen
    • C08G18/79—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates
    • C08G18/791—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates containing isocyanurate groups

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Image Analysis (AREA)
  • Adhesives Or Adhesive Processes (AREA)

Abstract

본 발명은 i) 삼량체 30 내지 100몰%가 하기 화학식 (2)의 이미노옥사디아진 디온이고, ⅱ) 삼량체 0 내지 70몰%가 하기 화학식 (1)의 이소시아누레이트이고, ⅲ) 폴리이소시아네이트 혼합물의 10% 미만이 우레트온이민 구조형이고, ⅳ) 우레트디온의 몰 %에 대한 화학식 (1)과 (2)의 삼량체의 전체 몰%의 비율이 4:1 초과인, 이소시아네이트 살량체를 함유하는 폴리이소시아네이트 혼합물에 관한 것이다.
상기 식 중, R1, R2및 R3은 동일하거나 또는 상이하며, NCO함량이 70% 미만인 지방족, 시클로지방족, 방향족 및(또는) 아르알리파틱 이소시아네이트 및(또는) 이들의 올리고모로부터 이소시아네이트기를 제거하여 얻은 기를 나타낸다.
본 발명은 또한 상기 이소시아네이트 살량체, 상기 이소시아네이트 삼량체와 다른 폴리이소시아네이트와의 혼합물 및 상기 이소시아네이트 삼량체(여기서, 이소시아네이트기는 임의로 차단제에 의해 차단될 수 있음) 및 2종 이상의 이소시아네이트 반응성 기를 함유하는 화합물을 함유하는 조성물의 제조 방법에 관한 것이다.

Description

아미노옥사디아진 디온기를 함유하는 이소시아네이트 삼량체, 그의 제조 방법 및 용도
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (6)

  1. ⅰ) 삼량체 30 내지 100몰%가 하기 화학식 (2)의 아미노록사디아진 디온이고, ⅱ) 삼량체 0 내지 70몰%가 하기 화학식 (1)의 이소시아누레이트이고, ⅲ) 폴리이소시아네이트 혼합물의 10몰% 미만이 하기 화학식 (7)의 우레트온 이민 구조형이고, ⅳ) 하기 화학식 (6)의 우레트디온의 몰%에 대한 화학식 (1)과 (2)의 삼량체의 전체 몰%의 비율이 4:1 초과인, 이소시아네이트 삼량체를 함유하는 폴리이소시아네이트 혼합물.
    상기 식 중, R1,R2및 R3은 동일하거나 또는 사이하며, NCO함량이 70% 미만인 지방족, 시클로지방족, 방향족 및(또는) 아르알리파틱 이소시아네이트 및(또는) 이들의 올리고머로부터 이소시아네이트기를 제거하여 얻은 기를 나타낸다.
  2. 제1항에 있어서, R1,R2및 R3이 (시클로)지방족 디이소시아네이트 및 (또는)그의 올리고머로부터 이소시아네이트기를 제거하여 얻은 기를 나타내는 것인 폴리이소시아네이트 혼합물.
  3. 제1항에 있어서, R1,R2및 R3이 1,6-헥사메틸렌 디이소시아네이트 및(또는) 이소포론 디이소시아네이트 및(또는) 이들의 올리고머로부터 이소시아네이트기를 제거하여 얻은 기를 나타내는 것인 폴리이소시아네이트 혼합물.
  4. NCO 함량이 75% 미만인 지방족, 시클로지방족, 방향족 및(또는) 아르알리파틱 이소시아네이트의 이소시아네이트기의 적어도 일부를 화학식 M〔nF-(HF)m〕(식 중, M은 n가 양이온 또는 n가 라디칼이고, m/n〉0임)에 상응하는 수소 (폴리)플루오라이드 촉매의 존재하에 삼량체화시키고, 삼량체화 반응을 목적하는 정도에서 종결시키고, 임의로 미반응 이소시아네이트를 제거하는 것으로 이루어지는, 제1항 기재의 폴리이소시아네이트 혼합물의 제조 방법.
  5. 제1항 기재의 폴리이소시아네이트 혼합물과 함께 우레탄, 알로파네이트, 우레아, 비우레트, 우레트디온 및(또는) 옥사디아진 트리온기를 함유하는 1종 이상의 폴리이소시아네이트를 함유하는 조성물.
  6. 이소시아네이트기가 차단제에 의해 임의로 차단될 수 있는 제1항 기재의 폴리이소시아네이트 혼합물 및 2종 이상의 이소시아네이트 반응성 기를 함유하는 화합물을 함유하는 조성물.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019970010220A 1996-03-26 1997-03-25 이미노옥사디아진디온기를함유하는이소시아네이트삼량체,그의제조방법및용도 KR100453869B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19611849A DE19611849A1 (de) 1996-03-26 1996-03-26 Neue Isocyanattrimerisate und Isocyanattrimerisatmischungen, deren Herstellung und Verwendung
DE19611849.2 1996-03-26

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KR970065526A true KR970065526A (ko) 1997-10-13
KR100453869B1 KR100453869B1 (ko) 2004-12-30

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US (1) US5914383A (ko)
EP (1) EP0798299B1 (ko)
JP (1) JP3995300B2 (ko)
KR (1) KR100453869B1 (ko)
AT (1) ATE248154T1 (ko)
CA (1) CA2200823C (ko)
DE (2) DE19611849A1 (ko)
DK (1) DK0798299T3 (ko)
ES (1) ES2205081T3 (ko)
PT (1) PT798299E (ko)

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ES2205081T3 (es) 2004-05-01
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DE19611849A1 (de) 1997-10-02
PT798299E (pt) 2004-01-30
JPH09268212A (ja) 1997-10-14
US5914383A (en) 1999-06-22
EP0798299B1 (de) 2003-08-27
CA2200823A1 (en) 1997-09-26
JP3995300B2 (ja) 2007-10-24
DE59710635D1 (de) 2003-10-02
MX9702231A (es) 1997-09-30
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EP0798299A1 (de) 1997-10-01
CA2200823C (en) 2005-10-04

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